Palladium catalyst for oxidation of methane and method of preparation and use thereof
US-2018369787-A1 · Dec 27, 2018 · US
US2022194792A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2022194792-A1 |
| Application number | US-202017604247-A |
| Country | US |
| Kind code | A1 |
| Filing date | Apr 15, 2020 |
| Priority date | Apr 16, 2019 |
| Publication date | Jun 23, 2022 |
| Grant date | — |
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An ozone generation method comprising: Supplying a crude feed gas comprising oxygen and methane Performing a catalytic oxidation of methane from the crude feed gas to obtain a treated feed gas Generating ozone from the treated feed gas.
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1 . An ozone generation method comprising: Supplying a crude feed gas comprising oxygen and methane Performing a catalytic oxidation of methane from the crude feed gas to obtain a treated feed gas Generating ozone from the treated feed gas. 2 . The ozone generation method according to claim 1 , comprising the additional step of heating the crude feed gas to a temperature of at least 150° C. and at most 700° C. before and/or during performing the catalytic oxidation of methane from the crude feed gas to obtain a treated feed gas. 3 . The ozone generation method according to claim 2 , further comprising the additional steps of: Recovering at least a part of the heat from the treated feed gas Heating the crude feed gas with the recovered heat before and/or during the heating of the crude feed gas to a temperature of at least 150° C. and at most 700° C. 4 . The ozone generation method according to claim 1 , wherein the catalytic oxidation is performed with a catalyst chosen among palladium, platinum and platinum-palladium. 5 . The ozone generation method according to claim 1 , comprising the additional step of drying the treated feed gas to remove at least some water before generating ozone from the treated feed gas. 6 . The ozone generation method according to claim 1 , comprising the additional step of cooling the treated feed gas before generating ozone from the treated feed gas. 7 . The ozone generation method according to claim 1 , comprising the additional step of cooling the ozone generator with a cooling liquid. 8 . The ozone generation method according to claim 6 , wherein the step of cooling the treated feed gas is performed with at least part of the cooling liquid outputted from the ozone generator. 9 . An ozone generation device, comprising: A supply of a crude feed gas comprising oxygen and methane A catalytic unit adapted to perform a catalytic oxidation of methane from the crude feed gas to obtain a treated feed gas An ozone generator adapted to be fed by the treated feed gas. 10 . The ozone generation device according to claim 9 , further comprising a heating unit adapted to heat the crude feed gas and/or the catalytic unit to at least 150° C. and at most 700° C. 11 . The ozone generation device according to claim 10 , further comprising a heat exchanger adapted to recover at least part of the heat from the treated feed gas and to heat the crude feed gas and/or the catalytic unit with the recovered heat. 12 . The ozone generation device according to claim 9 , further comprising a drying unit adapted to remove at least some water from the treated feed gas. 13 . The ozone generation device according to claim 9 , further comprising a cooling unit adapted to cool the treated feed gas. 14 . The ozone generation device according to claim 9 , wherein the ozone generator is adapted to be cooled by a cooling liquid. 15 . The ozone generation device according to claim 9 , further comprising circulation means adapted to circulate toward the cooling unit at least part of the cooling liquid outputted from the ozone generator. 16 . The ozone generation device according to claim 9 , wherein the catalytic unit comprises a catalyst chosen among platinum-palladium and platinum-palladium.
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