Spinning nozzle, process for producing fibrous mass, fibrous mass, and paper
US-2015376815-A1 · Dec 31, 2015 · US
US2016177471A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2016177471-A1 |
| Application number | US-201414899225-A |
| Country | US |
| Kind code | A1 |
| Filing date | Jun 13, 2014 |
| Priority date | Jun 18, 2013 |
| Publication date | Jun 23, 2016 |
| Grant date | — |
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The present invention relates to a direct dissolving process for the production of polysaccharide fibers which contain α(1→3)-glucan as a fiber-forming substance, with aqueous sodium hydroxide solution as a solvent, as well as to the fibers made thereby, and to their use.
Opening claim text (preview).
1 . A method for the production of a polysaccharide fiber whose fiber-forming substance is α(1→3)-glucan, wherein the method is a direct dissolving process which comprises the step of spinning the fiber by extruding a spinning solution comprising an aqueous sodium hydroxide solution, wherein the spinning occurs in a spin bath, and wherein a spun fiber is formed. 2 . The method according to claim 1 , wherein the aqueous sodium hydroxide solution concentration in the spinning solution is between 4.0 and 5.5% by weight related to the total quantity of the spinning solution. 3 . The method according to claim 1 , wherein the spin bath comprises H 2 SO 4 in a concentration between 200 and 500 g/l. 4 . The method according to claim 1 , wherein the H 2 SO 4 concentration in the spin bath is between 20 and 60 g/l. 5 . The method according to claim 1 , wherein the spun fiber is subsequently stretched in an acid regeneration bath. 6 . The method according to claim 1 , wherein at least 90% of the α(1→3)-glucan are hexose units and at least 50% of the hexose units are linked via α(1→3)-glycosidic bonds. 7 . The method according to claim 1 , 2 , 3 , 4 , 5 , or 6 , wherein the fiber is selected from the group consisting of a staple fiber and a continuous filament. 8 . A polysaccharide fiber whose fiber-forming substance is α(1→3)-glucan, wherein the fiber is produced using a direct dissolving process in aqueous sodium hydroxide solution. 9 . The fiber according to claim 8 , wherein at least 90% of the α(1→3)-glucan are hexose units and at least 50% of the hexose units are linked via α(1→3)-glycosidic bonds. 10 . The fiber according to claim 8 or 9 , wherein the fiber is selected from the group consisting of a staple fiber and a continuous filament. 11 . A textile product comprising the fiber according to claim 8 , wherein the textile product is selected from the group consisting of yarns, woven fabrics, and knitted fabrics. 12 . A product comprising the fiber according to claim 8 , wherein the product is selected from the group consisting of nonwovens, hygiene products and knitted fabrics. 13 . The textile product according to claim 11 , wherein the fiber is selected from the group consisting of a staple fiber and a continuous filament. 14 . The product according to claim 12 , wherein the fiber is selected from the group consisting of a staple fiber and a continuous filament. 15 . The product according to claim 12 , wherein the hygiene products are selected from the group consisting of tampons, panty liners and diapers.
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