Improved process-intensified flow reactor

Patent metadata

Field	Value
Publication number	US-2020246772-A1
Application number	US-201816635069-A
Country	US
Kind code	A1
Filing date	Jul 31, 2018
Priority date	Jul 31, 2017
Publication date	Aug 6, 2020
Grant date	—

Abstract

A flow reactor has a module having a process fluid passage with an interior surface, a portion of the passage including a cross section along the portion having a cross-sectional shape, and a cross-sectional area with multiple minima along the passage. The cross-sectional shape varies continually along the portion and the interior surface of the portion includes either no pairs of opposing flat parallel sides or only pairs of opposing flat parallel sides which extend for a length of no more than 4 times a distance between said opposing flat parallel sides along the portion and the portion contains a plurality of obstacles distributed along the portion.

First claim

1 . A flow reactor comprising:
a module having a process fluid passage therein, the process fluid passage comprising an interior surface, the process fluid passage further comprising a portion thereof which portion further comprises:
(1) an input end at which process fluid is to flow into the portion during use and
(2) an output end at which process fluid is to flow out of the portion during use, and
(3) a cross section along the portion delimited by the interior surface of the passage along the portion, the cross section having a cross-sectional area and a cross-sectional shape, the cross-sectional area having multiple minima along the passage between the input end and the output end, the passage characterized in that (1) the cross-sectional shape of the portion varies continually along the portion, (2) the interior surface of the portion includes either no pairs of opposing flat parallel sides or only pairs of opposing flat parallel sides which extend for a length of no more than 4 times a distance between said opposing flat parallel sides along the portion, and (3) the portion contains a plurality of obstacles positioned along the portion between the input end and the output end.

2 . The flow reactor according to claim 1 wherein the portion further comprises successive chambers each with a nozzle-like entrance and a narrowing exit.

3 . The flow reactor according to claim 2 wherein one chamber of said successive chambers is nested with a next-succeeding chamber of said successive chambers such that the narrowing exit of the one chamber forms the nozzle-like entrance of the next adjacent succeeding chamber.

4 . The flow reactor according to claim 2 wherein at least one of the plurality of obstacles is located within a first chamber and intersects a straight line having a first endpoint located at a center of the entrance of the first chamber and a second endpoint locate at a center of the exit of the first chamber.

5 . The flow reactor according to claim 4 wherein the at least one of the plurality of obstacles intersects every straight line having a first end point within the entrance of the first chamber and a second endpoint within the exit of the first chamber.

6 . The flow reactor according to claim 4 having one or more bypass paths, positioned between the at least one obstacle and an inside surface of the first chamber, around the at least one obstacle of the plurality of obstacles.

7 . The flow reactor according to claim 6 wherein said one or more bypass paths have a total cross-sectional area greater than the total cross-sectional area of the exit of the first chamber.

8 . The flow reactor according to claim 6 wherein said at least one obstacle has one or more openings extending through said at least one obstacle.

9 . The flow reactor according to claim 6 wherein said at least one obstacle has no openings extending through said at least one obstacle.

10 . The flow reactor according to claim 4 wherein the plurality of obstacles comprises at least three or more obstacles.

11 . The flow reactor according to claim 4 wherein the at least one obstacle of the plurality of obstacles comprises at least one obstacle per chamber.

12 . The flow reactor according to claim 4 further comprising two or more obstacles in a single chamber.

13 . The flow reactor according to claim 4 wherein said at least one obstacle has two or more bypass paths.

14 . The flow reactor according to claim 13 wherein said at least one obstacle has three or more bypass paths.

15 . The flow reactor according to claim 13 wherein said bypass paths are separated by the obstacle by a distance of at least twice a maximum diameter of the exit of the chamber.

16 . The flow reactor according to claim 4 wherein said at least one obstacle has a single bypass path.

17 . The flow reactor according to claim 4 wherein said at least one obstacle has a two bypass paths, said two bypass paths positioned on opposite sides of the process fluid passage relative to one another.

18 . The flow reactor of claim 1 wherein the at least one of the plurality of obstacles comprises a flat or concave surface aligned generally perpendicularly to the process fluid passage.

19 . The flow reactor of claim 18 wherein the flat or concave surface faces in a downstream direction.

20 . The flow reactor of claim 18 wherein the flat or concave surface faces in an upstream direction.

21 . The flow reactor of claim 1 wherein the at least one of the plurality of obstacles comprises a tapering elongated end pointing in a downstream direction.

22 . The flow reactor of claim 1 wherein the at least one obstacle of the plurality of obstacles comprises a tapering elongated end pointing in an upstream direction.

23 . The flow reactor of claim 1 further comprising an internal screw thread structure on an inner surface of the process fluid passage.

24 . The flow reactor of claim 1 further comprising an internal screw thread structure on an inner surface of the portion of the process fluid passage.

25 . A flow reactor comprising:
a body having a process fluid passage contained therein, the process fluid passage having a portion thereof, said portion comprising a fluid input end and a fluid output end and successive cross-sectional-area minima between the input end and the output end, the portion further having a cross-sectional shape defined, at any position along the portion, as a cross section of the process fluid passage, at that position of the portion, angularly oriented such that, for a fluid flowing from the input to the output end of the portion, a net fluid flow through said cross section is maximized; the portion further having a passage shape defined at any position along the portion as a planar cross section of the process fluid passage passage taken at that position in a plane perpendicular to the predominant flow direction at that position; the passage shape having both a width and a height, perpendicular to the width, each varying continually with position along the flow passage; the flow passage comprising successive chambers each with a narrow entrance and a narrowing exit which protrudes into the next adjacent chamber (if any) forming the narrow entrance thereof, and an internal screw thread structure on an inner surface of the portion of the process fluid passage.

Assignees

• Corning Inc

Inventors

• Jean Patrick
• Lavric Elena Daniela

Classifications

• B01J19/0093 Primary

  Microreactors, e.g. miniaturised or microfabricated reactors (laboratory containers with capillary fluid transport in microfabricated channels or chambers B01L3/5027) · CPC title

• B01F25/4231

  using baffles · CPC title

• B01F25/25

  Mixing by jets impinging against collision plates · CPC title

• B01F33/30

  Micromixers · CPC title

• B01F2101/2204

  Mixing chemical components in generals in order to improve chemical treatment or reactions, independently from the specific application · CPC title