Method for impregnating a porous body by a suspension and installation for implementing same

Patent metadata

Field	Value
Publication number	US-2016107941-A1
Application number	US-201514919140-A
Country	US
Kind code	A1
Filing date	Oct 21, 2015
Priority date	Aug 2, 2011
Publication date	Apr 21, 2016
Grant date	—

Abstract

The present invention relates to a method for impregnating a porous body ( 14 ) by a suspension ( 12 ) containing at least partly particles, said body comprising a multiplicity of channels ( 16 ) delimited by porous walls ( 22 ) extending from one ( 18 ) of the faces to the other ( 20 ) face of said body, part of said channels being obstructed at one face and the other part of the channels being obstructed at the other face.
According to the invention, the method consists in:
making a suspension whose particle size distribution meets a D V90 /D pores ratio below 0.25 and whose viscosity is such that said suspension is brought inside the walls while depositing part of the particles on the surface of the pores of the walls, communicating one ( 18, 20 ) of the faces of body ( 14 ) with an enclosure ( 30 ) containing the suspension, feeding the suspension into the body, exerting a force on the suspension introduced so that said suspension flows through the walls, passing a fluid through the walls.

First claim

26 . A method for impregnating a porous body by a suspension containing at least partly particles, said body comprising a multiplicity of channels delimited by porous walls extending from one face of said body to another face of said body, part of said channels being obstructed at the one face and another part of the channels being obstructed at the another face, characterized in that the method comprises:
making a suspension whose particle size distribution meets D v90 /D pores ratio below 0.25 and whose viscosity is such that said suspension is brought inside the walls while depositing part of the particles on the surface of the pores of the walls, communicating the one face of the body with an enclosure containing the suspension, feeding the suspension into the body, exerting a force on the suspension introduced so that the suspension flows through the walls passing a fluid through the walls.

27 . A method for impregnating a porous body as claimed in claim 26 , characterized in that it comprises exerting a pressure on the suspension introduced.

28 . A method for impregnating a porous body as claimed in claim 26 , characterized in that it comprises exerting an underpressure on the suspension introduced.

29 . A method for impregnating a porous body as claimed in claim 26 , characterized in that it comprises using a gas as the fluid.

30 . A method for impregnating a porous body as claimed in claim 26 , characterized in that it comprises using an inert gas as the fluid.

31 . A method for impregnating a porous body as claimed in claim 26 , characterized in that it comprises carrying out at least another suspension impregnation in the body.

32 . A method for impregnating a porous body as claimed in claim 26 , characterized in that it comprises turning the body over so as to carry out at least another impregnation.

33 . A method for impregnating a porous body as claimed in claim 26 , characterized in that it comprises communicating the another face of the body with a collector base.

34 . A method for impregnating a porous body as claimed in claim 33 , characterized in that it comprises connecting the collector base to a suspension and/or fluid recovery device.

35 . A method for impregnating a porous body as claimed in claim 26 , characterized in that it comprises placing the body in a sealed sheath.

36 . A method for impregnating a porous body as claimed in claim 26 , characterized in that it comprises drying and calcining the body after impregnation.

37 . A process of treating at least one pollutant contained in an exhaust gas by contacting said exhaust gas with said porous body impregnated according to the method of claim 26 .

38 . A process of filtering a liquid stream by contacting said liquid stream with said porous body impregnated according to the method of claim 26 .

39 . Installation intended for impregnation of a porous body comprising a multiplicity of channels delimited by porous walls extending from one face of said body to another face of said body, part of said channels being obstructed at the one face to form outlet channels and another part of the channels being obstructed at the another face to form inlet channels, the installation comprising an enclosure containing an impregnation suspension with at least partly particles, said enclosure communicating with the one face of the porous body, characterized in that said installation comprises a device for pressurizing the enclosure with a fluid for forcing the suspension into the porous body through the inlet channels and while maintaining the fluid pressure flowing the fluid into the inlet channels, through the porous body and outlet channels to discharge excess suspension.

40 . A porous body impregnation installation as claimed in claim 39 , characterized in that it comprises a sealed sheath intended to receive the body.

41 . A porous body impregnation installation as claimed in claim 40 , characterized in that it comprises a sealing membrane between the sheath and the body.

42 . A porous body impregnation installation as claimed in claim 41 , characterized in that the membrane is an expansible membrane.

43 . A porous body impregnation installation as claimed in claim 42 , characterized in that the membrane is an inflatable membrane.

44 . A porous body impregnation installation as claimed in claim 39 , characterized in that it comprises a collector base.

45 . A porous body impregnation installation as claimed in claim 44 , characterized in that the collector base comprises suspension discharge means.

46 . A porous body impregnation installation as claimed in claim 39 , further comprising a recovery device communicating with the another face of the porous body for collecting at least one of suspension and pressurized fluid forced through the porous body.

47 . A method for impregnating a porous body as claimed in claim 26 , wherein said fluid is a pressurized gas which is fed into the enclosure after said feeding the suspension into the body for exerting said force on the suspension introduced so that the suspension flows through the porous walls and, while maintaining the force of the pressurized gas on the suspension introduced, the pressurized gas is passed through the porous walls to discharge excess suspension contained in the pores of the walls and carry out a first drying of a film of the suspension deposited.

48 . A method for impregnating a porous body as claimed in claim 26 ,
wherein said channels obstructed at the another face form inlet channels and said channels obstructed at the one face form outlet channels, wherein said step of feeding the suspension into the body introduces the suspension through the one face into the inlet channels in the body prior to said step of exerting a force, wherein after said feeding of said suspension into said inlet channels said step of exerting a force on the suspension introduced is performed with introducing a pressurized gas in said enclosure as said fluid to flow the suspension introduced through the walls and then pass the pressurized gas through the walls.

49 . A porous body impregnation installation as claimed in claim 39 , wherein the enclosure is a vertical enclosure that has a lower opening through which suspension in the enclosure is communicated with the one face of the porous body located below the lower opening.

50 . A porous body impregnation installation as claimed in claim 49 , further comprising a collector base located below the porous body communicating with the another face of the porous body, the collector base comprising suspension discharge means.

Assignees

• IFP Energies Nouvelles
• Ceramiques Tech Et Ind S A
• Ceramiques Tech Et Ind S A

Inventors

• Lambert Arnold
• Leminter Philippe
• Becue Thierry
• Joulin Jean-Pierre
• Cartoixa Bruno

Classifications

• B01J23/63

  with rare earths or actinides · CPC title

• B01J37/0201

  Impregnation · CPC title

• B01J23/464

  Rhodium · CPC title

• B01D2255/1023

  Palladium · CPC title

• C04B41/009

  characterised by the material treated · CPC title