Rare earth oxyfluoride sintered body and method for producing same
US-2019345069-A1 · Nov 14, 2019 · US
US12559381B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-12559381-B2 |
| Application number | US-202117528682-A |
| Country | US |
| Kind code | B2 |
| Filing date | Nov 17, 2021 |
| Priority date | Nov 25, 2020 |
| Publication date | Feb 24, 2026 |
| Grant date | Feb 24, 2026 |
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A sintered body, a method of fabricating the sintered body, a semiconductor fabricating device, and a method of fabricating the semiconductor fabricating device, the sintered body including 50 mass % or more of Y 5 O 4 F 7 , wherein the sintered body has a relative density of 97.0% or more and a Vickers hardness of 2.4 GPa or more.
Opening claim text (preview).
What is claimed is: 1 . A method of fabricating a sintered body, the method comprising: molding a molded body including a Y 5 O 4 F 7 powder; forming a composite sintered body by sintering the molded body at a temperature of 1,000° C. or higher under an argon gas atmosphere or a vacuum atmosphere of 10 −3 Pa or less; and selecting a sintered body from the composite sintered body, wherein the selected sintered body includes 50 mass % or more of Y 5 O 4 F 7 , has a relative density of 97.0% or more, and has a Vickers hardness of 2.4 GPa or more; wherein the selected sintered body has a whiteness L* in a Lab color space of an external color of 65 or more. 2 . The method as claimed in claim 1 , wherein molding the molded body includes performing slip casting or uniaxial pressing. 3 . The method as claimed in claim 2 , wherein forming the composite sintered body includes performing pressureless sintering at 1,000° C. to 1,400° C. 4 . The method as claimed in claim 3 , further comprising processing the composite sintered body by performing hot isostatic pressing (HIP) after forming the composite sintered body to form a HIP composite sintered body, wherein selecting the sintered body includes selecting the sintered body from the HIP composite sintered body. 5 . The method as claimed in claim 4 , wherein a relative density of the composite sintered body before performing the HIP is 90% or more. 6 . The method as claimed in claim 4 , wherein, in the composite sintered body before performing the HIP: the relative density is 94% or more; and a whiteness L* in a Lab color space of an external color is 75 or more. 7 . The method as claimed in claim 1 , wherein: molding the molded body includes performing uniaxial pressing; and forming the composite sintered body includes performing a hot press at 1,000° C. to 1,400° C. 8 . The method as claimed in claim 7 , wherein the sintered body has a relative density of 99.0%. 9 . The method as claimed in claim 1 , wherein the sintered body includes 99 mass % or more of Y 5 O 4 F 7 . 10 . The method as claimed in claim 1 , wherein selecting the sintered body from the composite sintered body includes isolating the sintered body from the composite sintered body. 11 . The method as claimed in claim 1 , wherein the molded body further includes an adjuvant. 12 . The method as claimed in claim 11 , wherein the adjuvant includes a lanthanoid oxide, a lanthanoid fluoride, or a lanthanoid oxyfluoride.
wherein a ram exerts pressure on the material in a moulding space; Ram heads of special form · CPC title
L* (lightness axis) · CPC title
Other properties not specified above · CPC title
Setting, e.g. drying, dehydrating or firing ceramic articles (B28B11/242 takes precedence) · CPC title
Compositional purity · CPC title
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