Cross-section processing-and-observation method and cross-section processing-and-observation apparatus
US-9347896-B2 · May 24, 2016 · US
US2016343541A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2016343541-A1 |
| Application number | US-201615162133-A |
| Country | US |
| Kind code | A1 |
| Filing date | May 23, 2016 |
| Priority date | Sep 3, 2013 |
| Publication date | Nov 24, 2016 |
| Grant date | — |
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A cross-section processing-and-observation method includes: a cross-section exposure step of irradiating a sample with a focused ion beam to expose a cross-section of the sample; a cross-sectional image acquisition step of irradiating the cross-section with an electron beam to acquire a cross-sectional image of the cross-section; and a step of repeatedly performing the cross-section exposure step and the cross-sectional image acquisition step along a predetermined direction of the sample at a setting interval to acquire a plurality of cross-sectional images of the sample. In the cross-sectional image acquisition step, a cross-sectional image is acquired under different condition settings for a plurality of regions of the cross-section.
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What is claimed is: 1 . A cross-section processing-and-observation method comprising: a cross-section exposure step of irradiating a sample with a focused ion beam to expose a cross-section of the sample; a cross-sectional image acquisition step of irradiating the cross-section with an electron beam to acquire a cross-sectional image of the cross-section; and a step of repeatedly performing the cross-section exposure step and the cross-sectional image acquisition step along a predetermined direction of the sample at a setting interval to acquire a plurality of cross-sectional images, including a first sectional image and a second sectional image, of the sample, wherein in the cross-sectional image acquisition step, the first cross-sectional image is acquired by irradiating the cross-section with the electron beam a first number of times, and the second cross-sectional image is acquired by irradiating the cross-section with the electron beam a second number of times different from the first number. 2 . The cross-section processing-and-observation method according to claim 1 wherein the setting interval is equal to or an integer multiple of a pixel size of any one of the plurality of regions, or the pixel size is an integer multiple of the setting interval. 3 . The cross-section processing-and-observation method according to claim 1 , further comprising a specific observation target detection step of detecting a predetermined specific observation target, wherein in the specific observation target detection step, after a predetermined specific observation target is detected, a condition setting of the cross-section exposure step and the condition setting of the cross-sectional image acquisition step are updated. 4 . The cross-section processing-and-observation method according to claim 3 , wherein when the condition setting of the cross-section exposure step is updated, the setting interval is set to be shorter than that before the specific observation target is detected. 5 . The cross-section processing-and-observation method according to claim 3 , wherein plural types of the specific observation targets are set, and different condition setting of the cross-section exposure step and different condition setting of the cross-sectional image acquisition step are set for individual regions where the respective specific observation targets are detected. 6 . The cross-section processing-and-observation method according to claim 3 , wherein when the condition setting of the cross-section exposure step and the condition setting of the cross-sectional image acquisition step are set, the setting interval is equal to or an integer multiple of a pixel size of the cross-sectional image. 7 . The cross-section processing-and-observation method according to claim 3 , wherein in the specific observation target detection step, an EDS measurement or an EBSD measurement of the cross-section is performed. 8 . The cross-section processing-and-observation method according to claim 3 , wherein the specific observation target detection step including observing a contrast change of a cross-sectional image obtained in the cross-sectional image acquisition step. 9 . The cross-section processing-and-observation method according to claim 3 , wherein in the specific observation target detection step performed after the specific observation target is detected, cross-section processing-and-observation method is not performed on other portions of the sample when the specific observation target is not detected anymore. 10 . A cross-section processing-and-observation method comprising: a cross-section exposure step of irradiating a sample with a focused ion beam to expose a cross-section of the sample; a cross-sectional image acquisition step of irradiating the cross-section with an electron beam to acquire a cross-sectional image of the cross-section; and a step of repeatedly performing the cross-section exposure step and the cross-sectional image acquisition step along a predetermined direction of the sample at a setting interval to acquire a plurality of cross-sectional images of the sample, wherein in the cross-sectional image acquisition step, when the cross-sectional image is acquired with a high magnification, the setting interval is set smaller than the setting interval in a case that the cross-sectional image is acquired with a magnification lower than the high magnification 11 . The cross-section processing-and-observation method according to claim 10 wherein the setting interval is equal to or an integer multiple of a pixel size of any one of the plurality of regions, or the pixel size is an integer multiple of the setting interval. 12 . The cross-section processing-and-observation method according to claim 10 , further comprising a specific observation target detection step of detecting a predetermined specific observation target, wherein in the specific observation target detection step, after a predetermined specific observation target is detected, a condition setting of the cross-section exposure step and the condition setting of the cross-sectional image acquisition step are updated. 13 . The cross-section processing-and-observation method according to claim 12 , wherein when the condition setting of the cross-section exposure step is updated, the setting interval is set to be shorter than that before the specific observation target is detected. 14 . The cross-section processing-and-observation method according to claim 12 , wherein plural types of the specific observation targets are set, and different condition setting of the cross-section exposure step and different condition setting of the cross-sectional image acquisition step are set for individual regions where the respective specific observation targets are detected. 15 . The cross-section processing-and-observation method according to claim 12 , wherein when the condition setting of the cross-section exposure step and the condition setting of the cross-sectional image acquisition step are set, the setting interval is equal to or an integer multiple of a pixel size of the cross-sectional image. 16 . The cross-section processing-and-observation method according to claim 12 , wherein in the specific observation target detection step, an EDS measurement or an EBSD measurement of the cross-section is performed. 17 . The cross-section processing-and-observation method according to claim 12 , wherein the specific observation target detection step including observing a contrast change of a cross-sectional image obtained in the cross-sectional image acquisition step. 18 . The cross-section processing-and-observation method according to claim 12 , wherein in the specific observation target detection step performed after the specific observation target is detected, cross-section processing-and-observation method is not performed on other portions of the sample when the specific observation target is not detected anymore.
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