Solid-state structures with volatile sintering aids, and methods for fabrication and use thereof
US-2024429439-A1 · Dec 26, 2024 · US
US2024216881A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2024216881-A1 |
| Application number | US-202218577250-A |
| Country | US |
| Kind code | A1 |
| Filing date | Jun 22, 2022 |
| Priority date | Aug 2, 2021 |
| Publication date | Jul 4, 2024 |
| Grant date | — |
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In a reaction apparatus, a reaction furnace is cylindrical and includes a supply port for receiving a raw material to be supplied at one end and a discharge port for discharging a reaction product at another end. A temperature control region includes an apparatus for controlling a temperature of the reaction furnace. A screw extends from the one end of the reaction furnace to the other end and is configured to be able to convey the raw material toward the discharge port by rotating. A first fluid control region includes a first fluid inlet and outlet for allowing a first fluid to pass through the reaction furnace in a predetermined region in the intermediate part. A second fluid control region includes a second fluid inlet and outlet for allowing a second fluid to pass through a region different from the first fluid control region in the intermediate part.
Opening claim text (preview).
1 . A reaction apparatus comprising: a cylindrical reaction furnace including a supply port configured to receive a raw material to be supplied at one end and a discharge port configured to discharge a reaction product at another end; a temperature control region including a heating apparatus or a cooling apparatus configured to control a temperature of the reaction furnace at a predetermined position in an intermediate part between the supply port and the discharge port; a screw extending from the one end of the reaction furnace to the other end thereof configured to be able to convey the raw material supplied from the supply port toward the discharge port by rotating; a first fluid control region including a first fluid inlet and a first fluid outlet configured to allow a first fluid to pass through the reaction furnace in a predetermined region in the intermediate part; and a second fluid control region including a second fluid inlet and a second fluid outlet configured to allow a second fluid to pass through a region different from the first fluid control region in the intermediate part. 2 . The reaction apparatus according to claim 1 , further comprising a screw drive apparatus configured to vary a rotational speed of the screw. 3 . The reaction apparatus according to claim 1 , wherein the screw has a structure in which a pitch of projections for conveying the raw material varies in a convey direction. 4 . The reaction apparatus according to claim 1 , wherein the screw including a projection having a surface or arrangement forming an angle in a range of 0 degrees to 180 degrees with respect to the convey direction for the purpose of retaining, stirring, mixing, kneading, or grinding the raw material. 5 . The reaction apparatus according to claim 1 , further comprising a plurality of the screws arranged in parallel inside the reaction furnace. 6 . The reaction apparatus according to claim 1 , wherein each of the first or second fluid control region includes a forced discharge mechanism configured to forcibly discharge a fluid from the reaction furnace. 7 . The reaction apparatus according to claim 1 , further comprising an airflow stirring part including a blowing hole for generating an airflow inside the reaction furnace in the intermediate part. 8 . The reaction apparatus according to claim 7 , wherein the airflow stirring part has a labyrinth structure in which the blowing hole includes a bent part. 9 . The reaction apparatus according to claim 1 , wherein the reaction furnace comprises a plurality of the supply ports receiving a plurality of different raw materials, respectively, at the one end of the reaction furnace. 10 . A reaction system comprising a first reaction apparatus and a second reaction apparatus, the first reaction apparatus and the second reaction apparatus being the reaction apparatus according to claim 1 coupled in series. 11 . A reaction system comprising: at least one of a kneader configured to manufacture a kneaded product by kneading a plurality of powders with different compositions, a granulator configured to manufacture a granulated product by granulating the kneaded product, and a dryer configured to manufacture the raw material by drying the granulated product; and the reaction apparatus according to claim 1 configured to receive any one of the kneaded product, the granulated product, and the raw material and manufacture a reaction product. 12 . A battery material manufacturing system comprising: a kneaded product manufacturing apparatus configured to knead a solid electrolyte manufactured as the reaction product by the reaction apparatus according to claim 1 and a binder resin and continuously extrude a mixture of the solid electrolyte and the binder resin to thereby manufacture a kneaded product; and a sheet manufacturing apparatus configured to form the kneaded product into a sheet. 13 . The battery material manufacturing system according to claim 12 , further comprising, as the reaction apparatus: a first reaction apparatus; and a second reaction apparatus configured to receive a first reaction product manufactured by the first reaction apparatus and manufacture the solid electrolyte as a second reaction product, wherein the kneaded product manufacturing apparatus receives the second reaction product and manufactures the kneaded product. 14 . A battery manufacturing system comprising: the battery material manufacturing system according to claim 12 ; and a laminator configured to laminate a positive electrode sheet containing a positive electrode sheet containing a positive electrode active material on one surface of an electrolyte sheet formed by the sheet manufacturing apparatus included in the battery material manufacturing system and a negative electrode sheet containing a negative electrode active material on another surface of the electrolyte sheet. 15 . A material manufacturing system comprising: a kneaded product manufacturing apparatus configured to knead the reaction product manufactured by the reaction apparatus according to claim 1 and a binder resin and continuously extrude a mixture of the solid electrolyte and the binder resin to thereby manufacture a kneaded product; and a sheet manufacturing apparatus configured to form the kneaded product into a sheet. 16 . The material manufacturing system according to claim 15 , further comprising, as the reaction apparatus: a first reaction apparatus; and a second reaction apparatus configured to receive a first reaction product manufactured by the first reaction apparatus and manufacture a second reaction product, wherein the kneaded product manufacturing apparatus receives the second reaction product and manufactures the kneaded product. 17 . A reaction product manufacturing method comprising: receiving a predetermined material to a cylindrical reaction furnace including a supply port configured to receive a raw material to be supplied at one end and a discharge port configured to discharge a reaction product at another end from the supply port; conveying the raw material toward the discharge port by a screw extending from the one end of the reaction furnace to the other end thereof; controlling a temperature of the reaction furnace at a predetermined position in an intermediate part between the supply port and the discharge port; allowing a first fluid to pass through the reaction furnace in a first fluid control region provided in the intermediate part; allowing a second fluid to pass through the reaction furnace in a second fluid control region, the second fluid control region being different from the first fluid control region in the intermediate part; and discharging the reaction product passed through the second fluid control region from the discharge port. 18 . A battery material manufacturing method comprising: receiving a predetermined material to a cylindrical reaction furnace including a supply port configured to receive a raw material to be supplied at one end and a discharge port configured to discharge a reaction product at another end from the supply port; conveying the raw material toward the discharge port by a screw extending from the one end of the reaction furnace to the other end thereof; controlling a temperature of the reaction furnace at a predetermined position in an intermediate part between the supply port and the discharge port; allowing a first fluid to pass through the reaction furnace in a first fluid control region provided in the intermediate part; allowing a second fluid to
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