Method for extracting a mineral from biotites

Patent metadata

Field	Value
Publication number	US-2021009433-A1
Application number	US-202016923203-A
Country	US
Kind code	A1
Filing date	Jul 8, 2020
Priority date	Jul 8, 2019
Publication date	Jan 14, 2021
Grant date	—

Abstract

A method for extracting a mineral contained in biotite. The method includes a step of freezing the biotite, followed by a step of thawing the biotite. A method for characterizing a paleoalteration, in which at least one mineral is studied that is contained in cleavages of biotite extracted from a felsic rock that is at least partially altered.

First claim

1 . A method for extracting a mineral contained in biotite, characterized in that the method comprises a step of freezing the biotite, followed by a step of thawing the biotite.

2 . The method for extracting a mineral according to claim 1 , wherein biotite is used in which the mineral is contained in cleavages of the biotite.

3 . The method for extracting a mineral according to claim 1 , wherein the mineral is chosen from the following minerals: potassium feldspar, quartz, plagioclase and prehnite.

4 . The method for extracting a mineral according to claim 1 , wherein the biotite is brought into contact with water prior to the freezing and thawing steps, and are kept in contact with water during the freezing step and at least part of the thawing step.

5 . The method for extracting a mineral according to claim 1 , wherein the thawing step takes place in a freeze dryer.

6 . The method for extracting a mineral according to claim 1 , wherein the freezing step is carried out at a temperature of up to −40° C.

7 . The method for extracting a mineral according to claim 1 , wherein the thawing of the biotite takes place at approximately 1 mbar.

8 . The method for extracting a mineral according to claim 7 , wherein at least part of the freezing step is carried out under a pressure of approximately 1 mbar.

9 . A method for extracting a mineral according to claim 4 , wherein the thawing step lasts from 36 to 76 hours during which the temperatures of the biotite and of the water are gradually raised to a temperature ranging from 18 to 25° C. under a pressure of approximately 1 mbar.

10 . The method for extracting a mineral according to claim 9 , wherein the gradual rise in temperature comprises the following stages, following one another in this order:
6 hours at −40° C., 10 hours at −30° C., 10 hours at −20° C., 10 hours at −10° C., 12 hours at +20° C.

11 . The method for extracting a mineral according to claim 10 , comprising a step subsequent to the thawing step, during which the temperatures of the biotite and the water are gradually raised to a temperature of approximately 30° C., under a pressure of approximately 0.001 mbar, said step lasting from 25 to 65 hours.

12 . The method for extracting a mineral according to claim 1 , wherein the thawing of the biotite is a lyophilization.

13 . The method for extracting a mineral according to claim 1 , further comprising a step of releasing the minerals contained in the biotite by subjecting the biotite to vibrations large enough to release the minerals.

14 . A method for characterizing a paleoalteration, characterized in that at least one mineral is studied that is contained in cleavages of biotite extracted from an at least partially altered felsic rock, in which method the mineral contained in cleavages of biotite is extracted using the extraction method according to claim 1 , and the characterization of the paleoalteration is carried out by studying the extracted mineral.

15 . The characterization method according to claim 14 , wherein the characterization consists of dating the mineral extracted by means of a 39 Ar- 40 Ar analysis.

16 . The method for extracting a mineral according to claim 9 , wherein the thawing step lasts from 41 to 66 hours.

17 . The method for extracting a mineral according to claim 9 , wherein the thawing step lasts from 46 to 50 hours.

18 . The method for extracting a mineral according to claim 9 , wherein the temperatures of the biotite and of the water are gradually raised to a temperature ranging from 19 to 23° C.

19 . The method for extracting a mineral according to claim 11 , wherein the step subsequent to the thawing step lasts from 35 to 55 hours.

20 . The method for extracting a mineral according to claim 13 , wherein the step of releasing the minerals contained in the biotite comprises releasing the minerals in the cleavages of the biotite.

Assignees

• Brgm
• Total Sa

Inventors

• Wyns Robert
• Baptiste Julien
• Duron Jéromine
• Roig Jean-Yves
• Montech Sébastien

Classifications

• C01B33/26 Primary

  Aluminium-containing silicates {, i.e. silico-aluminates} · CPC title

• C01B33/38

  Layered base-exchange silicates, e.g. clays, micas or alkali metal silicates of kenyaite or magadiite type {(activation of naturally occurring clays B01J20/12; pillared layered base-exchange silicates B01J29/049)} · CPC title

• B01D11/0288 Primary

  Applications, solvents · CPC title

• C01B33/42

  Micas {; Interstratified clay-mica products (delaminated mica or vermiculite platelets obtained by a process involving cation-exchange C04B14/208)} · CPC title