Processes of Increasing Crystallinity Alignment of Protein Films and Products Thereof
US-2018105659-A1 · Apr 19, 2018 · US
US12545786B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-12545786-B2 |
| Application number | US-202017436475-A |
| Country | US |
| Kind code | B2 |
| Filing date | Mar 6, 2020 |
| Priority date | Mar 7, 2019 |
| Publication date | Feb 10, 2026 |
| Grant date | Feb 10, 2026 |
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The present invention relates to plant based materials, methods for their manufacture and biomaterials incorporating plant based materials.
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The invention claimed is: 1 . A thermoreversible process to obtain plant-based hydrogels comprising: a) forming a solution comprising one or more plant-based protein(s) in a solvent system, wherein the one or more plant-based protein(s) are selected from the group consisting of soybean, pea, rice, potato, wheat, or sorghum, and the solvent system comprises miscible co-solvents; wherein a first co-solvent increases solubility of the plant-based protein(s), and a second co-solvent decreases solubility of the plant based protein(s); and b) inducing the protein in the solution to undergo a sol-gel transition to form a plant-based protein hydrogel. 2 . The method according to claim 1 , further comprising: c) forming the plant-based protein hydrogel into a structured material selected from the group consisting of a film, a thin film, a micropatterned film, a micropatterned thin film, a microstructured thin film, a nanostructured thin film, a microgel, a microcapsule, a microbead, a bioscaffold, a bio-support, a sponge, a microscale-sponge, a hard capsule, or a functional coating. 3 . The method according to claim 1 , wherein the first co-solvent is an organic acid selected from the group consisting of acetic acid, glycolic acid, lactic acid, malic acid, citric acid and/or tartaric acid; and/or wherein a second or further co-solvent(s) is an aqueous buffer selected from the group consisting of water, ethanol, methanol, acetone, acetonitrile, dimethylsulfoxide, dimethylformamide, formamide, 2-propanol, 1-butanol, 1-propanol, hexanol, t-butanol, ethyl acetate or hexafluoroisopropanol. 4 . The method according to claim 1 , wherein solvent system comprises a ratio of the first co-solvent to the second co-solvent of about 20-80% v/v. 5 . The method according to claim 1 , further comprising mechanical shear of said protein solution comprising one or more plant-based protein(s) and a solvent system. 6 . The method of claim 1 , wherein the solvent system is thereafter removed such that the plant-based protein hydrogel no longer has thermoreversible properties. 7 . The method of claim 1 , wherein the solution is heated to a first temperature above the sol-gel temperature of the one or more plant-based protein(s), then reduced to a second temperature below the sol-gel temperature of the one or more plant-based protein(s).
Coating compositions based on proteins; Coating compositions based on derivatives thereof (foodstuff preparations A23J3/00) · CPC title
used for films · CPC title
used for foams · CPC title
for biomedical use · CPC title
Characterised by the use of proteins; Derivatives thereof · CPC title
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