Device for separating air by cryogenic distillation

Patent metadata

Field	Value
Publication number	US-12546533-B2
Application number	US-202118265027-A
Country	US
Kind code	B2
Filing date	Dec 2, 2021
Priority date	Dec 2, 2020
Publication date	Feb 10, 2026
Grant date	Feb 10, 2026

Abstract

A device for separating air by cryogenic distillation, comprising a first module containing a main air compressor, a second module, a third module containing a purification unit, a fourth module containing a heat exchanger and a system of columns comprising at least one distillation column that is or is not contained in the fifth module, the second module containing a connection for connecting the compressor of the first module to the purification unit of the third module in order to send compressed air from the compressor to the purification unit and also containing a connection for connecting the purification unit to the heat exchanger of the fourth module in order to send purified air in the purification unit to the heat exchanger.

First claim

The invention claimed is:

1 . A device for separating air by cryogenic distillation, the device comprising:
a first module configured to contain a main air compressor, a third module having a total length, a fourth module containing a purification unit, a fifth module configured to contain a heat exchanger, and a system of columns comprising at least one distillation column, wherein the fifth module is connected to said at least one distillation column of the system of columns by at least two fluid connections such that the device is configured to send the air to be separated to the heat exchanger and to the at least one distillation column of the system of columns, and to allow at least one fluid separated in the system of columns to be heated within the heat exchanger, wherein the third module is a horizontally oriented structural module arranged on the ground and configured to provide direct structural support from an upper surface of the third module to a lower surface of the fourth module, such that the fourth module is positioned directly on top of and supported by the upper surface of the third module, wherein the third module defines a central piping connection zone along the total length of the third module, said central piping connection zone having a length corresponding to between one-fifth and two-thirds of the total length of the third module, said central piping connection zone being distinct from end portions of the third module, wherein the first module is fluidically connected via piping to interfaces located within said central piping connection zone of the third module to supply compressed air to the interfaces, wherein the fifth module is fluidically connected via piping through a sidewall of the third module to interfaces located within said central piping connection zone of the third module to exchange process fluids therewith, and wherein said at least one of the first module and the fifth module so connected is located facing said central piping connection zone of the third module, and, wherein at least one of said end portions of the third module, located outside said central piping connection zone, houses at least one non-cryogenic operational component selected from the group consisting of: an electrical cabinet, an instrumentation cabinet, a control cabinet, an analysis device, a regeneration gas heater, and combinations thereof.

2 . The device as claimed in claim 1 , wherein the third module contains an element that is a heat exchanger that is configured to cool the air coming from the first module destined for the fourth module.

3 . The device as claimed in claim 1 , wherein the third module contains an element that is an electrical cabinet.

4 . The device as claimed in claim 1 , wherein the third module contains an element that is an instrumentation/monitoring and control cabinet.

5 . The device as claimed in claim 1 , wherein the third module contains an element that is an analysis device.

6 . The device as claimed in claim 1 , wherein the third module contains an element that is a heat exchanger for heating a residual gas coming from a column and/or from the fifth module destined for the purification unit of the fourth module.

7 . The device as claimed in claim 1 , wherein the third module contains an element that is a heat exchanger for cooling the air downstream of a compression stage of an air compressor.

8 . The device as claimed in claim 1 , wherein the third module contains an element that is an air cooling heat exchanger connected to a cooling water circuit and optionally to a cooling water pump.

9 . The device as claimed in claim 1 , wherein the length of the central piping connection zone is between one fifth and two thirds of the total length of the third module.

10 . The device as claimed in claim 9 , wherein an element selected from the group consisting of a first heat exchanger configured to cool air from the first module, an electrical cabinet, analysis device, a second heat exchanger configured to heat a residual gas coming from a column and/or from the fifth module, a third heat exchanger configured to cool air downstream of a compression stage of an air compressor, an air cooling heat exchanger connected to a cooling water circuit, and combinations thereof, is arranged in the third module but outside the central part.

11 . The device as claimed in claim 9 , wherein an element, which is selected from the group consisting of a first heat exchanger configured to cool air from the first module, an electrical cabinet, analysis device, a second heat exchanger configured to heat a residual gas coming from a column and/or from the fifth module, a third heat exchanger configured to cool air downstream of a compression stage of an air compressor, an air cooling heat exchanger connected to a cooling water circuit, and combinations thereof, is arranged in the third module but outside the central part at a first end of the third module and at least a second element, which is selected from the group consisting of the first heat exchanger configured to cool air from the first module, an electrical cabinet, analysis device, the second heat exchanger configured to heat the residual gas coming from the column and/or from the fifth module, the third heat exchanger configured to cool air downstream of the compression stage of an air compressor, an air cooling heat exchanger connected to the cooling water circuit, and combinations thereof, is arranged in the third module but outside the central part at the second end of the third module.

12 . The device as claimed in claim 1 , wherein the fourth module has a central part comprising between one fifth and two thirds of a total length of the fourth module, two adsorbent recipients being arranged on either side of the central part.

13 . The device as claimed in claim 1 , wherein the third and/or the fourth module has the dimensions of a standardized container in accordance with ISO 668 standards.

14 . The device as claimed in claim 1 , wherein for the third and/or fourth module, the ratio between the length of the module and its width is greater than three.

15 . The device as claimed in claim 1 , wherein for the third and/or fourth module, the ratio between the length of the module and its height is greater than three.

16 . The device as claimed in claim 1 , further comprising a second module containing a booster air compressor.

17 . The device as claimed in claim 1 , wherein the third module does not provide load-bearing support for any modules other than the fourth module.

18 . The device as claimed in claim 1 , wherein the third module has an inner volume in which both the central piping zone and the at least one non-cryogenic operational component are disposed.

19 . A device for separating air by cryogenic distillation, the device comprising:
a first module configured to contain a main air compressor; a third module having a total length; a fourth module containing a purification unit wherein the purification unit comprises a first adsorbent container and a second adsorbent container; a fifth module configured to contain a heat exchanger; and a system of columns comprising at least one distillation column, wherein the third module comprises fluid transport means that are configured to fluidly connect the other modules together, wherein the fifth module is connected to said at least one distillation column of the system of columns by at least two fluid connections such that the device is configured to send the air

Assignees

• Air Liquide

Inventors

• Davidian Benoit

Classifications

• F25J3/04339

  of air · CPC title

• F25J3/04157 Primary

  Afterstage cooling and so-called "pre-cooling" of the feed air upstream the air purification unit and main heat exchange line (F25J3/04618 takes precedence) · CPC title

• F25J3/04351

  of nitrogen · CPC title

• F25J3/044

  using a single pressure main column system only (F25J3/0446, F25J3/04624, F25J3/04636 take precedence) · CPC title

• F25J3/0489 Primary

  Modularity and arrangement of parts of the air fractionation unit, in particular of the cold box, e.g. pre-fabrication, assembling and erection, dimensions, horizontal layout "plot" (F25J3/04872 takes precedence) · CPC title