Processing biomass

Patent metadata

Field	Value
Publication number	US-2016201152-A1
Application number	US-201514897947-A
Country	US
Kind code	A1
Filing date	Jul 21, 2015
Priority date	Jul 21, 2014
Publication date	Jul 14, 2016
Grant date	—

Abstract

Biomass feedstocks (e.g., plant biomass, animal biomass, and municipal waste biomass) are processed to produce useful products, such as fuels. For example, systems are described that can be useful for separating solids and high molecular weight species from liquids of bioprocessed biomass material slurries.

First claim

1 . A purification method comprising:
producing a first permeate from a bioprocessed feedstock by retaining material from the bioprocessed feedstock with a molecular weight above about a first molecular weight from the bioprocessed feedstock utilizing a first membrane filter, and producing a second permeate from the first permeate by retaining from the first permeate material with a molecular weight above about a second molecular weight from the first permeate utilizing a second membrane filter.

2 . The method of claim 1 , wherein the bioprocessed feedstock is produced by saccharification of a biomass material.

3 . The method of claim 2 , wherein saccharification is done by contacting the biomass material with an enzyme or organism.

4 . The method of claim 2 , wherein the biomass material is a cellulosic or lignocellulosic material.

5 . The method of claim 1 , wherein the bioprocessed feedstock is in the form of a slurry that includes less than about 1% solids.

6 . The method of claim 5 , wherein the solids have a median particle size of less than about 10 μm.

7 . The method of claim 5 , wherein the bioprocessed feedstock is filtered to remove solids prior to utilizing the first membrane filter.

8 . The method of claim 7 , wherein the bioprocessed feedstock includes at least about 1% solids before being filtered.

9 . The method of claim 7 , wherein the bioprocessed feedstock is filtered by a method selected from decanter centrifuging, disc centrifuging, stack filtration, plate filtration, micro filtration, column filtration, Vibratory Enhanced Separation Processes and combinations of these.

10 . The method of claim 1 , wherein the bioprocessed feedstock is a fermentation product.

11 . The method of claim 1 , wherein the bioprocessed feedstock is a distillation residue including at least one sugar.

12 . The method of claim 1 , wherein the bioprocessed feedstock comprises between about 0.1 and about 50% xylose.

13 . The method of claim 1 , wherein the bioprocessed feedstock has had at least one volatile compound removed therefrom under vacuum prior to it being filtered by the first membrane filter.

14 . The method of claim 13 , wherein the volatile compound is an ester.

15 . The method of claim 13 , wherein the volatile compound is an alcohol.

16 . The method of claim 14 , wherein the concentration of alcohol in the bioprocessed feedstock is less than about 5.

17 . The method of claim 1 , wherein the first molecular weight is higher than the second molecular weight.

18 . The method of claim 1 , wherein the first molecular weight is at least about 100 kDa.

19 . The method of claim 1 , wherein the first membrane filter retains particles larger than about 0.05 μm from the bioprocessed feedstock.

20 . The method of claim 1 , wherein the second molecular weight is at least about 2 kDa.

21 . The method of claim 1 , wherein the first permeate has a turbidity of less than about 5 Nephelometric turbidity units, or the second permeate has a turbidity of at least about 5 NTU.

22 . The method of claim 1 , wherein the second permeate has a color of less than about 200 units by the Platinum-Cobalt ASTM Test Method D1209.

23 . The method of claim 1 , wherein the first and second membrane filters are configured as cross flow filters.

24 . The method of claim 23 , wherein the first and/or second membrane filters are spiral wound filters, tube filters or hollow fiber filters.

25 . The method of claim 23 , wherein the first and/or second membrane filters are configured as tube filters with a diameter between about ¼ and about 1 inch.

26 . The method of claim 23 , wherein the inlet pressure at the first and/or the second membrane filter is between about 90 and about 500 PSIG and the outlet pressure at the first and/or second membrane filter is between about 20 and about 430 PSIG.

27 . The method of claim 25 , wherein the bioprocessed feedstock flows through the tube at a flow rate between about 1 and about 20 GPM.

28 . The method of claim 25 , wherein the first and/or second membrane filters are configured as modules including two or more bundles of tube filters per module.

29 . The method of claim 28 , wherein more than one module is utilized to process the liquefied biomass material and/or the first permeate.

30 . The method of claim 1 , wherein the bioprocessed feedstock and the first permeate are at a temperature between about 30 and about 70 deg C. when filtered through the first and second membrane filters.

31 . The method of claim 1 , further comprising concentrating the first permeate.

32 . The method of claim 1 , further comprising concentrating the second permeate.

33 . The method of claim 1 , wherein the second permeate is processed utilizing a system selected from the group consisting of an evaporator, electrodialysis, electrodialysis reversal, simulated moving bead chromatography, and combinations thereof.

34 . The method of claim 9 , wherein the bioprocessed feedstock is filtered by through a process comprising two centrifuges utilized in series.

35 . The method of claim 14 , wherein the volatile compound comprises a butyrate ester, or a lactate ester.

Assignees

• Xyleco Inc

Inventors

• Medoff Marshall
• Masterman Thomas Craig
• Cahill John M

Classifications

• Y02E50/10

  Biofuels, e.g. bio-diesel · CPC title

• C13B20/165 Primary

  using membranes, e.g. osmosis, ultrafiltration (electrodialysis C13B20/18) · CPC title

• C13K13/002

  Xylose · CPC title

• B01D61/58 Primary

  Multistep processes · CPC title

• B01D2315/12

  Feed-and-bleed systems · CPC title