Apparatus and method for producing a graphene material

Patent metadata

Field	Value
Publication number	US-2016186341-A1
Application number	US-201514976267-A
Country	US
Kind code	A1
Filing date	Dec 21, 2015
Priority date	Dec 25, 2014
Publication date	Jun 30, 2016
Grant date	—

Abstract

An apparatus for producing a graphene material includes a tank, a container, an agitating module, a second electrode disposed in the tank, and a power supply module. The container is used for receiving a graphite material, and is formed with a plurality of through holes for the electrolyte solution to pass therethrough. The agitating module includes a control unit and an agitating unit used as a first electrode, and inserted into the container for agitating the electrolyte solution and the graphite material. The power supply module is electrically connected to the agitating unit and the second electrode for supplying electric power to generate an electrical potential difference.

First claim

What is claimed is:

1 . An apparatus for producing a graphene material, comprising:
a tank that is adapted for receiving an electrolyte solution; a container that is placed in said tank, that is adapted for receiving a graphite material, and that is formed with a plurality of through holes for the electrolyte solution to pass therethrough; an agitating module that includes a control unit and an agitating unit controlled by said control unit, said agitating unit being electrically conductive to be used as a first electrode, and being inserted into said container for agitating the electrolyte solution and the graphite material; a second electrode that is disposed in said tank and that is spaced apart from said agitating unit of said agitating module; and a power supply module electrically connected to said agitating unit and said second electrode for supplying electric power to said agitating unit and said second electrode to generate an electrical potential difference between said agitating unit and said second electrode.

2 . The apparatus as claimed in claim 1 , wherein each of said through holes of said container has a maximum diameter not greater than 5 μm.

3 . The apparatus as claimed in claim 1 , wherein said agitating unit includes a shank that is connected to said control unit, and a plurality of blades mounted to said shank opposite to said control unit.

4 . The apparatus as claimed in claim 1 , wherein said agitating module is a homogenizer.

5 . A method for producing a graphene material, comprising the steps of:
providing an apparatus of claim 1 ; disposing an electrolyte solution in the tank and the container; disposing a graphite material into the container; electrolyzing the electrolyte solution to form ions by generating a first electrical potential difference between the agitating unit and the second electrode; intercalating the ions into the graphite material; and agitating the electrolyte solution and the graphite material with the agitating module to exfoliate the graphite material.

6 . The method as claimed in claim 5 , wherein, in the agitating step, a second electrical potential difference is generated between the agitating unit and the second electrode.

7 . The method as claimed in claim 6 , wherein, in the agitating step, the agitating unit has an electrical potential higher than an electrical potential of the second electrode.

8 . The method as claimed in claim 6 , wherein, in the agitating step, the agitating unit has an electrical potential lower than an electrical potential of the second electrode.

9 . The method as claimed in claim 5 , wherein, in the electrolyzing step, the agitating unit has an electrical potential higher than an electrical potential of the second electrode.

10 . The method as claimed in claim 5 , wherein, in the electrolyzing step, the agitating unit has an electrical potential lower than an electrical potential of the second electrode.

11 . The method as claimed in claim 5 , wherein, in the providing step, a surfactant is added into the electrolyte solution.

12 . The method as claimed in claim 5 , wherein, in the electrolyzing step, the electrolyte solution and the graphite material are agitated by the agitating module at a first agitating rate.

13 . The method as claimed in claim 12 , wherein, in the agitating step, the electrolyte solution and the graphite material are agitated by the agitating module at a second agitating rate that is greater than the first agitating rate.

Assignees

• Univ Nat Taiwan Normal

Inventors

• Yang Chii-Rong
• Chang shu-fang
• Teng Tun-Ping
• Chen Yu-Ting
• Chen zi-ying
• Chang Sheng-Chang
• Huang Meng-Hung

Classifications

• C01B2204/04

  Specific amount of layers or specific thickness · CPC title

• C25B15/02 Primary

  Process control or regulation · CPC title

• C25B1/00

  Electrolytic production of inorganic compounds or non-metals · CPC title

• C01B2204/32

  Size or surface area · CPC title

• C01P2004/64

  Nanometer sized, i.e. from 1-100 nanometer · CPC title