Process for removing catalyst fines from a liquid stream from a fixed bed reactor
US-2015360151-A1 · Dec 17, 2015 · US
US2018071703A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2018071703-A1 |
| Application number | US-201615563116-A |
| Country | US |
| Kind code | A1 |
| Filing date | Feb 16, 2016 |
| Priority date | Apr 1, 2015 |
| Publication date | Mar 15, 2018 |
| Grant date | — |
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A device for mixing and distributing fluids for a downward flow catalytic reactor, said device comprising: a collection zone comprising at least one collection means; at least one substantially vertical collection conduit adapted to receive a reaction fluid collected by said collection means and at least one injection means; a mixing zone; and a distribution zone comprising a distribution plate supporting a plurality of chimneys; characterised in that said mixing zone is disposed at the same level as the distribution zone, said mixing and distribution zones being delimited by at least one annular wall comprising at least one lateral passage section adapted for the passage of the fluids from said mixing zone to said distribution zone.
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1 . A device for mixing and distributing fluids for a downward flow catalytic reactor, said device comprising: at least one collection zone (A) comprising at least one collection means ( 5 ); at least one substantially vertical collection conduit ( 7 ) adapted to receive a reaction fluid collected by said collection means ( 5 ) and at least one injection means ( 8 ) opening into said collection conduit ( 7 ) to inject a quench fluid; at least one mixing zone (B) disposed downstream of the collection means ( 5 ) in the direction of flow of the fluids, said mixing zone (B) comprising at least one mixing chamber ( 9 ) connected to said collection conduit ( 7 ) and an outlet end ( 10 ) for discharge of the fluids; and at least one distribution zone (C) disposed downstream of said mixing zone (B) in the direction of flow of the fluids comprising a distribution plate ( 12 ) supporting a plurality of chimneys; characterised in that said mixing zone (B) is disposed at the same level as the distribution one (C), said mixing zone (B) and said distribution zone (C) being delimited by at least one annular wall ( 16 ) comprising at least one lateral passage section ( 17 a , 17 b ) adapted for the passage of the fluids from said mixing zone (B) to said distribution zone (C). 2 . A device according to claim 1 characterised in that said mixing zone (B) is included in an annular enclosure ( 15 ) comprising said annular wall ( 16 ). 3 . A device according to claim 2 characterised in that said annular wall ( 16 ) internally delimits said distribution zone (C). 4 . A device according to claim 1 characterised in that said annular wall ( 16 ) is positioned at a spacing d 2 from the enclosure of the reactor, the spacing d 2 varying from 2% to 20% of the diameter of the reactor. 5 . A device according to claim 1 characterised in that said mixing chamber ( 9 ) is positioned at a spacing d 1 from the enclosure of the reactor, the spacing d 1 being between 5 and 30 mm. 6 . A device according to claim 2 characterised in that the height of said annular enclosure ( 15 ) is between 200 and 800 mm. 7 . A device according to claim 1 characterised in that the annular wall ( 16 ) comprises a plurality of lateral passage sections ( 17 a , 17 b ) distributed on at least two levels. 8 . A device according to claim 1 characterised in that said annular wall ( 16 ) is substantially cylindrical. 9 . A device according to claim 1 characterised in that the section of said mixing chamber ( 9 ) is of a parallelogram configuration and has a ratio between the height “h” of the section and the width “l” of said section of between 0.2 and 5.0. 10 . A device according to claim 1 characterised in that said mixing zone (B) comprises two mixing chambers ( 9 ) which are in diametrally opposite relationship in said mixing zone (B). 11 . A device according to claim 1 characterised in that the chimneys ( 13 ) which are disposed at the periphery of said distribution zone (C) are prolonged below the distribution plate ( 12 ) and are angled, the angling angle α between the longitudinal axis of prolongation of the chimneys ( 13 ) below said distribution chamber ( 12 ) and the plane perpendicular to the longitudinal axis of the enclosure being between 0 and 90 degrees. 12 . A device according to claim 1 characterised in that it further comprises a dispersive system disposed below said distribution plate ( 12 ), said dispersive system comprising at least one dispersion device ( 19 ). 13 . A device according to claim 12 characterised in that said dispersion device ( 19 ) is a grid comprising at least one guide system ( 21 ) adapted to collect and transport at least a part of the flow of liquid issuing from said distribution zone (C). 14 . A device according to claim 1 characterised in that said mixing and distribution zones (B and C) are delimited by two annular walls ( 16 ) each comprising at least one lateral passage section ( 17 a , 17 b ) adapted for the passage of the fluids from said mixing zone (B) to said distribution zone (C). 15 . A downward flow catalytic reactor comprising an enclosure ( 1 ) enclosing at least two fixed catalyst beds ( 2 , 14 ) separated by an intermediate zone comprising a fluid mixing and distribution device according to claim 1 .
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