Processes for preparing multiple capsules

Patent metadata

Field	Value
Publication number	US-2017281480-A1
Application number	US-201515504766-A
Country	US
Kind code	A1
Filing date	Aug 19, 2015
Priority date	Aug 19, 2014
Publication date	Oct 5, 2017
Grant date	—

Abstract

Methods of preparing a capsule delivery system having two or more different capsules. Also disclosed are capsule delivery systems and consumer products containing such a capsule delivery system.

First claim

1 - 36 . (canceled)

37 . A method of preparing a capsule delivery system having two different capsules, the method comprising:
(a) providing a first emulsion containing a first benefit agent and a first capsule wall-forming material; (b) providing a second emulsion containing a second benefit agent and a second capsule wall-forming material; (c) mixing the first emulsion and the second emulsion to obtain an emulsion mixture; (d) causing the formation of a first capsule and a second capsule to obtain a mixed capsule slurry, the first capsule containing the first benefit agent encapsulated by a first capsule wall formed of the first capsule wall-forming material, the second capsule containing the second benefit agent encapsulated by a second capsule wall formed of the second capsule wall-forming material, and the first capsule being different from the second capsule; and (e) curing the mixed capsule slurry to obtain the capsule delivery system,
wherein the first or second benefit agent, independently, is a fragrance, flavor, malodor counteracting agent, or combination thereof.

38 . The method of claim 37 , wherein each of the first and second capsule walls, independently, is formed of a polyacrylate, polyurea, polyurethane, polyacrylamide, poly(acrylate-co-acrylamide), starch, silica, gelatin and gum Arabic, poly(melamine-formaldehyde), poly(urea-formaldehyde), or combination thereof.

39 . The method of claim 38 , wherein the first or second capsule wall, independently, is formed of a polyurea, polyurethane, or combination thereof.

40 . The method of claim 39 , wherein the first or second capsule wall, independently, is a reaction product between a polyisocyanate and an amine cross-linker, an alcohol cross-linker, or a hybrid cross-linker, the polyisocyanate is an aromatic or aliphatic isocyanate having two or more isocyanate groups, the amine cross-linker has two or more amine groups, the alcohol cross-linker has two or more hydroxyl groups, and the hybrid cross-linker has one or more amine groups and one or more hydroxyl groups.

41 . The method of claim 37 , wherein the mixed capsule slurry is cured at 55° C. to 130° C.

42 . The method of claim 37 , further comprising the step of adding a catalyst to the first emulsion, the second emulsion, or the emulsion mixture.

43 . The method of claim 37 , further comprising the step of adding a malodor counteracting agent to the capsule delivery system.

44 . The method of claim 37 , further comprising the step of adding a third, fourth, fifth, or sixth emulsion to the emulsion mixture or mixed capsule slurry, and causing the formation of a third, fourth, fifth, or sixth capsule, in which each of these capsules has a size of 0.01 to 1000 microns and contains a benefit agent encapsulated by a capsule wall.

45 . A method of preparing a capsule delivery system containing two different capsules, the method comprising:
(a) providing a first capsule slurry including a first capsule, in which the first capsule contains a first benefit agent encapsulated by a first capsule wall that is formed of a first wall-forming material; (b) providing a second emulsion including a second benefit agent and a second wall-forming material; (c) mixing the first capsule slurry and the second emulsion to obtain a capsule mixture; (d) causing the formation of a second capsule to obtain a mixed capsule slurry, in which the second capsule contains the second benefit agent encapsulated by a second capsule wall, the second capsule wall is formed of the second wall-forming material, and the second capsule is different from the first capsule; and (e) curing the mixed capsule slurry to obtain the capsule delivery system,
wherein the first or second benefit agent, independently, is a fragrance, flavor, malodor counteracting agent, or combination thereof.

46 . The method of claim 45 , wherein each of the first and second capsule wall, independently, is formed of a polyacrylate, polyurea, polyurethane, polyacrylamide, poly(acrylate-co-acrylamide), silica, gelatin and gum Arabic, poly(melamine-formaldehyde), poly(urea-formaldehyde), or combination thereof.

47 . The method of claim 46 , wherein the first or second capsule wall, independently, is formed of a polyurea, polyurethane, or combination thereof, the polyurea is a reaction product between a polyisocyanate and an amine cross-linker, an alcohol cross-linker, or a hybrid cross-linker, the polyisocyanate is an aromatic or aliphatic isocyanate having two or more isocyanate groups, the amine cross-linker has two or more amine groups, the alcohol cross-linker has two or more hydroxyl groups, and the hybrid cross-linker has one or more amine groups and one or more hydroxyl groups.

48 . The method of claim 45 , further comprising, before step (c), the step of curing the first capsule slurry at 55° C. to 130° C.

49 . A method of preparing a capsule delivery system containing two different capsules, the method comprising:
(a) providing a first capsule emulsion including a first water phase, a first wall-forming material, and a first core material, in which the first core material has a first benefit agent and is dispersed in the first capsule emulsion as oil droplets having a size of 0.01 to 1000 microns; (b) adding a second core material and a second wall-forming material to the first capsule emulsion, in which the second core material has a second benefit agent; (c) emulsifying the second core material to obtain a second capsule emulsion, in which the second core material is dispersed in the second capsule emulsion as oil droplets having a size of 0.01 to 1000 microns; (d) causing the formation of a first and second capsules to obtain a mixed capsule slurry, in which the first capsule is different from the second capsule, the first capsule contains the first benefit agent encapsulated by a first capsule wall, the first capsule wall is formed of the first wall-forming material, the second capsule contains the second benefit agent encapsulated by a second capsule wall, the second capsule wall is formed of the second wall-forming material; and (e) curing the mixed capsule slurry to obtain the capsule delivery system,
wherein the first or second benefit agent is a fragrance, flavor, malodor counteracting agent, or combination thereof.

50 . The method of claim 49 , wherein each of the first and second capsule walls, independently, is formed of a polyacrylate, polyurea, polyurethane, polyacrylamide, poly(acrylate-co-acrylamide), silica, gelatin and gum Arabic, poly(melamine-formaldehyde), poly(urea-formaldehyde), or combination thereof.

51 . The method of claim 49 , further comprising, before step (c), the step of (b1) adding a second water phase and a second dispersant to the first capsule emulsion.

52 . The method of claim 49 , further comprising, before step (b), the step of (a1) causing the formation of a first capsule, in which the first capsule contains the first benefit agent encapsulated by a first capsule wall, and the first capsule wall is formed of the first wall-forming material.

53 . The method of claim 52 , further comprising, after step (a1) and before step (b), the step of (a2) curing the first capsule.

54 . A capsule delivery system prepared by a method of claim 37 .

55 . A consumer product comprising a capsule delivery system of claim 54 .

56 . The consumer product of claim 55 , wherein the consumer product is a personal care product, beauty care product, fabric care product, home ca

Assignees

• Int Flavors & Fragrances Inc

Inventors

• Pringgosusanto Franklin
• Popplewell Lewis Michael
• Brahms John
• Lei Yabin
• Kerschner Judith
• Imperiale Michael V

Classifications

• C11D3/001

  Softening compositions · CPC title

• A61K8/87

  Polyurethanes · CPC title

• A61Q15/00

  Anti-perspirants or body deodorants (deodorisation of air A61L9/00) · CPC title

• A61K8/11 Primary

  Encapsulated compositions · CPC title

• A61K2800/805

  Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95 · CPC title