Discrete extract collection system for co2-based fluid extraction

Patent metadata

Field	Value
Publication number	US-2019282923-A1
Application number	US-201916353194-A
Country	US
Kind code	A1
Filing date	Mar 14, 2019
Priority date	Mar 15, 2018
Publication date	Sep 19, 2019
Grant date	—

Abstract

The present disclosure relates to methodologies, systems, and devices for discretely collecting extracts from an extract collection container of a CO 2 -based extraction system. A removable liner can be placed within the extract collection container such that the extract is collected within the removable liner, which can be removed or collected at discrete times. The removable liner can be hung from an extract fluid inlet tube or attached to an internal sidewall of the extract collection container.

First claim

What is claimed is:

1 . A method of extracting solid materials from liquid, gas or liquid-gas solutions, the method comprising:
securing a first removable liner within an extract collection container of a CO 2 -based extraction system having a fluid stream inlet and a fluid stream outlet; closing a cap of the extract collection container; collecting a first solid material in the first removable liner by passing a first solution through the fluid stream inlet of the extract collection container; depressurizing the extract collection container and removing the removable liner from the extract collection container; and replacing and securing a second removable liner within the extract collection container.

2 . The method of claim 1 , further comprising: collecting a second solid material in the second removable liner by passing a second solution through the fluid stream inlet of the extract collection container.

3 . The method of claim 2 , wherein carryover of the first solid material into the second solid material is less than 10%.

4 . The method of claim 2 , wherein carryover of the first solid material into the second solid material is at least 10% less compared to carryover of the first solid material into the second solid material from a hydrocyclone separator without removable liners.

5 . The method of claim 1 , wherein passing the first solution through the fluid stream inlet generates an internal spiraling fluid flow to cause at least a partial material separation process.

6 . The method of claim 1 , wherein securing the first removable liner within the extract collection container includes securing the removable liner to a cylindrical section detachably connected to an open end of the extract collection container.

7 . The method of claim 6 , wherein securing the removable liner to the cylindrical section includes securing the removable liner to inlet tubing that circumferentially lines an internal surface of the cylindrical section.

8 . The method of claim 1 , wherein securing the first removable liner within the extract collection container includes positioning an inserted ring on a portion of an open end of the removable liner or using magnetic force to secure the open end of the removable liner to a portion of the extract collection container.

9 . A CO 2 -based extraction system comprising:
an extraction vessel of the CO2-based extraction system configured to generate an extract fluid flow including a mixture of an extract and CO 2 , an extract collection container having a fluid stream inlet and a fluid stream outlet, the fluid stream inlet configured to direct the extract fluid flow into the extract collection container and generate an internal spiraling fluid flow to cause at least a partial material separation process of the extract from the CO 2 ; and a removable liner disposed within the extract collection container and covering at least a portion of an inner surface of the extract collection container, wherein the removable liner is configured to collect the extract and is sized to fit within the extract collection container.

10 . The CO 2 -based extraction system of claim 9 , wherein the fluid stream inlet is a tangential inlet.

11 . The CO 2 -based extraction system of claim 9 , wherein the removable liner symmetrically covers the between 10% and 100% of the inner surface of the extract collection container.

12 . The CO 2 -based extraction system of claim 9 , further comprising a cylindrical section detachably connected to an open end of the extract collection container, and wherein the removable liner is connected to the cylindrical section.

13 . The CO 2 -based extraction system of claim 12 , wherein the fluid stream inlet includes inlet tubing that circumferentially lines an internal surface of the cylindrical section, and the removable liner is connected to the inlet tubing.

14 . The CO 2 -based extraction system of claim 9 , further comprising an inserted ring configured to cover a portion of an open end of the removable liner.

15 . The CO 2 -based extraction system of claim 9 , wherein the extract collection container is a cone-shaped vessel.

16 . A hydrocyclone separator, comprising:
a truncated cone-shaped vessel including a fluid stream inlet and a fluid stream outlet configured to generate an internal spiraling fluid flow in operation to cause at least a partial material separation process, and a truncated end; a cone-shaped collector including an open end detachably connected to the truncated end of the truncated cone-shaped vessel; and a removable liner disposed within the cone-shaped collector and covering at least a portion of an inner surface of the cone-shaped collector, wherein the liner is configured to collect solid material.

17 . The hydrocyclone separator of claim 16 , wherein the fluid stream inlet is a tangential inlet.

18 . The hydrocyclone separator of claim 16 , wherein the cone-shaped collector defines between 10% and 50% of a conical inner surface of the hydrocyclone separator.

19 . The hydrocyclone separator of claim 16 , wherein the truncated cone-shaped vessel includes a first flange at or near the truncated end, the cone-shaped collector includes a second flange at or near the open end, and a portion of the removable liner is secured between the first flange and the second flange.

20 . The hydrocyclone separator of claim 16 , wherein a conical angle of the truncated cone-shaped vessel and a conical angle of the cone-shaped collector are substantially the same.

Assignees

• Waters Technologies Corp

Inventors

• Ognibene Edward J
• Webster Michael
• Sulik Andrew
• Stricko Steven
• Aubin Andrew
• Hudalla Christopher J

Classifications

• B01D11/028

  Flow sheets · CPC title

• B01D11/0292

  Treatment of the solvent · CPC title

• B01D21/267

  by using a cyclone · CPC title

• B01D11/0207

  Control systems · CPC title

• B01D11/0203 Primary

  with a supercritical fluid · CPC title