Electrophoretic composition and method for preparing the same

Patent metadata

Field	Value
Publication number	US-12540408-B2
Application number	US-202217893719-A
Country	US
Kind code	B2
Filing date	Aug 23, 2022
Priority date	Aug 31, 2021
Publication date	Feb 3, 2026
Grant date	Feb 3, 2026

Abstract

The present disclosure relates to an electrophoretic composition and a method for preparing the same, and more particularly, to an electrophoretic composition which is applicable to a variable transmittance device which uses an electrophoretic method and a method for preparing the same. According to the exemplary embodiments of the present disclosure, an electrophoretic composition which minimizes the settling problem caused by the gravity and allows the electrophoretic particles to maintain the stably dispersed pattern in the solvent and a method for preparing the same may be provided.

First claim

What is claimed is:

1 . A method for preparing an electrophoretic composition, the method comprising:
mixing and circulating porous carbon particles and an acid; neutralizing with a base after cooling down; preparing the porous carbon particles having COOH group introduced on a surface by washing and drying; mixing and primarily dispersing the porous carbon particles having COOH group introduced on the surface, a dispersant including an NH group, and a solvent; forming a porous carbon particle-dispersant complex by heating the primarily dispersed mixture, wherein the NH group of the dispersant reacts with the COOH of the surface of the porous carbon particle and forms an amid bond so that at least a part may form the porous carbon particle-dispersant complex; obtaining the porous carbon particle-dispersant complex formed by removing an unreacted material; and controlling a concentration of the dispersant to allow the complex to form a micelle, wherein the base includes ammonia (NH 3 ), lithium acetate (CH 3 COOLi), sodium acetate, potassium acetate (CH 3 COOK), sodium hydrogen carbonate (NaHCO 3 ), potassium hydrogen carbonate (KHCO 3 ), sodium carbonate (Na 2 CO 3 ), potassium carbonate (K 2 CO 3 ), or a mixture thereof.

2 . The method for preparing an electrophoretic composition according to claim 1 , wherein a specific surface area of the porous carbon particle is 200 to 2000 m 2 /g.

3 . The method for preparing an electrophoretic composition according to claim 1 , wherein the acid is nitric acid (HNO 3 ), sulfuric acid (H 2 SO 4 ), hydrochloric acid (HCl), hydrobromic acid (HBr), hydroiodic acid (HI), perchloric acid (HClO 4 ), or mixtures thereof.

4 . The method for preparing an electrophoretic composition according to claim 1 , wherein the solvent is an isoparaffinic solvent having a specific gravity of 0.6 to 1.0.

5 . The method for preparing an electrophoretic composition according to claim 1 , wherein the dispersant including the NH group is polyisobutylene succinimide (PIBSI).

6 . The method for preparing an electrophoretic composition according to claim 1 , wherein the primary dispersion is performed 5 to 15 times at a pressure of 10000 to 25000 Psi.

7 . The method for preparing an electrophoretic composition according to claim 1 , wherein in the obtaining the porous carbon particle-dispersant complex formed by removing an unreacted material, a lower layer is collected by primary centrifugation and secondarily dispersed and then, an upper layer is collected by secondary centrifugation.

8 . The method for preparing an electrophoretic composition according to claim 7 , wherein 30 vol % or lower of the lower layer is collected from the entire primarily centrifuged solution.

9 . The method for preparing an electrophoretic composition according to claim 7 , wherein the secondary dispersion is performed 1 to 5 times at a pressure of 10000 to 25000 Psi.

10 . The method for preparing an electrophoretic composition according to claim 7 , wherein 70 vol % or lower of the upper layer is collected from the entire secondarily centrifuged solution.

11 . The method for preparing an electrophoretic composition according to claim 1 , wherein in the controlling a concentration of the dispersant to allow the complex to form a micelle, the dispersant is added to control a concentration such that a weight ratio of the porous carbon particle and the dispersant becomes 1:2 to 7.

Assignees

• Lg Display Co Ltd
• Nano Solution Co Ltd

Inventors

• Lee Sujeong
• Kim Sunghee
• Kim Hyungyul
• Moon Hojun

Classifications

• C08K2201/006

  Additives being defined by their surface area · CPC title

• C25B15/083

  Separating products · CPC title

• C09D5/4407

  with polymers obtained by polymerisation reactions involving only carbon-to-carbon unsaturated bonds · CPC title

• C08K3/04

  Carbon · CPC title

• C25B7/00 Primary

  Electrophoretic production of compounds or non-metals (separation or purification of peptides, e.g. of proteins, by electrophoresis C07K1/26) · CPC title