Solid-state structures with volatile sintering aids, and methods for fabrication and use thereof
US-2024429439-A1 · Dec 26, 2024 · US
US2017008808A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2017008808-A1 |
| Application number | US-201615205070-A |
| Country | US |
| Kind code | A1 |
| Filing date | Jul 8, 2016 |
| Priority date | Jul 8, 2015 |
| Publication date | Jan 12, 2017 |
| Grant date | — |
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A method for efficiently producing fine particles in a complex state from a plurality of raw material components is provided. The method includes spraying a good solvent solution made from a good solvent and the plurality of raw material components dissolved in the good solvent into a poor solvent having a temperature of at least 165° C. higher than the boiling point of the good solvent and evaporating off the good solvent and precipitating a plurality of fine particles.
Opening claim text (preview).
What is claimed is: 1 . A method for producing particles comprising: spraying a good solvent solution comprising a good solvent and a plurality of raw material components dissolved in the good solvent into a poor solvent having a temperature of at least 165° C. higher than the boiling point of the good solvent, to evaporate off the good solvent and precipitate the plurality of particles. 2 . The method for producing particles according to claim 1 , wherein the good solvent solution is in a slurry further comprising at least one type of raw material component in powdered form dispersed in the good solvent. 3 . The method for producing particles according to claim 1 , wherein a total concentration of the plurality of raw material components dissolved in the good solvent is 10 g/l or greater. 4 . The method for producing particles according to claim 1 , wherein the plurality of raw material components are lithium sulfide, lithium iodide and lithium bromide, and the particles are raw material particles of a solid electrolyte material. 5 . Solid solution particles comprising: sulfur, lithium, iodine and bromine as solid solution components, wherein positions of peaks from x-ray diffraction using CuKα rays attributable to the (111) faces of lithium sulfide, lithium iodide and lithium bromide are in a range of diffraction angle 2θ=25.9° or greater and less than 28.0°, and wherein a mean primary particle size of the particles is no greater than 5 μm.
Mixing media, e.g. organic solvents · CPC title
Sulfides, tellurides or selenides · CPC title
Solid materials · CPC title
based on sulfides or selenides {or tellurides} · CPC title
in a liquid medium · CPC title
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