Short-path evaporation processes

Patent metadata

Field	Value
Publication number	US-2025049061-A1
Application number	US-202218721672-A
Country	US
Kind code	A1
Filing date	Dec 20, 2022
Priority date	Dec 21, 2021
Publication date	Feb 13, 2025
Grant date	—

Abstract

The present invention relates to effective processes for removing impurities from an edible fat, such as an edible butter or an edible oil, where the processes comprise the step of subjecting the edible fat to a short-path evaporation process and do not comprise the step of degumming the edible fat.

First claim

1 . A process for removing impurities from an edible fat, wherein the edible fat is a cocoa butter, a shea butter, a mango kernel oil, an illipe nut oil or a sal nut oil, the process comprising the step of subjecting the edible fat to a short-path evaporation on a short-path evaporation equipment having an evaporator surface, wherein the short-path evaporation is performed:
at a pressure of below 1 mbar; at an evaporator temperature in the range of from 80 to 280° C.; and, with a feed rate per unit area of the evaporator surface of the short-path evaporation equipment in the range of from 5 to 500 kg/h·m 2 ; to form a retentate edible fat and a distillate;
wherein the process does not comprise the step of degumming the edible fat.

2 . The process of claim 1 , wherein the edible fat is a cocoa butter.

3 . The process of claim 1 , wherein the edible fat is a crude edible fat, wherein the crude edible fat has not previously been refined.

4 . The process of claim 3 , wherein the crude edible fat has not previous been deodorized, or bleached, or degummed, or deodorized and bleached, or deodorized and degummed, or bleached and degummed, or deodorized, and bleached and degummed.

5 . The process of claim 1 , wherein the process removes free fatty acids (FFA) from the edible fat.

6 . The process of claim 1 , wherein the process removes diacyl glycerides (DAG) from the edible fat.

7 . The process of claim 1 , wherein the process reduces the Aroma Index of the starting material by at least 70%, as expressed by the Aroma Index method.

8 . The process of claim 1 , wherein the short-path evaporation is performed at a pressure below 0.01 mbar.

9 . The process of claim 1 , wherein the short-path evaporation is performed at a temperature of from 80 to 140° C.

10 . The process of claim 1 , wherein the short-path evaporation is performed at a temperature of from 140 to 220° C.

11 . The process of claim 1 , wherein the short-path evaporation is performed at a temperature of from 220 to 280° C.

12 . The process of claim 1 , wherein the process does not comprise the step of deodorizing the edible fat by treatment with steam; optionally, wherein the process does not comprise the step of deodorizing the edible fat by treatment with steam at a temperature of from 160 to 280° C.

13 . The process of claim 1 , wherein the short-path evaporation is performed under the following conditions:
an operating pressure of 0.001 mbar (plus or minus 10%) and an operating temperature of from 120 to 140° C.; or, an operating pressure of 0.01 mbar (plus or minus 10%) and an operating temperature of from 130 to 150° C.; or, an operating pressure of 0.1 mbar (plus or minus 10%) and an operating temperature of from 150 to 170° C.

14 . The process of claim 1 , wherein the process does not comprise the step of bleaching the edible fat.

15 . The process of claim 1 , wherein the process does not comprise the step of drying the edible fat.

16 . The process of claim 1 , wherein the process consists of subjecting the edible fat to a short-path evaporation, after filtering the edible fat to remove solid matter.

17 . A retentate edible fat obtained from, or obtainable from, the process of claim 1 .

18 . A method of using short-path evaporation on an edible fat, wherein the short-path evaporation conditions comprise a pressure below 1 mbar, a temperature of from 80 to 280° C., and a feed rate per unit area of the evaporator surface of a short-path evaporation equipment of from 5 kg/h·m 2 to 500 kg/h·m 2 , wherein the short-path evaporation reduces free fatty acids (FFA) content from the edible fat, wherein the edible fat is a cocoa butter, a shea butter, a mango kernel oil, an illipe nut oil or a sal nut oil.

19 . The method according to claim 18 , wherein the use does not comprise degumming the edible fat.

20 . The method use according to claim 18 , wherein the edible fat is a cocoa butter.

21 - 24 . (canceled)

Assignees

• Cargill Inc

Inventors

• Bruese Falk
• Lykomitros Dimitris
• Van Rossum Gijsbertus Johannes

Classifications

• C11B3/12 Primary

  by distillation · CPC title

• B01D3/12

  Molecular distillation · CPC title

• A23D9/02

  characterised by the production or working-up · CPC title

• C11B3/001

  by a combination of two or more of the means hereafter · CPC title

• C11B3/008

  by filtration, e.g. including ultra filtration, dialysis (C11B3/005 takes precedence) · CPC title