Preparation method of titanium alloy powders
US-12083602-B2 · Sep 10, 2024 · US
US2016138149A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2016138149-A1 |
| Application number | US-201615005281-A |
| Country | US |
| Kind code | A1 |
| Filing date | Jan 25, 2016 |
| Priority date | Jul 19, 2010 |
| Publication date | May 19, 2016 |
| Grant date | — |
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Processes for forming an article from an α+β titanium alloy are disclosed. The α+β titanium alloy includes, in weight percentages, from 2.90 to 5.00 aluminum, from 2.00 to 3.00 vanadium, from 0.40 to 2.00 iron, and from 0.10 to 0.30 oxygen. The α+β titanium alloy is cold worked at a temperature in the range of ambient temperature to 500° F., and then aged at a temperature in the range of 700° F. to 1200° F.
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What is claimed is: 1 . A process comprising: cold drawing an α+β titanium alloy workpiece at a temperature in the range of ambient temperature to 500° F.; and direct aging the cold drawn α+β titanium alloy workpiece at a temperature in the range of 700° F. to 1200° F.; the α+β titanium alloy comprising, in weight percentages, from 2.90 to 5.00 aluminum, from 2.00 to 3.00 vanadium, from 0.40 to 2.00 iron, from 0.10 to 0.30 oxygen, titanium, and incidental impurities. 2 . The process of claim 1 , comprising cold drawing the α+β titanium alloy workpiece to a 20% to 60% reduction in area. 3 . The process of claim 1 , wherein the cold drawing of the α+β titanium alloy comprises at least two drawing cycles, wherein each drawing cycle comprises cold drawing the α+β titanium alloy workpiece to an at least 10% reduction in area. 4 . The process of claim 1 , comprising cold drawing the α+β titanium alloy workpiece at ambient temperature. 5 . The process of claim 1 , comprising direct aging the α+β titanium alloy workpiece at a temperature in the range of 800° F. to 1100° F. 6 . The process of claim 1 , comprising direct aging the α+β titanium alloy workpiece for 0.5 to 10 hours at temperature. 7 . The process of claim 1 , further comprising hot working the α+β titanium alloy workpiece at a temperature in the range of 300° F. to 25° F. below the β-transus temperature of the α+β titanium alloy, wherein the hot working is performed before the cold drawing. 8 . The process of claim 1 , further comprising hot working the α+β titanium alloy workpiece at a temperature in the range of 1500° F. to 1775° F., wherein the hot working is performed before the cold drawing. 9 . The process of claim 7 , further comprising annealing the α+β titanium alloy at a temperature in the range of 1200° F. to 1500° F., wherein the annealing is performed between the hot working and the cold drawing. 10 . The process of claim 1 , wherein the cold drawing and direct aging forms an α+β titanium alloy article having an ultimate tensile strength in the range of 155 ksi to 200 ksi and an elongation in the range of 8% to 20%, at ambient temperature. 11 . The process of claim 10 , wherein the α+β titanium alloy article is selected from the group consisting of a billet, a bar, a rod, a tube, a slab, a plate, and a fastener. 12 . The process of claim 10 , wherein the α+β titanium alloy article has a diameter or thickness greater than 0.5 inches, an ultimate tensile strength greater than 165 ksi, a yield strength greater than 155 ksi, and an elongation greater than 12%. 13 . A process comprising: cold working an α+β titanium alloy workpiece at a temperature in the range of ambient temperature to 500° F.; and direct aging the cold worked α+β titanium alloy workpiece at a temperature in the range of 700° F. to 1200° F.; the α+β titanium alloy comprising, in weight percentages, from 2.90 to 5.00 aluminum, from 2.00 to 3.00 vanadium, from 0.40 to 2.00 iron, from 0.10 to 0.30 oxygen, titanium, and incidental impurities. 14 . The process of claim 13 , wherein cold working the α+β titanium alloy comprises cold working by at least one operation selected from the group consisting of rolling, forging, extruding, pilgering, and drawing. 15 . The process of claim 13 , comprising direct aging the α+β titanium alloy workpiece for 0.5 to 10 hours at temperature. 16 . The process of claim 13 , further comprising hot working the α+β titanium alloy workpiece at a temperature in the range of 300° F. to 25° F. below the β-transus temperature of the α+β titanium alloy, wherein the hot working is performed before the cold working. 17 . The process of claim 16 , further comprising annealing the α+β titanium alloy at a temperature in the range of 1200° F. to 1500° F., wherein the annealing is performed between the hot working and the cold working. 18 . The process of claim 13 , wherein the cold working and direct aging forms an α+β titanium alloy article having an ultimate tensile strength in the range of 155 ksi to 200 ksi and an elongation in the range of 8% to 20%, at ambient temperature. 19 . The process of claim 18 , wherein the α+β titanium alloy article is selected from the group consisting of a billet, a bar, a rod, a tube, a slab, a plate, and a fastener. 20 . The process of claim 18 , wherein the α+β titanium alloy article has a diameter or thickness greater than 0.5 inches, an ultimate tensile strength greater than 165 ksi, a yield strength greater than 155 ksi, and an elongation greater than 12%. 21 . A process comprising: hot working an α+β titanium alloy workpiece at a temperature in the range of 1500° F. to 1775° F.; annealing the α+β titanium alloy at a temperature in the range of 1200° F. to 1500° F.; cold working the α+β titanium alloy workpiece at ambient temperature to a 20% to 60% reduction in area; and direct aging the cold worked α+β titanium alloy workpiece at a temperature in the range of 800° F. to 1100° F.; the α+β titanium alloy comprising, in weight percentages, from 2.90 to 5.00 aluminum, from 2.00 to 3.00 vanadium, from 0.40 to 2.00 iron, from 0.10 to 0.30 oxygen, titanium, and incidental impurities.
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