Method for forming a cutting element and downhole tools incorporating the same
US-9193038-B2 · Nov 24, 2015 · US
US2016047171A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2016047171-A1 |
| Application number | US-201514921040-A |
| Country | US |
| Kind code | A1 |
| Filing date | Oct 23, 2015 |
| Priority date | Dec 9, 2011 |
| Publication date | Feb 18, 2016 |
| Grant date | — |
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Cutting elements include an ultrahard material body formed at high pressure and high temperature conditions in the absence of catalyzing material to provide a material microstructure comprising a matrix phase of bonded together ultrahard material particles and interstitial regions disposed throughout the matrix phase providing porosity of less than about 6 volume percent. The body may include a substrate attached thereto, and may include an infiltrant material disposed in a population of the interstitial regions. The body may have regions with different porosities, e.g., with a higher porosity region located adjacent a substrate interface and/or along a central region. The body may include more than one infiltrant, each located in different regions. The infiltrant may be introduced into the body during a separate high pressure/high temperature process. The body may include a region which extends a depth from a working surface that is substantially free of any infiltrant.
Opening claim text (preview).
What is claimed is: 1 . A bit for drilling earthen formations comprising: a bit body; and one or more cutting elements attached thereto, wherein one or more of the cutting elements are prepared by: subjecting a material comprising a plurality of ultrahard material particles to a sufficiently high pressure/high temperature condition to form a sintered ultrahard material body, wherein the ultrahard material body has a material microstructure comprising a matrix phase of bonded together ultrahard material particles and interstitial regions disposed throughout the matrix phase providing a porosity in the range from about 1 to 6% volume, based on the total volume of the ultrahard material body; removing the sintered ultrahard material body from the high pressure and temperature conditions; and introducing an infiltrant material into the interstitial regions of the ultrahard material body subsequent by subjecting the ultrahard material body and an infiltrant material to a second high pressure/high pressure condition. 2 . The bit of claim 1 , further comprising one or more fixed blades projecting outwardly from the bit body and having one or more cutting elements disposed thereon. 3 . The bit of claim 1 , further comprising one or more legs extending from the bit body, each leg comprising a journal having a cone rotatably attached thereto, wherein one or more cutting elements are disposed thereon. 4 . The bit of claim 1 , wherein the porosity of the ultrahard material body after the step of subjecting is in the range of from about 2 to 5 volume %, based on the total volume of the ultrahard material body. 5 . The bit of claim 1 , wherein at least a portion of the ultrahard material particles comprise diamond particles. 6 . The bit of claim 1 , wherein the infiltrant material is selected from Group VIII metals, combinations, and alloys thereof. 7 . The bit of claim 1 , wherein the infiltrant material is selected from Groups IIA, IB, IIB metals, combinations, and alloys thereof. 8 . The bit of claim 1 , wherein the infiltrant material is selected from the group consisting of Si, Ti, Ge, combinations, and alloys thereof. 9 . The bit of claim 1 , wherein the infiltrant material is selected from carbonates of Group IA or IIA metals, their combinations or compounds which include them. 10 . The bit of claim 1 , wherein during the step of introducing, controlling introduction of infiltrant material to provide a first region in the ultrahard material body comprising the infiltrant material, and a second region that is substantially free of the infiltrant material. 11 . The bit of claim 14 , wherein the second region extends a depth from a working surface of the ultrahard material body. 12 . The bit of claim 1 , wherein the ultrahard material body produced during the step of subjecting comprises a first region having a porosity that is different from a second region. 13 . A method of making a bit for drilling earthen formations comprising operatively connecting one or more cutting elements to a bit body, wherein one or more of the cutting elements have been prepared by: subjecting a material comprising a plurality of ultrahard material particles to a first high pressure/high temperature condition to form a sintered ultrahard material body in the substantial absence of a catalyzing material, wherein the ultrahard material body has a material microstructure comprising a matrix phase of bonded together ultrahard material particles and interstitial regions disposed throughout the matrix phase providing a porosity in the range from about 1 to 6 volume percent based on the total volume of the ultrahard material body; removing the ultrahard material body from the first high pressure/high temperature condition; and introducing an infiltrant material into at least a portion of the interstitial regions of the ultrahard material body during a second high pressure/high temperature condition. 14 . The method of claim 13 , wherein after the step of removing, a material containing the infiltrant material is positioned adjacent a surface of the ultrahard material body. 15 . The method of claim 14 , wherein during the step of introducing, the high pressure/high temperature condition is sufficient to melt the infiltrant material and cause it to infiltrate into at least a portion of the interstitial regions of the ultrahard material body. 16 . The method of claim 14 wherein during the temperature during the step of subjecting is higher than the melting temperature of the infiltrant material during the step of introducing. 17 . The method of claim 13 , further comprising treating the ultrahard material body to remove a portion of the infiltrant material from a region extending a depth from a working surface of the ultrahard material body, wherein the infiltrant material remains in another region of the body. 18 . The method of claim 13 , wherein during the step of introducing, controlling introduction of infiltrant material to provide a first region in the ultrahard material body comprising the infiltrant material, and a second region that is substantially free of the infiltrant material. 19 . The method of claim 18 , wherein the second region extends a depth from a working surface of the ultrahard material body. 20 . The method of claim 13 , wherein the ultrahard material body produced during the step of subjecting comprises a first region having a porosity that is different from a second region.
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