Method for determining a chemical intake capacity of a process medium in a measuring point and measuring point for determining a chemical intake capacity of a process medium

Patent metadata

Field	Value
Publication number	US-12487222-B2
Application number	US-202016942439-A
Country	US
Kind code	B2
Filing date	Jul 29, 2020
Priority date	Jul 29, 2019
Publication date	Dec 2, 2025
Grant date	Dec 2, 2025

Abstract

A method for determining a chemical intake capacity of a process medium includes steps of providing a measuring point and an analytical measuring device, closing an outlet valve to the drain so that no process medium is discharged and closing the inlet valve so that no additional process medium is fed from the first inlet. The method includes circulating the analyte and process medium through the pump so the mixture flows into the analytical measuring device at a predetermined flow velocity. Further, the method includes detecting a measured value using the analytical measuring device until the measured value exceeds a limit value. The predetermined volumes are summed to form a total volume of the analyte, and a chemical intake capacity of the predetermined medium is determined based on the total volume of the analyte fed in.

First claim

The invention claimed is:

1 . A method for determining a chemical intake capacity of a process medium relative to an analyte in a measuring point, wherein the method comprises at least the following steps:
providing the measuring point through which the process medium flows and an analytical measuring device, wherein the measuring point has an inlet valve, an outlet valve, an analysis container, a dosing container and a pump,
wherein the inlet valve is connected to a first inlet, a second inlet, the analysis container and the dosing container, wherein the first inlet is configured to feed in the process medium, wherein the second inlet is configured to feed in the analyte,
wherein the outlet valve is connected to a drain, the analysis container and the dosing container,
wherein the inlet valve, the analysis container, the dosing container and the outlet valve are connected to one another in such a way that a flow circuit can be realized in the measuring point,
wherein the pump is arranged in such a way that it is suitable for generating the flow circuit,
wherein the analytical measuring device is arranged in the analysis container and is in contact with the process medium,
closing the outlet valve, so that no process medium is discharged through the outlet valve to the drain, closing the inlet valve so that no additional process medium is fed from the first inlet into the measuring point and a predetermined volume of process medium is located in the measuring point, measuring a first measured value of a first measurand of the process medium using the analytical measuring device,
feeding a predetermined volume of the analyte into the measuring point through the inlet valve from the second inlet,
circulating the analyte and the process medium through the pump, so that the flow circuit is generated and an analyte process medium mixture flows into the analytical measuring device,
wherein a predetermined flow velocity of the analyte process medium mixture is set by the pump,
measuring a second measured value of a second measurand of the analyte process medium mixture using the analytical measuring device,
comparing the first measured value of the first measurand with the second measured value of the second measurand,
repeating the steps of feeding, circulating, measuring and comparing while the second measured value of the second measurand does not exceed the first measured value of the first measurand and until the second measured value of the second measurand is equal to or exceeds the first measured value of the first measurand;
summing the fed-in predetermined volumes to form a total volume of the analyte fed into the measuring point; and
determining the chemical intake capacity of the process medium based on the total volume of the analyte fed into the measuring point.

2 . The method according to claim 1 , wherein the first measured value and the second measured value are a disinfectant content and the analytical measuring device is a disinfection sensor.

3 . The method according to claim 1 , wherein the first measured value of the first measurand and the second measured value of the second measurand are a depletion rate of a disinfectant.

4 . The method according to claim 3 , wherein there is a time interval between the measurement of the first measured value of the first measurand and the second measured value of the second measurand of less than 10 minutes.

5 . The method according to claim 4 , wherein the steps of feeding, circulating and measuring the first measured value of the first measurand occur during a time interval of less than one minute.

6 . A measuring point for determining a chemical intake capacity of a process medium, wherein the chemical intake capacity of the process medium is determined according to claim 1 , comprising:
an inlet valve, an outlet valve, an analysis container, a dosing container and a pump with a regulatable delivery rate, wherein the inlet valve is connected to a first inlet, a second inlet, the analysis container and the dosing container, wherein the inlet valve is configured to feed in the process medium, wherein the second inlet is configured to feed in an analyte, wherein the outlet valve is connected to a drain, the analysis container and the dosing container, wherein the inlet valve, the analysis container, the dosing container and the outlet valve are connected to one another in such a way that a flow circuit can be realized in the measuring point, wherein the pump is arranged in such a way that it is suitable for generating the flow circuit, wherein an analytical measuring device is arranged in the analysis container in such a way that the flow circuit provides flow of an analyte process medium mixture to the analytical measuring device; wherein the measuring point is configured to repeat steps of feeding, circulating, measuring and comparing while the a second measured value of a second measurand does not exceed a first measured value of a first measurand and until the second measured value of the second measurand is equal to or exceeds the first measured value of the first measurand wherein the measuring point further comprises a bypass channel which connects the first inlet and the drain in order to guide a part of the process medium from the first inlet past the analysis container and the dosing container to the drain, wherein a first turbine of the pump is arranged in the bypass channel and a second turbine of the pump is arranged in the flow circuit, wherein the first turbine is suitable for driving the second turbine.

7 . The measuring point according to claim 6 , wherein the inlet valve is configured as a multi-way valve.

8 . The measuring point according to claim 7 , wherein the analytical measuring device is an electrochemical chlorine sensor, electrochemical chlorine dioxide sensor, bromine sensor, a pH sensor, a conductivity sensor or a dissolved oxygen sensor.

9 . A method for determining a chemical intake capacity of a process medium relative to an analyte in a measuring point, wherein the method comprises at least the following steps:
providing the measuring point through which the process medium flows and an analytical measuring device, wherein the measuring point has an inlet valve, an outlet valve, an analysis container, a dosing container and a pump,
wherein the inlet valve is connected to a first inlet, a second inlet, the analysis container and the dosing container, wherein the first inlet is configured to feed in the process medium, wherein the second inlet is configured to feed in the analyte,
wherein the outlet valve is connected to a drain, the analysis container and the dosing container,
wherein the inlet valve, the analysis container, the dosing container and the outlet valve are connected to one another in such a way that a flow circuit can be realized in the measuring point,
wherein the pump is arranged in such a way that it is suitable for generating the flow circuit,
wherein the analytical measuring device is arranged in the analysis container and is in contact with the process medium,
closing the outlet valve, so that no process medium is discharged through the outlet valve to the drain, closing the inlet valve so that no additional process medium is fed from the first inlet into the measuring point and a predetermined volume of process medium is located in the measuring point, measuring a first measured value of a first measurand of the process medium using the analytical measuring device,
feeding a predetermined volume of the analyte into the measuring point through the inlet valve from the second inlet,
circulating the analyte and the process medium through the pump, so that the flow circuit is gen

Assignees

• Endress Hauser Conducta Gmbh Co Kg

Inventors

• Hanko Michael
• Hennings Erik

Classifications

• G01N33/182

  Specific anions in water · CPC title

• G01N1/2035

  by deviating part of a fluid stream, e.g. by drawing-off or tapping · CPC title

• G01N2001/205

  using a valve · CPC title

• G01N33/1813

  Specific cations in water, e.g. heavy metals · CPC title

• G01N33/1893 Primary

  using flow cells · CPC title