Sintered body production method
US-2024307956-A1 · Sep 19, 2024 · US
US2025277295A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2025277295-A1 |
| Application number | US-202519209906-A |
| Country | US |
| Kind code | A1 |
| Filing date | May 16, 2025 |
| Priority date | Dec 12, 2022 |
| Publication date | Sep 4, 2025 |
| Grant date | — |
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New 5xxx aluminum alloy sheet products and methods for making the same are disclosed. The new 5xxx aluminum alloy sheet products may realize a low yield point elongation (YPE) thereby facilitating reduction or elimination of Type A Lüdering (stretcher-strain lines). The new 5xxx aluminum alloy sheet products may be hot rolled into an intermediate gauge product, then cold rolled to a final gauge product, wherein no intermediate annealing occurs prior to or during the cold rolling, and then post cold roll annealing at a temperature and for a time sufficient to first realize a recovered but unrecrystallized microstructure, and then converting of at least some of the recovered but unrecrystallized microstructure to a recrystallized microstructure via a second annealing operation of the post cold roll annealing step.
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What is claimed is: 1 . A method comprising: (a) hot rolling a 5xxx aluminum alloy to an intermediate gauge product; (b) after the hot rolling step, conducting a cold rolling operation to achieve a final gauge product, wherein the cold rolling operation includes at least one cold rolling step, and wherein no intermediate annealing occurs prior to or during the cold rolling operation; (c) after the cold rolling operation, post cold roll annealing the final gauge product, wherein the post cold roll annealing step (c) comprises: (i) first annealing at a first temperature for a first duration, wherein, due to the first annealing step, the final gauge product contains a recovered but unrecrystallized microstructure; and (ii) after the first annealing step, applying a second annealing step to the final gauge product, thereby converting at least some of the recovered but unrecrystallized microstructure to a recrystallized microstructure. 2 . The method of claim 1 , wherein the post cold roll annealing step comprises annealing the final gauge product at a temperature and for a time sufficient for the final gauge product to realize a YPE of not greater than 0.60%. 3 . The method of claim 2 , wherein the final gauge product realizes at least one of: (A) an area weighted average grain size of not greater than 40 micrometers; (B) a Brass texture amount of not greater than 14%; and (C) an S texture amount of not greater than 19%. 4 . The method of claim 3 , wherein, due to the second annealing step, the final gauge product realizes at least two of (A), (B) and (C). 5 . The method of claim 1 , wherein the final gauge product realizes an area weighted average grain size of from 15 to 39 micrometers. 6 . The method of claim 5 , wherein the final gauge product realizes a Brass texture amount of from 1% to 13%. 7 . The method of claim 6 , wherein the final gauge product realizes an S texture amount of from 5% to 18%, or an S texture amount of not greater than 17%, or an S texture amount of not greater than 16%, or an S texture amount of not greater than 15%, or an S texture amount of not greater than 14%. 8 . The method of claim 1 , wherein the second temperature is at least 25° F. higher than the first temperature; wherein the first duration is at least 30 minutes; wherein the second duration is at least 1 second. 9 . The method of claim 8 , wherein the first temperature is below a recrystallization temperature of the final gauge product, and wherein the second temperature is above the recrystallization temperature of the final gauge product. 10 . The method of claim 9 , wherein the first temperature is from 350° F. to 500° F. 11 . The method of claim 10 , wherein the first duration is from at least 1 hour to not greater than 10 days. 12 . The method of claim 11 , wherein the second temperature is from greater than 500° F. to 900° F. 13 . The method of claim 12 , wherein the second duration is from 5 seconds to 48 hours. 14 . The method of claim 1 , wherein the cold rolling operation is accomplished with a single cold rolling pass. 15 . The method of claim 1 , wherein the cold rolling operation is accomplished with multiple cold rolling passes. 16 . The method of claim 1 , wherein the cold rolling operation comprises reducing a thickness of the intermediate gauge product by from 25% to 80%. 17 . The method of claim 1 , wherein the hot rolling comprises hot rolling an ingot or a continuously cast strip of the 5xxx aluminum alloy. 18 . A 5xxx aluminum alloy sheet product comprising from 4.0 to 6.0 wt. % Mg and having a thickness of from 0.5 to 5.0 mm, wherein the 5xxx aluminum alloy sheet product is at least 60% recrystallized and realizes an YPE of not greater than 0.60%; wherein the 5xxx aluminum alloy sheet product realizes at least one of: (A) an area weighted average grain size of not greater than 40 micrometers; (B) a Brass texture amount of not greater than 14%; and (C) an S texture amount of not greater than 19%. 19 . The 5xxx aluminum alloy sheet product of claim 18 , comprising: from 4.0 to 5.0 wt. % Mg up to 0.50 wt. % Mn; up to 0.75 wt. % Zn; up to 0.35 wt. % Fe; up to 0.20 wt. % Si; up to 0.15 wt. % Cu; up to 0.10 wt. % Cr; up to 0.10 wt. % Ti; the balance being aluminum, optional incidental elements and impurities. 20 . The 5xxx aluminum alloy sheet product of claim 19 , wherein the 5xxx aluminum alloy includes at least 0.25 wt. % Zn, or at least 0.30 wt. % Zn, or at least 0.35 wt. % Zn, or at least 0.40 wt. % Zn, or at least 0.45 wt. % Zn, or at least 0.50 wt. % Zn.
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