Method for increasing amount of water absorbed under load by water absorbent resin particles, and method for producing water absorbent resin particles

Patent metadata

Field	Value
Publication number	US-12478952-B2
Application number	US-202017597324-A
Country	US
Kind code	B2
Filing date	Jul 1, 2020
Priority date	Jul 5, 2019
Publication date	Nov 25, 2025
Grant date	Nov 25, 2025

Abstract

Disclosed is a method for improving a water absorption amount under load by water absorbent resin particles, the method including shaking a powder containing a plurality of water absorbent resin particles contained in a container. An amount of powder corresponding to a theoretical filling rate of less than 100% may be contained in the container.

First claim

The invention claimed is:

1 . A method for improving water absorbent resin particles, the method comprising:
filling a container with a powder containing a plurality of water absorbent resin particles, an amount of the powder contained in the container corresponding to a theoretical filling rate of 90% or less, wherein the theoretical filling rate is a value calculated by the following equation:
Theoretical filling rate [%]={( X [g]/ D [g/mL])/ V [mL]}×100,

where X represents a mass of the powder, D represents a tapped bulk density of the powder, and V represents a maximum capacity of the container; and
shaking the container filled with the powder so as to improve a water absorption under load of the water absorbent resin particles from a first water absorption amount under load to a second water absorption amount under load, a maximum value of an acceleration received by the powder during shaking being 0.050 to 4.0 G, the water absorbent resin particles prior to the shaking having the first water absorption amount under load, and the water absorbent resin particles after the shaking having the second water absorption amount under load that is at least 103% of the first water absorption amount.

2 . The method according to claim 1 ,
wherein a time for shaking the powder contained in the container is 10 minutes or longer in total.

3 . The method according to claim 1 , wherein the maximum value of the acceleration received by the powder during shaking is 0.050 to 2.5 G.

4 . The method according to claim 1 , wherein the amount of the powder contained in the container corresponds to a theoretical filling rate of 65% or more.

5 . A method for producing water absorbent resin particles, the method comprising:
obtaining water absorbent resin particles comprising a polymer having an ethylenically unsaturated monomer as a monomer unit by polymerizing a monomer comprising the ethylenically unsaturated monomer, and improving a water absorption amount under load of the water absorbent resin particles by treating the water absorbent resin particles with the method according to claim 1 .

Assignees

• Sumitomo Seika Chemicals

Inventors

• NISHIDA Moe

Classifications

• B01J20/28016

  Particle form · CPC title

• B01J20/267 Primary

  Cross-linked polymers · CPC title

• B01J20/261

  obtained by reactions only involving carbon to carbon unsaturated bonds (macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds per se C08F) · CPC title

• C08J3/12 Primary

  Powdering or granulating · CPC title

• B01J20/26

  Synthetic macromolecular compounds · CPC title