Powders and granules and process for making such powders and granules

US12545868B2 · US · B2

Patent metadata
FieldValue
Publication numberUS-12545868-B2
Application numberUS-202017786303-A
CountryUS
Kind codeB2
Filing dateDec 4, 2020
Priority dateDec 18, 2019
Publication dateFeb 10, 2026
Grant dateFeb 10, 2026

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  1. Title

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  2. Abstract

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  3. Assignees and inventors

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  4. Key dates

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  5. First independent claim

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  6. CPC / IPC classifications

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  7. Citations and related patents

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Abstract

Official abstract text for this publication.

The present invention is directed towards a process for making a powder or granule containing (A) at least one alkali metal salt of citric acid, and at least one additive selected from (B) at least one (co)polymer containing carboxylic acid groups, partially neutralized with alkali, in a weight ratio of (A):(B) of from 5:1 up to 100:1, wherein said powder or granule contains at least 75% by weight of citrate (A), said process comprising the steps of (a) mixing the at least one alkali metal salt of citric acid (A) and the at least one (co)polymer (B) in the presence of water, (b) removing most of said water by spray-drying or spray granulation using a gas with an inlet temperature of at least 125° C.

First claim

Opening claim text (preview).

The invention claimed is: 1 . A process for making a powder or granule containing (A) at least one alkali metal salt of citric acid, and at least one additive selected from (B) (co) polymer(s) comprising carboxylic acid groups, partially neutralized with alkali, in a weight ratio of (A):(B) of from 5:1 up to 100:1, wherein said powder or granule contains at least 75% by weight of citrate (A), referring to the solids content of said powder or granule, said process comprising the steps of (a) mixing the at least one alkali metal salt of citric acid (A) and the at least one (co) polymer (B) in the presence of water, and (b) removing most of said water by spray-drying or spray granulation using a gas with an inlet temperature of at least 125° C. 2 . The process according to claim 1 , wherein (A) is trisodium salt of citric acid. 3 . The process according to claim 1 , wherein (co)polymer (B) is selected from polyacrylic acid, random copolymers of acrylic acid with maleic anhydride or 2-acrylamido-2-methylpropanesulfonic acid, each (co) polymer being partially selected with alkali. 4 . The process according to claim 1 , wherein step (b) is performed with a two-fluid nozzle.

Assignees

Inventors

Classifications

  • Carboxylic acids or salts thereof · CPC title

  • Polycarboxylic acids-salts thereof · CPC title

  • Carboxylic acids-salts thereof · CPC title

  • Hard surfaces · CPC title

  • Preparation in the form of powder by spray drying · CPC title

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Frequently asked questions

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What does patent US12545868B2 cover?
The present invention is directed towards a process for making a powder or granule containing (A) at least one alkali metal salt of citric acid, and at least one additive selected from (B) at least one (co)polymer containing carboxylic acid groups, partially neutralized with alkali, in a weight ratio of (A):(B) of from 5:1 up to 100:1, wherein said powder or granule cont…
Who is the assignee on this patent?
Basf Se
What technology area does this patent fall under?
Primary CPC classification C11D3/2086. Mapped technology areas include Chemistry & Metallurgy.
When was this patent published?
Publication date Tue Feb 10 2026 00:00:00 GMT+0000 (Coordinated Universal Time) (B2). Legal status and post-grant events are not shown on this page.
What related patents are in patentsdb?
We list 8 related publications on this page (citations in our corpus or others sharing the same primary CPC).