Method for removing hydrogen phosphate from an aqueous solution using alpha zirconium phosphate
US-9517424-B2 · Dec 13, 2016 · US
US12569824B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-12569824-B2 |
| Application number | US-202118008719-A |
| Country | US |
| Kind code | B2 |
| Filing date | May 26, 2021 |
| Priority date | Jun 8, 2020 |
| Publication date | Mar 10, 2026 |
| Grant date | Mar 10, 2026 |
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The present invention relates to a chitosan-titanium composite, a preparation method and use thereof, and more particularly, a chitosan-titanium composite capable of effectively adsorbing and desorbing 68 Ge/ 68 Ga by combining small molecular chitosan with titanium metal oxide to increase adsorption reactivity to 68 Ge and 68 Ga desorption reactivity, and a preparation method and use thereof.
Opening claim text (preview).
The invention claimed is: 1 . A method for manufacturing a chitosan-titanium composite, the method comprising: a step of preparing a first solution by adding small molecular chitosan powder to an acetic acid solution; a step of preparing a second solution by adding a titanium solution to the first solution; a step of forming a bead by dropping the second solution into ammonia water; and a step of washing, drying and sintering the bead, wherein the small molecular chitosan has a molecular weight of 50,000 to 190,000 Da, and wherein the bead has a diameter of 200 to 400 μm. 2 . The method according to claim 1 , wherein in the step of forming beads by dropping the second solution into aqueous ammonia, the falling flow rate of the second solution is adjusted to 5 to 10 mL/min. 3 . The method according to claim 1 , wherein the sintering step is performed at 400 to 500° C. for 6 to 8 hours. 4 . The method according to claim 1 , wherein the chitosan-titanium composite is used for the adsorption of radioactive isotope. 5 . The method according to claim 4 , wherein the radioactive isotope is 68 Ge.
Chemical treatments not covered by groups B01J20/3007 - B01J20/3078 · CPC title
Thermal treatment, e.g. calcining or pyrolizing · CPC title
Washing or leaching · CPC title
Other properties, e.g. density, crush strength · CPC title
Naturally occurring macromolecular compounds, e.g. humic acids or their derivatives · CPC title
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