Metal organic framework-derived carbon aerogel, preparation method thereof and application in lithium ion batteries
US-12183924-B2 · Dec 31, 2024 · US
US2017288204A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2017288204-A1 |
| Application number | US-201715625584-A |
| Country | US |
| Kind code | A1 |
| Filing date | Jun 16, 2017 |
| Priority date | Dec 16, 2014 |
| Publication date | Oct 5, 2017 |
| Grant date | — |
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A method for making a battery slurry is disclosed. The method comprises providing a plurality of solid raw materials and at least one liquid raw material, the at least one liquid raw material is divided into a first part solvent and a second part solvent to be used; mixing the plurality of solid raw materials to obtain a dry powder; kneading the dry powder and the first part solvent to obtain a doughy mixture; and dispersing the doughy mixture to the second part solvent to obtain the battery slurry.
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What is claimed is: 1 . A method for making a battery slurry, comprising: providing a plurality of solid raw materials and at least one liquid raw material, the at least one liquid raw material comprising a first part solvent and a second part solvent; mixing the plurality of solid raw materials to obtain a dry powder; kneading the dry powder and the first part solvent to obtain a doughy mixture; and dispersing the doughy mixture to the second part solvent to obtain the battery slurry. 2 . The method of claim 1 , wherein the plurality of solid raw materials are mixed in a vacuum environment. 3 . The method of claim 2 , wherein the plurality of solid raw materials are mixed at a temperature range from about 30° C. to about 150° C. 4 . The method of claim 2 , wherein the plurality of solid raw materials are mixed for a period of about 30 minutes to about 120 minutes 5 . The method of claim 1 , wherein a mass ratio of the dry powder to the first part solvent is in a range from about 1:9 to about 1:1. 6 . The method of claim 1 , wherein the dry powder and the first part solvent are kneaded in a vacuum environment. 7 . The method of claim 6 , wherein a vacuum pressure of the vacuum environment is lower than −0.09 MPa. 8 . The method of claim 6 , wherein the dry powder and the first part solvent are kneaded at a temperature range from about 25° C. to about 45° C. 9 . The method of claim 6 , wherein the dry powder and the first part solvent are kneaded for a period of about 30 minutes to about 120 minutes. 10 . The method of claim 1 , wherein the doughy mixture is dispersed to the second part solvent by stirring at a speed greater than or equal to about 15 m/s. 11 . The method of claim 10 , wherein the speed is in a range from about 15 m/s to about 70 m/s. 12 . The method of claim 10 , wherein the doughy mixture and the second part solvent are dispersed for a period of about 5 minutes to about 30 minutes. 13 . The method of claim 1 , wherein the doughy mixture and the second part solvent are dispersed at a temperature range from about 25° C. to about 45° C. 14 . The method of claim 1 , wherein a component of the first part solvent is the same as a component of the second part solvent. 15 . The method of claim 1 , wherein the battery slurry is an electrode slurry of the lithium ion battery, the plurality of solid raw materials comprise an active material, a conducting agent, and a binder, and at least one liquid raw materials can be at least one of N-methyl-2-pyrrolidone (NMP), N,N-dimethyl formamide (DMF), N,N-diethyl formamide (DEF), dimethyl sulfoxide (DMSO), tetrahydrofuran (THF), acetone, ethanol, and deionized water.
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