Powder milling

Patent metadata

Field	Value
Publication number	US-12539519-B2
Application number	US-202318122833-A
Country	US
Kind code	B2
Filing date	Mar 17, 2023
Priority date	Mar 17, 2022
Publication date	Feb 3, 2026
Grant date	Feb 3, 2026

Abstract

A method can include milling a powder with a test grinding media, and determining an amount of abraded grinding media that abrades from the test grinding media into the powder due to the milling of the powder. The method can include creating a compensated powder to account for the amount of the abraded grinding media such that the powder milling process results in a desired powder composition.

First claim

What is claimed is:

1 . A method, comprising:
milling a powder with a test grinding media; determining an amount of abraded grinding media that abrades from the test grinding media into the powder due to the milling of the powder; and creating a compensated powder to account for the amount of the abraded grinding media such that the powder milling process results in a powder composition.

2 . The method of claim 1 , further comprising milling the compensated powder with a similar grinding media to the test grinding media to result in the powder composition including the abraded grinding media.

3 . The method of claim 2 , wherein determining the amount of the abraded grinding media includes:
detecting an amount of a detectable tracer material integrated within a bulk material of the test grinding media; and correlating the amount tracer material to the amount of the abraded grinding media.

4 . The method of claim 3 , wherein correlating the amount of the abraded grinding media includes correlating the amount of tracer material to a thickness of the test grinding media.

5 . The method of claim 4 , wherein correlating the amount of tracer material to a thickness includes using a diffusion profile.

6 . The method of claim 2 , further comprising creating the test grinding media to include the detectable tracer material.

7 . The method of claim 6 , wherein creating the test grinding media includes diffusing the detectable tracer material into a bulk material of the test grinding media.

8 . The method of claim 7 , wherein a bulk material of the similar grinding media is made only of one or more constituent materials of the desired powder composition.

9 . The method of claim 8 , wherein the bulk material of the similar grinding media is the same as the bulk material of the test grinding media.

10 . The method of claim 9 , wherein the similar grinding media does not include a tracer material.

11 . The method of claim 10 , wherein the test grinding media and/or the similar grinding media includes one or more grinding balls.

12 . A method, comprising:
forming one or more test grinding media to include:
a bulk material; and
a detectable tracer material integrated with the bulk material and configured to allow for correlation between an amount of a tracer material that is in a milled powder to an abraded amount of grinding media from the grinding media.

13 . The method of claim 12 , further comprising diffusing the tracer material into a bulk material to form a diffusion profile that is a function of depth.

14 . The method of claim 13 , further comprising providing diffusion profile information to a user to correlate the amount of the tracer material to the amount of abraded grinding media.

15 . The method of claim 12 , further comprising forming the grinding media to have a constant amount of tracer material integrated within the bulk material.

16 . A test grinding media, comprising:
a bulk material; and a detectable tracer material integrated with the bulk material and configured to allow for correlation between an amount of a tracer material that is in a milled powder to an abraded amount of grinding media from the grinding media.

17 . The media of claim 16 , wherein the test grinding media is formed as one or more balls.

18 . The media of claim 16 , wherein the tracer material is not radioactive, and wherein the bulk material is alumina.

Assignees

• Univ Central Florida Res Found Inc

Inventors

• Gaume Romain
• Julian Matthew

Classifications

• B02C17/20

  Disintegrating members · CPC title

• B02C17/1805 Primary

  Monitoring devices for tumbling mills · CPC title