Alternating current (ac) transition-metal catalysis
US-2023407492-A1 · Dec 21, 2023 · US
US2024167176A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2024167176-A1 |
| Application number | US-202318489882-A |
| Country | US |
| Kind code | A1 |
| Filing date | Oct 19, 2023 |
| Priority date | Nov 21, 2022 |
| Publication date | May 23, 2024 |
| Grant date | — |
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The present invention provides a stirring-free scalable electrochemical reactor enabled by alternating current and uses thereof in a method of performing electrosynthesis of organic reaction.
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What is claimed is: 1 . An electrochemical reactor comprising at least one apparatus comprising: at least one reactor body; at least one 3D porous electrode and at least one AC source; wherein said electrochemical reactor does not include a stirring element. 2 . An electrochemical reactor according to claim 1 , wherein said at least one 3D porous electrode is an RVC electrode. 3 . An electrochemical reactor according to claim 1 , wherein said at least one 3D porous electrode has a porosity of at least 5 ppi. 4 . An electrochemical reactor according to claim 1 , wherein said at least one 3D porous electrode has a porosity of at least 10 ppi. 5 . An electrochemical reactor according to claim 1 , wherein said at least one 3D porous electrode has a porosity of between about 5 to 30 ppi. 6 . An electrochemical reactor according to claim 1 , wherein said reactor is a batch reactor. 7 . An electrochemical reactor according to claim 1 , wherein said reactor is a flow reactor. 8 . An electrochemical reactor according to claim 1 , comprising at least two 3D porous electrodes. 9 . An electrochemical reactor according to claim 1 , comprising at least two 3D porous electrodes; wherein each of said 3D porous electrodes is separated in said reactor by at least one glass separator. 10 . An electrochemical reactor according to claim 1 , being scaled to industrial organic electrosynthesis reactions. 11 . A method of performing organic electrosynthesis, said method comprising providing an electrochemical reactor comprising at least one apparatus comprising: at least one reactor body; at least one 3D porous electrode and at least one AC source; wherein said electrochemical reactor does not include a stirring element; filling said reactor with electrosynthesis reactants; and applying AC through said filled electrochemical reactor; thereby performing said organic electrosynthesis. 12 . A method according to claim 11 , wherein said electrosynthesis is selected from redox-neutral reaction, amination reaction, esterification reaction, etherification reaction and any combinations thereof. 13 . A method according to claim 11 , wherein said at least one 3D porous electrode is an RVC electrode. 14 . A method according to claim 11 , wherein said at least one 3D porous electrode has a porosity of at least 5 ppi. 15 . A method according to claim 11 , wherein said at least one 3D porous electrode has a porosity of at least 10 ppi. 16 . A method according to claim 11 , wherein said at least one 3D porous electrode has a porosity of between about 5 to 30 ppi. 17 . A method according to claim 11 , wherein said reactor is a batch reactor or a flow reactor. 18 . A method according to claim 11 , comprising at least two 3D porous electrodes. 19 . A method according to claim 11 , comprising at least two 3D porous electrodes; wherein each of said 3D porous electrodes is separated in said reactor by at least one glass separator. 20 . A method according to claim 11 , being scaled to industrial organic electrosynthesis reactions.
Carbon, e.g. diamond or graphene · CPC title
based on inorganic materials · CPC title
with diaphragms · CPC title
Porous electrodes · CPC title
Reduction · CPC title
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