Catalyst for hydrogenation reaction and method for producing same
US-12485407-B2 · Dec 2, 2025 · US
US2024043621A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2024043621-A1 |
| Application number | US-202118027383-A |
| Country | US |
| Kind code | A1 |
| Filing date | Aug 26, 2021 |
| Priority date | Sep 29, 2020 |
| Publication date | Feb 8, 2024 |
| Grant date | — |
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A method for producing a crosslinked polyarylene sulfide resin (PAS resin) that reduces a difference in melt viscosity among lots and has excellent quality stability is provided. Further specifically, the method includes steps of compression-molding an uncrosslinked PAS resin in a powder form to obtain a compression-molded material, measuring a true specific gravity of the compression-molded material, grinding the compression-molded product having a specific range of true specific gravity to obtain a pulverized material, granulating the pulverized material to obtain a granulated material, and oxidatively crosslinking the granulated material obtained in the above step. Also provided are a method for producing a composition containing the crosslinked PAS, and a method for producing a molded article by melt-molding the composition.
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1 . A method for producing a crosslinked polyarylene sulfide, the method comprising steps of: compression-molding an uncrosslinked polyarylene sulfide in a powder form to obtain a compression-molded material; measuring a true specific gravity of the compression-molded material; grinding the compression-molded product having a specific range of true specific gravity to obtain a pulverized material; granulating the pulverized material to obtain a granulated material; and oxidatively crosslinking the granulated material obtained in the above step. 2 . The method for producing a crosslinked polyarylene sulfide according to claim 1 , wherein a shape of the granulated material is amorphous. 3 . The method for producing a crosslinked polyarylene sulfide according to claim 1 or 2 , wherein the specific range of true specific gravity is within a range of 1.10 to 1.30. 4 . A method for producing a resin composition, the method comprising steps of: producing a crosslinked polyarylene sulfide produced by the method according to any one of claims 1 to 3 ; and melt-kneading the obtained crosslinked polyarylene sulfide with another component. 5 . A method for producing a molded article, the method comprising steps of: producing a resin composition by the method according to claim 4 ; and melt-molding the obtained resin composition.
Modification with inorganic compounds · CPC title
Powdering or granulating · CPC title
Heating methods · CPC title
Polythioethers; Polythioether-ethers · CPC title
Crosslinking, e.g. vulcanising, of macromolecules (mechanical aspects B29C35/00; crosslinking agents C08K) · CPC title
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