Sensor assembly for a differential scanning calorimeter

Patent metadata

Field	Value
Publication number	US-12596086-B2
Application number	US-202318371640-A
Country	US
Kind code	B2
Filing date	Sep 22, 2023
Priority date	Sep 26, 2022
Publication date	Apr 7, 2026
Grant date	Apr 7, 2026

Abstract

A sensing unit for a differential scanning calorimeter includes a superposition of layers of a thermoelectric arrangement, a layer of an electrical heater arrangement and a layer of an absolute temperature measurement arrangement. The thermoelectric arrangements, the electrical heater arrangements and the absolute temperature measurement arrangements are symmetrically arranged on a sample-side and a reference-side of the sensor.

First claim

What is claimed is:

1 . A sensing unit for a differential scanning calorimeter comprising:
a disc-like substrate suitable for being mounted in heat conductive contact with a temperature-controlled heat source of said differential scanning calorimeter, said disc-like substrate comprising:
sample-side and reference-side pan support regions adapted to receive thereon in heat conductive contact therewith a bottom of a sample pan and a reference pan, respectively;
sample-side and reference-side thermoelectric arrangements for generating between two terminal portions thereof sample-side and reference-side electrical voltage signals, respectively, indicative of flows of heat across sample-side and reference-side measuring regions, respectively; and
sample-side and reference-side electrical heater arrangements beneath said sample-side and reference-side pan support regions, respectively; and
sample-side and reference-side absolute temperature measurement arrangements beneath said sample-side and reference-side pan support regions, respectively.

2 . The sensing unit of claim 1 , wherein:
a thickness of said disc-like substrate is reduced beneath said sample-side and reference-side measuring regions, respectively.

3 . The sensing unit of claim 1 , wherein:
each of said sample-side and reference-side electrical heater arrangements comprises a resistive heating trace meandering between a central portion and a peripheral portion of said sample-side and reference-side pan support regions, respectively.

4 . The sensing unit of claim 1 , wherein:
each of said sample-side and reference-side absolute temperature measurement arrangements comprises a temperature sensitive resistive trace meandering in a pattern that is symmetric in relation to a central axis across said sample-side and reference-side pan support regions, respectively.

5 . The sensing unit of claim 1 , wherein the disc-like substrate further comprises:
a plurality of connector pads adapted for having external wiring connected thereto.

6 . The sensing unit of claim 1 , further comprising:
at least one locating tab formed at an outer circumference of said disc-like substrate and configured to be brought into a positive fit with a complementarily formed positioning recess of said differential scanning calorimeter.

7 . The sensing unit of claim 1 , further comprising:
a multi-layered structure arranged on an upper side of the disc-like substrate, whereby, starting from the disk-like substrate, the multi-layered structure comprises the following layers, in the following sequence: a layer of electrical heater arrangements; an insulating layer; a second layer of thermoelectric arrangements; an insulating layer; a first layer of thermoelectric arrangements; and an insulating layer; whereby a layer of the absolute temperature measurement arrangements is arranged between the upper side of the disc-like substrate and the layer of the electrical heater arrangements; and whereby an additional insulating layer is arranged between the layer of the electrical heater arrangements and the layer of the absolute temperature measurement arrangements.

8 . A sensor assembly comprising:
the sensing unit of claim 1 ; and an elongate member extending along a longitudinal axis, whereby an axial end portion of the elongate member comprises an electrical contact arrangement to thereby form a plug member to be brought into electrical contact with a complementarily formed socket member of said differential scanning calorimeter, where said electrical contact arrangement is electrically connected to connector pads of said sensing unit.

9 . The sensor assembly of claim 8 , wherein:
said elongate member has a cylindrical outer circumference; and said electrical contact arrangement comprises elongate contact lugs that extend parallel to said longitudinal axis and are mutually spaced along the outer circumference and are electrically connected with said connector pads by connecting wires that are arranged in an axially extending hollow space formed in said elongate member.

Assignees

• Mettler Toledo Gmbh

Inventors

• Meyer Thomas
• Huetter Thomas

Classifications

• G01N25/486

  Sample holders · CPC title

• G01N25/4866 Primary

  by using a differential method · CPC title

• G01K17/00 Primary

  Measuring quantity of heat (measuring temperature by calorimetry G01K3/00 - G01K11/00; specially adapted for measuring thermal properties of materials, e.g. specific heat, heat of combustion G01N) · CPC title