Liquid crystal compound having difluoromethyleneoxy, liquid crystal composition and liquid crystal display device
US-2015376502-A1 · Dec 31, 2015 · US
US8952175B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-8952175-B2 |
| Application number | US-45234708-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 27, 2008 |
| Priority date | Jun 27, 2007 |
| Publication date | Feb 10, 2015 |
| Grant date | Feb 10, 2015 |
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There is provided a novel intermediate for producing pesticides. A method for producing the compound of Formula (3) comprises reacting an aromatic ketone compound of Formula (4) and a substituted acetophenone compound of Formula (5) as starting raw materials in an organic solvent or water in the presence or absence of an additive in the presence of a base in a suspended state. A method may comprise dehydrating the compound of Formula (3). A method for producing compound (2) in one step comprises reacting compound (4) and compound (5) to obtain compound (3). Further, a method for producing an isoxazoline compound of Formula (1) comprises reacting compound (2) and a hydroxylamine in an aliphatic or an aromatic hydrocarbon solvent which is optionally substituted by a halogen atom by adding an additive selected from a phase-transfer catalyst, a C 1 -C 6 alcohol and an aprotic polar solvent in the presence of a base and water.
Opening claim text (preview).
The invention claimed is: 1. A method for producing an isoxazoline compound represented by Formula (1): wherein R 1 , R 2 , X, A 1 , A 2 , A 3 , A 4 , A 5 , A 6 and A 7 represent the same meaning as described below), the method comprising reacting a 1,3-bis(substituted phenyl)-3-substituted-2-propen-1-one compound represented by Formula (2):…
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
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Chemistry & Metallurgy · mapped topic
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