Organotemplate-Free Solid-State Synthetic Method For Zeolite Molecular Sieves
US-2015298983-A1 · Oct 22, 2015 · US
US2019062170A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2019062170-A1 |
| Application number | US-201616073640-A |
| Country | US |
| Kind code | A1 |
| Filing date | May 18, 2016 |
| Priority date | Jan 28, 2016 |
| Publication date | Feb 28, 2019 |
| Grant date | — |
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The invention discloses a sound-absorbing material particle and a preparation method thereof. The method for preparing the sound-absorbing material particle comprises: mixing a sound-absorbing raw material with a solvent to form a sound-absorbing slurry; filling the sound-absorbing slurry into a mechanical compression die, and performing compression molding on the sound-absorbing slurry to form a particle; performing a hydrothermal crystallization reaction on the particle to crystallize the sound-absorbing raw material in the particle; and drying the particle to produce the sound-absorbing material particle.
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1 . A method for preparing a sound-absorbing material particle, comprising: mixing a sound-absorbing raw material with a solvent to make a sound-absorbing slurry; filling the sound-absorbing slurry into a mechanical compression die, and performing compression molding on the sound-absorbing slurry to form a particle; performing a hydrothermal crystallization reaction on the particle to crystallize the sound-absorbing raw material in the particle; and drying the particle to produce the sound-absorbing material particle. 2 . The method according to claim 1 , wherein the mass ratio of the sound-absorbing raw material in the sound-absorbing slurry ranges from 35% to 75%. 3 . The method according to claim 1 , wherein the particle has a diameter in the range of 0.05-1.0 mm. 4 . The method according to claim 1 , wherein the hydrothermal crystallization reaction is performed in a hydrothermal device, wherein the hydrothermal device has a reactant, and the reactant comprises a template agent. 5 . The method according to claim 1 , wherein the purity of the template agent is greater than 95%, and the mass ratio of the template agent in the reactant ranges from 1% to 35%. 6 . The method according to claim 1 , wherein the drying process is performed at a temperature in the range of 40° C. to 150° C., and the atmosphere for the drying process includes nitrogen gas. 7 . The method according to claim 1 , wherein the sound-absorbing material particle or the particle is subjected to a roasting process, wherein the roasting process is performed at a temperature in the range of 120° C. to 850° C., the heating rate of the roasting ranges from 20° C./h to 120° C./h, and the time range for the roasting is 0.5-96 h. 8 . The method according to claim 1 , wherein the content of oxygen in the atmosphere of the furnace gas for a roasting process is 0.1%-21%. 9 . A sound-absorbing material particle, wherein the sound-absorbing material particle has a particle size in the range of 0.05-1.0 mm, a specific surface area in the range of 250-850 m 2 /g, a pore volume in the range of 0.2-2.0 ml/g, and a bulk density in the range of 0.25-0.95 g/ml. 10 . The sound-absorbing material particle according to claim 9 , wherein the volume of micropore pores having a pore size of 0.5 μm to 45 μm in the sound-absorbing material particle accounts for 10% to 85% of the total pore volume of the sound-absorbing material particle.
Selection of materials · CPC title
Surface area · CPC title
Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof · CPC title
Powder tap density · CPC title
by pressing in moulds or between rollers · CPC title
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