Soft magnetic material powder and manufacturing method thereof, and magnetic core and manufacturing method thereof
US-2021054218-A1 · Feb 25, 2021 · US
US12505941B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-12505941-B2 |
| Application number | US-202318128273-A |
| Country | US |
| Kind code | B2 |
| Filing date | Mar 30, 2023 |
| Priority date | Mar 31, 2022 |
| Publication date | Dec 23, 2025 |
| Grant date | Dec 23, 2025 |
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A dust core including soft magnetic metal particles and a grain boundary phase, wherein the grain boundary phase includes Si and Ti.
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What is claimed is: 1 . A dust core comprising soft magnetic metal particles and a grain boundary phase, wherein the grain boundary phase includes Si and Ti, at least one soft magnetic metal particle of the soft magnetic metal particles comprises a core particle and an insulation layer formed on a surface of the core particle, a layer other than the insulation layer exists between the insulation layer and the surface of the core particle, a content of Ti in the grain boundary phase is higher than that in the insulation layer, the layer other than the insulation layer includes a phosphoric acid compound, an amount ratio of Ti in the grain boundary phase is within a range of 100 ppm or more and 3000 ppm or less by mass with respect to a total weight of the dust core, and an initial permeability μi of the dust core is 50.0 or more. 2 . The dust core according to claim 1 , wherein at least one soft magnetic metal particle of the soft magnetic metal particles includes Fe. 3 . The dust core according to claim 1 , wherein the insulation layer includes an oxide of Si. 4 . The dust core according to claim 1 , wherein an amount of the soft magnetic metal particles in the dust core is within a range of 90 wt % to 99.9 wt %. 5 . The dust core according to claim 1 , wherein a thickness of the insulation layer is in a range of 5 nm or more and 500 nm or less. 6 . The dust core according to claim 1 , wherein the layer other than the insulation layer has a thickness of 20 nm or less. 7 . The dust core according to claim 1 , wherein the grain boundary phase further includes a resin including Si, and Ti is mixed with the resin including Si. 8 . The dust core according to claim 7 , wherein the resin including Si is a methyl-based silicone resin. 9 . The dust core according to claim 7 , wherein the grain boundary phase further includes an epoxy resin, an imide resin, Si—O-based oxides, Ca—O-based oxides, Ba—O-based oxides, and/or Bi—O-based oxides. 10 . The dust core according to claim 1 , wherein the insulation layer includes Ti and an oxide of Si. 11 . The dust core according to claim 10 , wherein the insulation layer further includes at least one element selected from the group consisting of Ba, Ca, Mg, Al, Zr, Ni, Mn, and Zn, and a total amount ratio of the at least one element is 1 mol % or less with respect to a total amount of Ti in the insulation layer. 12 . The dust core according to claim 10 , wherein the oxide of Si is SiO 2 or a composite oxide which includes Si. 13 . The dust core according to claim 1 , wherein the core particle includes Fe. 14 . The dust core according to claim 13 , wherein the core particle further includes Si, Ni, or Co. 15 . A magnetic component including the dust core according to claim 1 . 16 . A dust core comprising soft magnetic metal particles and a grain boundary phase, wherein the grain boundary phase includes Si and Ti, at least one soft magnetic metal particle of the soft magnetic metal particles comprises a core particle and an insulation layer formed on a surface of the core particle, the insulation layer includes Ti and an oxide of Si, the insulation layer includes a simple substance of Ti and/or an organometallic compound including Ti, a content of Ti in the grain boundary phase is higher than that in the insulation layer, an amount ratio of Ti in the grain boundary phase is within a range of 100 ppm or more and 3000 ppm or less by mass with respect to a total weight of the dust core, and an initial permeability μi of the dust core is 50.0 or more. 17 . The dust core according to claim 16 , wherein at least one soft magnetic metal particle of the soft magnetic metal particles includes Fe. 18 . A magnetic component including the dust core according to claim 16 . 19 . A dust core comprising soft magnetic metal particles and a grain boundary phase, wherein the grain boundary phase includes Si and Ti, at least one soft magnetic metal particle of the soft magnetic metal particles comprises a core particle and an insulation layer formed on a surface of the core particle, the insulation layer includes Ti and an oxide of Si, the insulation layer includes a simple substance of Ti and/or an organometallic compound including Ti, the average value of Ti/(Si+Ti) in the insulation layer of all soft magnetic metal particles contained in the soft magnetic metal particles in the dust core is 1.3 mol % or higher, a content of Ti in the grain boundary phase is higher than that in the insulation layer, and an amount ratio of Ti in the grain boundary phase is within a range of 100 ppm or more and 3000 ppm or less by mass with respect to a total weight of the dust core. 20 . A magnetic component including the dust core according to claim 19 .
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