High-purity aluminium grain material and method for producing the same

Patent metadata

Field	Value
Publication number	US-2016289801-A1
Application number	US-201615089640-A
Country	US
Kind code	A1
Filing date	Apr 4, 2016
Priority date	Apr 6, 2015
Publication date	Oct 6, 2016
Grant date	—

Abstract

An object of the present invention is to provide an aluminium grain material having significantly high purity, and a method for producing the same. Disclosed is an aluminium grain material having an average mass per grain of 0.01 to 10 g, wherein the total content of twelve elements of silicon (Si), iron (Fe), copper (Cu), magnesium (Mg), titanium (Ti), vanadium (V), chromium (Cr), manganese (Mn), nickel (Ni), zinc (Zn), gallium (Ga), and zirconium (Zr) in the aluminium grain material, measured by glow discharge mass spectrometry, is 5 ppm by mass or less.

First claim

1 . An aluminium grain material having an average mass per grain of 0.01 to 10 g, wherein
the total content of twelve elements of silicon (Si), iron (Fe), copper (Cu), magnesium (Mg), titanium (Ti), vanadium (V), chromium (Cr), manganese (Mn), nickel (Ni), zinc (Zn), gallium (Ga), and zirconium (Zr) in the aluminium grain material, measured by glow discharge mass spectrometry, is 5 ppm by mass or less.

2 . The aluminium grain material according to claim 1 , wherein the total content of the twelve elements is 2.5 ppm by mass or less.

3 . The aluminium grain material according to claim 1 , wherein variation in mass indicated by a value obtained by dividing a standard deviation of the mass of the aluminium grain material by an average of the mass, is 5% or less, in the twenty aluminium grain materials.

4 . The aluminium grain material according to claim 2 , wherein variation in mass indicated by a value obtained by dividing a standard deviation of the mass of the aluminium grain material by an average of the mass, is 5% or less, in the twenty aluminium grain materials.

5 . The aluminium grain material according to claim 1 , wherein the aluminium grain material is a cut wire.

6 . The aluminium grain material according to claim 4 , wherein the aluminium grain material is a cut wire.

7 . The aluminium grain material according to claim 5 , wherein the cut wire has a wire diameter of 0.3 to 20 mm and a length of 1 to 50 mm.

8 . The aluminium grain material according to claim 6 , wherein the cut wire has a wire diameter of 0.3 to 20 mm and a length of 1 to 50 mm.

9 . The aluminium grain material according to claim 5 , wherein variation in wire diameter indicated by a value obtained by dividing a standard deviation of the wire diameter of the cut wire by an average of the wire diameter, is 5% or less, and variation in length indicated by a value obtained by dividing a standard deviation of the length of the cut wire by an average of the length, is 5% or less, in the twenty cut wires.

10 . The aluminium grain material according to claim 6 , wherein variation in wire diameter indicated by a value obtained by dividing a standard deviation of the wire diameter of the cut wire by an average of the wire diameter, is 5% or less, and variation in length indicated by a value obtained by dividing a standard deviation of the length of the cut wire by an average of the length, is 5% or less, in the twenty cut wires.

11 . The aluminium grain material according to claim 7 , wherein variation in wire diameter indicated by a value obtained by dividing a standard deviation of the wire diameter of the cut wire by an average of the wire diameter, is 5% or less, and variation in length indicated by a value obtained by dividing a standard deviation of the length of the cut wire by an average of the length, is 5% or less, in the twenty cut wires.

12 . The aluminium grain material according to claim 8 , wherein variation in wire diameter indicated by a value obtained by dividing a standard deviation of the wire diameter of the cut wire by an average of the wire diameter, is 5% or less, and variation in length indicated by a value obtained by dividing a standard deviation of the length of the cut wire by an average of the length, is 5% or less, in the twenty cut wires.

13 . The aluminium grain material according to claim 1 for forming a film of aluminium, or a film of aluminium-containing inorganic compound(s).

14 . The aluminium grain material according to claim 1 vacuum-packaged in a resin bag not containing a lubricant, an antioxidant, and an antiblocking agent.

15 . A method for producing the aluminium grain material according to claim 1 , which comprises:
a cutting step of cutting an aluminium wire material to obtain a cut wire, and a cleaning step of bringing the cut wire into contact with a cleaning liquid to obtain the aluminium grain material.

16 . The method according to claim 15 , wherein the cleaning liquid is a solution containing at least one selected from the group consisting of hydrochloric acid, nitric acid, sulfuric acid, oxalic acid, citric acid, sodium carbonate, tartaric acid, sodium hydroxide, phosphate, sodium gluconate, and sodium metasilicate.

17 . The method according to claim 15 , wherein a mass reduction rate of the cut wire after contacting with the cleaning liquid is in a range of 0.01 to 20% based on the mass of the cut wire before contacting with the cleaning liquid in the cleaning step.

18 . The method according to claim 16 , wherein a mass reduction rate of the cut wire after contacting with the cleaning liquid is in a range of 0.01 to 20% based on the mass of the cut wire before contacting with the cleaning liquid in the cleaning step.

19 . The method according to claim 15 , wherein a mass reduction rate of the cut wire after contacting with the cleaning liquid is in a range of 0.1 to 10% based on the mass of the cut wire before contacting with the cleaning liquid in the cleaning step.

20 . The method according to claim 16 , wherein a mass reduction rate of the cut wire after contacting with the cleaning liquid is in a range of 0.1 to 10% based on the mass of the cut wire before contacting with the cleaning liquid in the cleaning step.

Assignees

• Sumitomo Chemical Co

Inventors

• Hoshikawa Hiroaki
• Kubo Yuki
• Nagata Akira

Classifications

• C23G1/22

  Light metals · CPC title

• B65D81/2023

  in a flexible container (B65D81/2038 takes precedence) · CPC title

• B08B3/08

  the liquid having chemical or dissolving effect · CPC title

• B21F11/00

  Cutting wire · CPC title

• C23G1/125

  aluminium · CPC title