Method of producing a liquid tobacco extract

Patent metadata

Field	Value
Publication number	US-2025031747-A1
Application number	US-202418911021-A
Country	US
Kind code	A1
Filing date	Oct 9, 2024
Priority date	Jun 5, 2019
Publication date	Jan 30, 2025
Grant date	—

Abstract

A method of producing a liquid tobacco extract is provided, including: preparing a tobacco starting material including natural tobacco material; heating the tobacco starting material in a non-sealed extraction chamber at an extraction temperature of between 125° C. and 160° C. for between 90 minutes and 270 minutes to release gaseous volatile compounds from the tobacco starting material, the tobacco starting material not being in a liquid suspension during the heating step, a flow of inert gas being passed through the tobacco starting material during the heating in the extraction chamber, and the inert gas carrying the gaseous volatile compounds released from the tobacco starting material during heating away from the chamber; collecting the volatile compounds released and carried away from the tobacco starting material by the inert gas flow during the heating; and forming a liquid tobacco extract including the collected volatile compounds.

First claim

1 . A method of producing a liquid tobacco extract, the method comprising the steps of:
preparing a tobacco starting material comprising natural tobacco material; heating the tobacco starting material in a non-sealed extraction chamber at an extraction temperature of between 125 degrees Celsius and 160 degrees Celsius for between 90 minutes and 270 minutes to release gaseous volatile compounds from the tobacco starting material, wherein the tobacco starting material is not in a liquid suspension during the heating step, wherein a flow of inert gas is passed through the tobacco starting material during the heating step in the non-sealed extraction chamber, and wherein the inert gas carries the gaseous volatile compounds released from the tobacco starting material during heating away from the non-sealed extraction chamber; collecting the volatile compounds released and carried away from the tobacco starting material by the inert gas flow during the heating step; and forming a liquid tobacco extract comprising the collected volatile compounds.

2 . The method according to claim 1 , wherein the tobacco starting material is heated at an extraction temperature of between 125 degrees Celsius and 140 degrees Celsius.

3 . The method according to claim 2 , wherein the tobacco starting material is heated at the extraction temperature for at least 120 minutes.

4 . The method according to claim 2 , wherein the extraction temperature is selected to provide a liquid tobacco extract having a nicotine content of at least 0.2 percent by weight based on dry weight.

5 . The method according to claim 2 , wherein the extraction temperature is selected to provide a ratio by weight of (β-ionone+β-damascenone) to (phenol) of at least about 0.25.

6 . The method according to claim 2 , wherein the extraction temperature is selected to provide a ratio by weight of (furaneol+(2,3-diethyl-5-methylpyrazine)*100)) to (nicotine) of at least about 5×10 −4 .

7 . The method according to claim 1 , wherein the tobacco starting material is impregnated with an aerosol former before the heating step.

8 . The method according to claim 1 , wherein the volatile compounds are collected by condensation.

9 . The method according to claim 1 , wherein the volatile compounds are collected by absorption into a liquid solvent comprising an aerosol former.

10 . The method according to claim 9 , wherein the aerosol former comprises glycerin, propylene glycol, or a combination thereof.

11 . The method according to claim 1 , further comprising the step of drying or concentrating the collected volatile compounds.

12 . The method according to claim 1 , wherein the step of preparing the tobacco starting material comprises grinding the tobacco material to form a tobacco powder.

13 . A method of producing a liquid tobacco extract, the method comprising the steps of:
preparing a tobacco starting material comprising natural tobacco material; heating the tobacco starting material at an extraction temperature of between 125 degrees Celsius and 160 degrees Celsius for between 90 minutes and 270 minutes to release gaseous volatile compounds from the tobacco starting material, wherein a flow of inert gas is passed through the tobacco starting material during the heating step, and wherein the inert gas carries away the gaseous volatile compounds released from the tobacco starting material during heating; collecting the volatile compounds released and carried away from the tobacco starting material by the inert gas flow during the heating step; and forming a liquid tobacco extract comprising the collected volatile compounds.

Assignees

• Philip Morris Products Sa

Inventors

• Biasioli Matteo
• Farine Marie
• Frauendorfer Felix
• Kuc Jagoda
• Lanaspeze Sebastien
• Lauenstein Stefan
• Mivelaz Benoit
• Raphoz Christel
• Silvestrini Patrick Charles
• Tzimoulis Steve

Classifications

• A24B15/26

  Use of organic solvents for extraction · CPC title

• A24B15/243

  Nicotine · CPC title

• A24B7/00

  Cutting tobacco · CPC title

• B01D5/00

  Condensation of vapours; Recovering volatile solvents by condensation (B01D8/00 takes precedence; condensers F28B) · CPC title

• B01D11/00

  Solvent extraction · CPC title