Multi-component flux

Patent metadata

Field	Value
Publication number	US-2023278146-A1
Application number	US-202118019076-A
Country	US
Kind code	A1
Filing date	Aug 3, 2021
Priority date	Aug 5, 2020
Publication date	Sep 7, 2023
Grant date	—

Abstract

A solid metal flux comprised of compacted granules including (a) alkali chloride salt, (b) alkaline earth chloride salt and (c) at least one nitrate, carbonate, or sulfate salt and/or a fluoride containing salt.

First claim

1 - 18 . (canceled)

19 . A method of making a solid metal flux comprising providing materials in powder form, said materials including (a) at least one nitrate, carbonate, or sulfate salt and (b) the fines of a binary salt material including alkali chloride salt and alkaline-earth chloride salt and optionally (c) a fluoride containing salt, mixing the combined materials, melting the combined materials, solidifying the melted combined materials to obtain a fused compound, and crushing and sieving the fused compound.

20 . The method of making the salt of claim 1 wherein (c) is included in the fused compound.

21 . The method of claim 1 wherein the fused compound after sieving comprises granules having a grain size between about 1 and 3 mm.

22 . The method of claim 3 wherein the alkali chloride salt comprises the largest percentage of a granule by weight.

23 . The method of claim 3 wherein the alkaline-earth chloride salt comprises the largest percentage of a granule by weight.

24 . The method of claim 1 wherein the fused compound has a melting temperature of less than 720° C.

25 . The method of claim 3 wherein the granules are comprised of between 25 and 75 wt. % alkali chloride salt, between 5 and 60 wt. % alkaline-earth chloride salt, between 5 and 25 wt % fluoride containing salt, and between 5 and 25 wt. % nitrate, carbonate, or sulfate salt.

26 . The method of claim 3 wherein the granules are comprised of between 30 and 75 wt. % alkali chloride salt, between 20 and 60 wt. % alkaline-earth chloride salt, between 5 and 25 wt. % fluoride containing salt, and between 8 and 18 wt. % nitrate, carbonate, or sulfate salt.

27 . A method for the treatment of a metal bath comprising forming a fused binary salt of at least alkali chloride salt and alkaline earth chloride salt and obtaining the fines thereof, combining the fines with at least one nitrate, carbonate, sulfate salt, or fluoride containing salt to form a mixture, and supplying the mixture to the metal bath.

28 . The method of claim 9 wherein the mixture is comprised of between 25 and 75 wt. % alkali chloride salt, between 5 and 60 wt. % alkaline-earth chloride salt, between 5 and 25 wt. % fluoride containing salt, and between 5 and 25 wt. % of a nitrate, carbonate, or sulfate salt.

29 . The method of claim 9 wherein the mixture is comprised of between 30 and 75 wt. % alkali chloride salt, between 20 and 60 wt. % alkaline-earth chloride salt, between 5 and 25 wt. % fluoride containing salt, and between 8 and 18 wt. % of a nitrate, carbonate, or sulfate salt.

30 . The method of claim 9 wherein the alkali chloride salt comprises the largest percentage of the mixture by weight.

31 . The method of claim 9 wherein the alkaline-earth chloride salt comprises the largest percentage of the mixture by weight.

32 . The method of claim 9 wherein the mixture has a melting temperature of between 420 and 800° C.

33 . The method of claim 9 wherein the mixture is fused, crushed and sieved to form granules.

34 . A solid metal flux comprised of compacted granules having a grain size of between about 1 and 3 mm, said granules having a melting temperature in a range of between 400 and 600° C., said granules comprised of between 30 and 75 wt. % alkali chloride salt, between 20 and 60 wt. % alkaline-earth chloride salt, between 5 and 25 wt. % fluoride containing salt, and between 8 and 18 wt. % of a nitrate, carbonate, or sulfate salt.

35 . The solid metal flux of claim 16 wherein the granules have a density between about 1.5 and 2.0 g/cm 3 .

Assignees

• Pyrotek Inc

Inventors

• Mastor Michael
• Slavicek Viktor
• Zuo Xin
• Hargude Vijay

Classifications

• C22B19/32

  Refining zinc · CPC title

• C22B26/12

  Obtaining lithium · CPC title

• C22B26/22

  Obtaining magnesium · CPC title

• C22B9/10

  with refining or fluxing agents; Use of materials therefor, {e.g. slagging or scorifying agents}(C22B9/18 takes precedence){(C22B9/006 takes precedence)} · CPC title

• C22B21/062 Primary

  using salt or fluxing agents (C22B21/064, C22B21/066, and C22B21/068 take precedence) · CPC title