Flow reactor

Patent metadata

Field	Value
Publication number	US-12533651-B2
Application number	US-201917782556-A
Country	US
Kind code	B2
Filing date	Dec 20, 2019
Priority date	Dec 20, 2019
Publication date	Jan 27, 2026
Grant date	Jan 27, 2026

Abstract

A flow reactor can promote a reaction under appropriate temperature management, can precent reaction fluid or generated gas from being trapped in a heat transmission part, can be disassembled for easy cleaning, and to which a coating or lining can be applied. This flow reactor is provided with two flow paths, a reaction flow path and a second flow path, in a space formed between an inner cylinder and an outer cylinder that are concentric. A spiral heat transmission body is disposed between the inner cylinder and the outer cylinder, and the spiral heat transmission body has a substantially triangular cross-sectional shape in an axial cross-sectional view. The spiral heat transmission body partitions the space into the reaction flow path and the second flow path, and heat is exchanged via the spiral heat transmission body between a reaction fluid F 1 flowing through the reaction flow path and a heat medium F 2 flowing through the second flow path.

First claim

The invention claimed is:

1 . A flow reactor comprising a reaction flow path, the reaction flow path being circulated spirally to flow a fluid to be reacted, wherein
a heat transfer body is arranged in a space formed between an inner tube and an outer tube that are arranged concentrically, and at least any one of the inner tube and the outer tube is a cylinder having a circular shape in an axial-direction cross sectional-view, wherein the heat transfer body is spirally circulated and has a cross sectional shape of a substantially triangle in an axial-direction cross sectional-view, the space is partitioned into the reaction flow path and a second flow path by the heat transfer body, and a heat exchange is performed between the fluid to be reacted flowing in the reaction flow path and a heat medium flowing in the second flow path via the heat transfer body, and a ratio (λ/μ) of a maximum flow path width (λ) of the reaction flow path to a minimum flow path width (μ) of the reaction flow path in a radius direction is 2 or more (2≤λ/μ<∞).

2 . The flow reactor according to claim 1 , wherein the reaction flow path is not provided with a horizontal portion capable of accumulating the fluid to be reacted.

3 . The flow reactor according to claim 1 , wherein the reaction flow path and the second flow path are spirally circulated, respectively, and a gap is not formed between circulations adjacent to each other in an axial direction, or a gap of 4 mm or less is formed in a radial direction.

4 . The flow reactor according to claim 1 , wherein
cross sectional shapes of the reaction flow path and the second flow path in an axial-direction cross-sectional view is a substantially triangle whose apex angle θ is in the range of 30 degrees or more to 125 degrees or less.

5 . The flow reactor according to claim 1 , wherein
the side of the inner tube and the side of the outer tube are assembled so as to be separatable only by moving in an axial direction without rotating, and the heat transfer body is configurated so as not to interfere with other portion upon moving in the axial direction.

6 . The flow reactor according to claim 1 , wherein
cross sectional shapes of the reaction flow path and the second flow path in an axial-direction cross-sectional view is a substantially triangle having two slopes, a bottom surface, and a peak portion; and an axial-direction length (a) of the peak portion is shorter than an axial-direction length (b) of the slopes.

7 . The flow reactor according to claim 6 , wherein
the peak portion of at least any one of the reaction flow path and the second flow path has the axial-direction length (a) so that a cross-section area of the flow path is increased as compared with the case where the peak portion is the apex having no axial-direction length (a).

8 . The flow reactor according to claim 1 , wherein
a plurality of spaces is concentrically formed between the inner tube and the outer tube that are concentrically arranged.

9 . The flow reactor according to claim 1 , wherein
at least any one of a passing flow path through which the reaction fluid flows, including the reaction flow path, and a passing flow path through which the heat medium flows, including the second flow path, is coated with a corrosion resistant material.

10 . The flow reactor according to claim 9 , wherein
the coating with the corrosion resistant material is one of a glass lining, a fluorine resin coating, and a ceramic coating.

11 . The flow reactor according to claim 2 , wherein the reaction flow path and the second flow path are spirally circulated, respectively, and a gap is not formed between circulations adjacent to each other in an axial direction, or a gap of 4 mm or less is formed in a radial direction.

12 . The flow reactor according to claim 2 , wherein
cross sectional shapes of the reaction flow path and the second flow path in an axial-direction cross-sectional view is a substantially triangle whose apex angle θ is in the range of 30 degrees or more to 125 degrees or less.

13 . A flow reactor comprising a reaction flow path, the reaction flow path being circulated spirally to flow a fluid to be reacted, wherein
a heat transfer body that is spirally circulated is arranged in a space formed between an inner tube and an outer tube that are arranged concentrically, and the flow reactor is configured such that the space is partitioned into the reaction flow path and a second flow path by the heat transfer body, and that a heat exchange is performed between the fluid to be reacted flowing in the reaction flow path and a heat medium flowing in the second flow path via the heat transfer body, wherein the inner tube, the outer tube, and the heat transfer body are assembled so as to be separable into a side of the outer tube and a side of the inner tube, in the state of being separated into the side of the outer tube and the side of the inner tube, a flow path constitution surface that defines the reaction flow path is separated into the side of the outer tube and the side of the inner tube, and whole surfaces of the flow path constitution surfaces that define the reaction flow path are configured so as to be directly exposed without being hidden by any other portion when viewed from a radius direction perpendicular to an axial direction, wherein the reaction flow path is a path which spirally circulates, and a ratio (λ/μ) of a maximum flow path width (λ) of the reaction flow path to a minimum flow path width (μ) of the reaction flow path in a radius direction is 2 or more (2≤λ/μ<∞).

14 . The flow reactor according to claim 13 , wherein
the heat transfer body is fixed to any one side of the outer tube and the inner tube and is not fixed to other side of the outer tube and the inner tube, the heat transfer body is provided with a sterically shaped portion that has at least one bending portion and can form a space through which the fluids flow in both an inner surface side and an outer surface side thereof, wherein an exterior angle of all bending portions appearing on the flow path constitution surface that defines the reaction flow path is 90 degrees or greater.

15 . The flow reactor according to claim 13 , wherein the reaction flow path is not provided with a horizontal portion capable of accumulating the fluid to be reacted.

16 . The flow reactor according to claim 14 , wherein the reaction flow path is not provided with a horizontal portion capable of accumulating the fluid to be reacted.

17 . The flow reactor according to claim 13 , wherein the reaction flow path and the second flow path are spirally circulated, respectively, and a gap is not formed between circulations adjacent to each other in an axial direction, or a gap of 4 mm or less is formed in a radial direction.

18 . The flow reactor according to claim 14 , wherein the reaction flow path and the second flow path are spirally circulated, respectively, and a gap is not formed between circulations adjacent to each other in an axial direction, or a gap of 4 mm or less is formed in a radial direction.

19 . The flow reactor according to claim 13 , wherein
cross sectional shapes of the reaction flow path and the second flow path in an axial-direction cross-sectional view is a substantially triangle whose apex angle θ is in the range of 30 degrees or more to 125 degrees or less.

20 . The flow reactor according to claim 14 , wherein
cross sectional shapes of the reaction flow path and the second flow path in an axia

Assignees

• M Technique Co Ltd

Inventors

• Enomura Masakazu

Classifications

• B01J2219/0245

  of synthetic organic material · CPC title

• B01J2219/0218

  of ceramic · CPC title

• B01J2219/0209

  of glass · CPC title

• B01J2219/00081

  Tubes · CPC title

• B01J19/0013

  Controlling the temperature of the process · CPC title