Probe, a system and a method for analysis of a liquid in a mixture of the liquid and solid substance

Patent metadata

Field	Value
Publication number	US-12474265-B2
Application number	US-202318224135-A
Country	US
Kind code	B2
Filing date	Jul 20, 2023
Priority date	Jul 28, 2022
Publication date	Nov 18, 2025
Grant date	Nov 18, 2025

Abstract

According to an aspect of the present inventive concept there is provided a probe for analysis of a liquid in a mixture of the liquid and solid substance. The probe comprises: a tube comprising a sample end configured to be inserted into the mixture; a cap configured to come into contact with the mixture at the sample end, the cap comprising one or more openings configured for allowing passage of the liquid therethrough, and for preventing passage of the solid substance therethrough; and an optical measurement head arranged in the tube and configured to come into contact with the liquid having passed the one or more openings, wherein the optical measurement head is configured to collect measurement information for analysis of the liquid.

First claim

The invention claimed is:

1 . A probe for analysis of a liquid in a mixture of the liquid and solid substance, the probe comprising:
a tube comprising a sample end configured to be inserted into the mixture; a cap configured to come into contact with the mixture at the sample end, the cap comprising one or more openings configured for allowing passage of the liquid therethrough, and for preventing passage of the solid substance therethrough; and an optical measurement head arranged in the tube and configured to come into contact with the liquid having passed the one or more openings, wherein the optical measurement head is configured to collect measurement information for analysis of the liquid.

2 . The probe according to claim 1 , wherein the optical measurement head comprises an optical fiber comprising a fiber end, the fiber end being arranged to come into contact with the liquid having passed the one or more openings.

3 . The probe according to claim 2 , wherein the optical fiber is further configured to guide light through the fiber to the fiber end, to emit the light through the fiber end into the liquid, and to guide reflected light through the fiber away from the fiber end, wherein the reflected light is light reflected at the interface between the fiber end and the liquid.

4 . The probe according to claim 3 , wherein an inner portion of the cap has a shape for preventing light emitted through the fiber end from being reflected back from the inner portion of the cap towards the fiber end.

5 . The probe according to claim 3 , wherein an inner portion of the cap comprises a coating of a light absorbing material, for preventing light emitted through the fiber end from being reflected back from the inner portion of the cap towards the fiber end.

6 . The probe according to claim 3 , wherein the optical fiber is arranged in the tube with respect to the cap such that the light emitted through the fiber end does not impinge on the one or more openings of the cap.

7 . The probe according to claim 6 , wherein the cap further comprises:
a first portion arranged proximal to the fiber end, the first portion comprising all the one or more openings; and a second portion arranged distal to the fiber end, wherein the fiber end is further configured to emit the light as a light cone, such that the full light cone impinges on inner walls of the second portion.

8 . The probe according to claim 1 , further comprising an exhaust hole configured to allow air from inside the cap to pass therethrough, as the air is pushed out of the cap by the liquid passing through the one or more openings into the cap.

9 . The probe according to claim 2 , wherein the probe is configured for determining an index of refraction of the liquid.

10 . The probe according to claim 1 , wherein the tube has an outer diameter of 1.2 mm or less.

11 . The probe according to claim 1 , wherein each opening of the one or more openings has a diameter in the interval 0.45 μm to 1 mm, such as in the interval 10 μm to 1 mm.

12 . The probe according to claim 1 , wherein the probe is configured for determining a sugar content in the liquid.

13 . The probe according to claim 1 , wherein the cap has a pointed shape, thereby facilitating penetrating the solid substance.

14 . A system for analysis of a liquid in a mixture of the liquid and solid substance, the system comprising:
a probe according to claim 1 ; a light source configured to emit light; and a detector comprising a light sensitive element configured to generate an electric signal dependent on an intensity of light incident onto the light sensitive element.

15 . A method of performing analysis of a liquid in a mixture of the liquid and solid substance, the method comprising:
inserting a sample end of a tube into the mixture; causing a cap to come into contact with the mixture at the sample end; allowing the liquid to pass through one or more openings of the cap, preventing passage of the solid substance through the one or more openings of the cap; causing an optical measurement head, arranged in the tube, to come into contact with the liquid having passed the one or more openings; and collecting, by the optical measurement head, measurement information for analysis of the liquid.

Assignees

• Stichting Imec Nederland

Inventors

• Zentile Mark
• Zhang Xu
• Offermans Peter
• Young David
• Tibbe Arjan

Classifications

• G01N2201/08

  Optical fibres; light guides · CPC title

• G01N1/12

  Dippers; Dredgers · CPC title

• G01N33/025

  Fruits or vegetables · CPC title

• G01N21/4133 Primary

  Refractometers, e.g. differential · CPC title

• G01N2021/8571

  using filtering of sample fluid · CPC title