Process for processing hard metal

Patent metadata

Field	Value
Publication number	US-2023392231-A1
Application number	US-202118032831-A
Country	US
Kind code	A1
Filing date	Oct 8, 2021
Priority date	Nov 4, 2020
Publication date	Dec 7, 2023
Grant date	—

Abstract

The invention relates to a process for processing hard metal, in particular hard metal scrap, wherein the hard metal is alloyed with a low-melting alloy metal in a reaction space of a reactor ( 10 ) with a heat supply, wherein the alloy metal is converted into a vapor phase in the presence of inert gas, and wherein the alloy metal is subsequently at least partially condensed in a condensation step, and wherein an overpressure relative to ambient pressure is present in the reaction space at least during the condensation phase. According to the invention, provision is made in particular for the inert gas to be permanently supplied to the reaction chamber at least temporarily during the condensation phase from an inert gas source ( 60 ) disposed outside of the reaction chamber via an inert gas supply line ( 61 ), and for the inert gas to be discharged from of the condenser ( 30 ) into the environment at least at certain intervals during the condensation phase. In this way, the equipment required can be significantly reduced compared to prior art hard metal chemical extraction processes.

First claim

1 - 14 . (canceled)

15 . A method for processing metal carbide, comprising:
alloying the metal carbide with a low-melting point alloy metal in a reaction space of a reactor under a supply of heat; providing an inert gas to the reaction space with an inert gas supply line from an inert gas source disposed outside of the reaction space; converting the alloy metal into a vapor phase in the presence of the inert gas in the reaction space; conducting a vapor mixture including the inert gas and the vapor phase of the alloy metal from the reaction space to a condenser with a vapor conduit; condensing at least partially the vapor phase of the alloy metal in the condenser; discharging the inert gas from the condenser at least at intervals during the condensing step; and maintaining an overpressure in the reaction space relative to an ambient pressure of an environment exterior of the reactor at least during the condensing step.

16 . The method of claim 15 , wherein:
the overpressure relative to ambient pressure is in a range of from 1 mbar to 90 mbar.

17 . The method of claim 15 , further comprising:
prior to the alloying step, flushing air from the reaction space by introducing inert gas from the inert gas source into the reaction space so that the inert gas displaces the air present in the reaction space; venting the air into the environment through a closable opening; and then closing the closable opening.

18 . The method of claim 15 , further comprising:
heating a heating conduit section of the vapor conduit.

19 . The method of claim 15 , wherein:
the step of discharging the inert gas from the condenser includes discharging the inert gas into the environment and expanding the inert gas to the ambient pressure of the environment.

20 . The method of claim 15 , wherein:
the step of discharging the inert gas from the condenser includes compressing the inert gas and recirculating the inert gas to the reaction space.

21 . The method of claim 15 , wherein:
the step of discharging the inert gas from the condenser includes discharging the inert gas into a separator and separating remaining residual alloy metal from the inert gas in the separator.

22 . The method of claim 15 , wherein:
in the alloying step one or more receptacles are disposed in the reaction space, each receptacle including a receiving space for receiving the metal carbide, the one or more receptacles each including at least one flow channel forming a spatial connection between the receiving space and a gas-conveying area of the reactor located outside the receiving space such that the inert gas is supplied by the at least one flow channel to the receiving space and the inert gas is discharged from the receiving space together with the vapor phase of the alloy metal.

23 . The method of claim 22 , wherein:
each of the one or more receptacles includes a bottom and a perimetral wall rising from the bottom, the wall including a rim facing away from the bottom, the rim having a plurality of cut-outs formed therein to provide the at least one flow channel.

24 . The method of claim 23 , wherein:
each of the cut-outs has a cross-section area in a range of from 1 square mm to 30 square mm.

25 . The method of claim 22 , wherein:
the one or more receptacles includes a plurality of receptacles and each of the receptacles includes a discharge channel communicated with the receiving space, and a plurality of the receptacles are superposed such that the discharge channels of the receptacles are aligned with each other, and a line section of the vapor conduit is routed through the aligned discharge channels such that an annular channel is left between an outer wall of the line section and the aligned discharge channels for discharging the inert gas and the vapor phase of the alloy metal from the receiving spaces of the receptacles.

26 . The method of claim 15 , wherein:
the inert gas supply line includes an opening which opens into an upper area of the reaction space, and the vapor conduit includes a conduit inlet disposed in the reaction space at a geodetic height below the opening of the inert gas supply line.

27 . The method of claim 26 , wherein:
the condenser includes a cup-shaped collection vessel, and the vapor conduit opens into the cup-shaped collection vessel.

28 . The method of claim 15 , wherein:
the discharging step includes discharging the inert gas from the condenser with a pressure valve communicated with a gas-conveying area of the condenser when a pressure threshold value in the gas-conveying area exceeds a pressure threshold value.

29 . The method of claim 28 , wherein:
the step of discharging the inert gas from the condenser includes discharging the inert gas into a separator and separating remaining residual alloy metal from the inert gas in the separator, and the pressure valve is disposed downstream of the separator.

Assignees

• Betek Gmbh & Co Kg

Inventors

• Philipp Matthias
• Haller Alexander
• Hilgert Tobias
• Much Manuel
• Huber David

Classifications

• C22B9/05 Primary

  Refining by treating with gases, e.g. gas flushing {also refining by means of a material generating gas in situ} · CPC title

• C22B7/001

  Dry processes · CPC title

• F27B14/04

  adapted for treating the charge in vacuum or special atmosphere · CPC title

• F27D7/02

  Supplying steam, vapour, gases or liquids · CPC title

• F27D2007/023

  Conduits · CPC title