Titanium Porous Body and Method for Producing Titanium Porous Body

Patent metadata

Field	Value
Publication number	US-2025073778-A1
Application number	US-202218718084-A
Country	US
Kind code	A1
Filing date	Nov 24, 2022
Priority date	Dec 27, 2021
Publication date	Mar 6, 2025
Grant date	—

Abstract

The titanium porous body according to the present invention is in a form of a sheet, and has a thickness of 0.3 mm or less and a compressive strain amount of 0.20 or less upon pressurization at 80 MPa, wherein a half width of a first peak that is the highest peak height in a pore size distribution showing a relationship between a diameter and a volume of pores is less than or equal to 3.5 μm, and a peak height of a second peak that is the second highest peak height after the first peak is less than or equal to 10% of the peak height of the first peak.

First claim

1 . A titanium porous body in a form of a sheet, wherein:
the titanium porous body has a thickness of 0.3 mm or less and a compressive strain amount of 0.20 or less upon pressurization at 80 MPa; and a half width of a first peak that is the highest peak height in a pore size distribution showing a relationship between a diameter and a volume of pores is less than or equal to 3.5 μm, and a peak height of a second peak that is the second highest peak height after the first peak is less than or equal to 10% of the peak height of the first peak.

2 . The titanium porous body according to claim 1 , wherein the titanium porous body has a pore diameter of less than or equal to 10.0 μm at a position where the first peak appears in the pore size distribution.

3 . The titanium porous body according to claim 1 , wherein the titanium porous body has a porosity of less than or equal to 45%.

4 . The titanium porous body according to claim 1 , wherein the titanium porous body has an area of more than or equal to 10000 mm 2 .

5 . The titanium porous body according to claim 1 , wherein the titanium porous body has a Ti content of more than or equal to 98% by mass.

6 . The titanium porous body according to claim 1 , wherein the peak height of the second peak is less than or equal to 5% of the peak height of the first peak.

7 . A method for producing a titanium porous body in a form of a sheet by heating and sintering titanium powder on a molding surface of a mold, the method comprising:
a powder preparation step of preparing titanium powder having a 10% particle diameter D10 of 5 μm or more and 15 μm or less and a 90% particle diameter D90 of 15 μm or more and 25 μm or less; a mold release layer formation step of forming no mold release layer on an adhesive region of an outer edge portion of the molding surface but forming the mold release layer on an easily releasable region other than the adhesive region; after the mold release layer formation step, a powder deposition step of depositing the titanium powder on the molding surface in a dry process; after the powder deposition step, a heating step of heating the titanium powder to a maximum reaching temperature of more than or equal to 950° C. and sintering the titanium powder to obtain a sintered body; and after the heating step, a cooling step of cooling the sintered body on the molding surface, wherein a time required for cooling from at least 950° C. to 800° C. is less than or equal to 1500 seconds; and wherein the method produces a titanium porous body having a thickness of less than or equal to 0.3 mm.

8 . The method for producing a titanium porous body according to claim 7 , wherein the method produces the titanium porous body having an area of more than or equal to 10000 mm 2 .

9 . The method for producing a titanium porous body according to claim 7 , wherein the titanium powder prepared in the powder preparation step has an average circularity of less than or equal to 0.83.

10 . The method for producing a titanium porous body according to claim 7 , wherein a material of the mold having the molding surface comprises at least one selected from the group consisting of carbon, quartz, graphite, magnesia (MgO), calcia (CaO), zirconia (ZrO 2 ) and yttria (Y 2 O 3 ).

11 . The method for producing a titanium porous body according to claim 7 , wherein a time for bringing the titanium powder to more than or equal to 950° C. in the heating step be from 30 to 480 minutes.

Assignees

• Toho Titanium Co Ltd

Inventors

• Inoue Yosuke

Classifications

• B22F5/006

  of flat products, e.g. sheets (B22F3/1103 takes precedence; by using pressure rollers only see B22F3/18) · CPC title

• B22F3/1017

  Multiple heating or additional steps (B22F3/101 takes precedence) · CPC title

• B22F3/1109

  Inhomogenous pore distribution (composite layers of porous nature B22F7/002) · CPC title

• B22F7/008

  characterised by the composition · CPC title

• C22C1/0458

  Alloys based on titanium, zirconium or hafnium · CPC title