Reductive preparation of tertiary dimethylamines from nitriles
US-2016368856-A1 · Dec 22, 2016 · US
US8946459B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-8946459-B2 |
| Application number | US-201213598685-A |
| Country | US |
| Kind code | B2 |
| Filing date | Aug 30, 2012 |
| Priority date | Aug 31, 2011 |
| Publication date | Feb 3, 2015 |
| Grant date | Feb 3, 2015 |
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A process for reacting ethylenediamine-formaldehyde adduct (EDFA) and/or ethylene-diamine-monoformaldehyde adduct (EDMFA) with hydrogen cyanide (HCN) in a reactor with limited backmixing at a temperature in the range from 20 to 120° C., wherein the residence time in the reactor is 300 seconds or less.
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The invention claimed is: 1. A process which comprises reacting ethylenediamine-formaldehyde adduct (EDFA) and/or ethylenediamine-monoformaldehyde adduct (EDMFA) with hydrogen cyanide (HCN) in a reactor with limited backmixing at a temperature in the range from 20 to 120° C., wherein the residence time in the reactor is 300 seconds or less. 2. The process according to claim 1 , wherein the residence time in the reactor is less than 60 seconds.…
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
Chemistry & Metallurgy · mapped topic
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