Process for preparing powders by spray drying and powders obtainable thereby

Patent metadata

Field	Value
Publication number	US-12446606-B2
Application number	US-202218291942-A
Country	US
Kind code	B2
Filing date	Jul 28, 2022
Priority date	Jul 28, 2021
Publication date	Oct 21, 2025
Grant date	Oct 21, 2025

Abstract

The present invention relates to a use of octenylsuccinyl anhydride substituted starch (OSA starch) for increasing the dry weight content and/or the fat content of a liquid composition that is subjected to a spray-drying step, and also to a process for preparing powders. The present invention enables the spray-drying of emulsions that contain a high amount of fat. The present invention also relates to the powder products obtainable by the process and nutritional products such as an infant milk powder, grow up milk, toddler milk or as a medical nutritional product that can be formulated therewith.

First claim

The invention claimed is:

1 . A method for producing a nutritional powder, comprising fat, an emulsifier, digestible carbohydrates, and proteinaceous material comprising the steps of
a. preparing a liquid containing the digestible carbohydrate and the emulsifier in water by adding the digestible carbohydrate and the emulsifier consecutively or simultaneously to water at a temperature of between 50 and 90 deg C., optionally using a homogenization step; b. providing a fat ingredient containing at least one fat; c. combining the liquid and the fat ingredient to provide a pre-emulsion; d. performing a homogenization step to homogenize the pre-emulsion to form an emulsion, and optionally increasing the dry matter content of the emulsion by a concentration step; e. spray drying the emulsion obtained in step d to provide a base powder; f. optionally further drying the base powder of step e;
wherein the emulsifier is octenylsuccinyl anhydride substituted starch (OSA starch),
wherein the fat content of the base powder is at least 32 wt % on total dry weight of the base powder, wherein the free fat content is less than 3 wt % based on total weight of the fat,
g. adding one or more dry ingredients by dry blending, to obtain the nutritional powder,

wherein the nutritional powder is an infant formula, follow-on formula or growing-up milk,
wherein the nutritional powder comprises 40-60 wt. % of the base powder,
wherein the nutritional powder contains 95-100 wt. % amino acids based on total proteinaceous material.

2 . The method of claim 1 , wherein the fat content of the base powder is 35 to 70 wt % on total dry weight of the base powder.

3 . The method according to claim 2 , wherein the fat content of the base powder is 40 to 60 wt % on total dry weight of the base powder.

4 . The method of claim 1 , wherein the pre-emulsion additionally contains at least one further component.

5 . The method according to claim 4 , wherein the at least one further component is a vitamin, mineral or protein.

6 . The method according to claim 1 , wherein the OSA starch is derived from waxy maize starch, tapioca starch, rice starch, potato starch, wheat starch, starch from other plant origin substituted with octenylsuccinic acid groups.

7 . The method according to claim 1 , wherein the further dry ingredients of step (g) contain at least one of a digestible carbohydrate, a digestible protein, a hydrolysed protein, a peptide, an amino acid, a biotic, a non-digestible carbohydrate or fibre, a vitamin, mineral or a mixture of two or more of these.

8 . The method according to claim 1 , wherein the weight ratio of the digestible carbohydrate to the emulsifier in the liquid composition of step (a) is in the range of 15/1-1/3.

9 . The method according to claim 8 , wherein the weight ratio of the digestible carbohydrate to the emulsifier in the liquid composition of step (a) is in the range of 10/1 to 1/1.

10 . The method according to claim 9 , wherein the weight ratio of the digestible carbohydrate to the emulsifier in the liquid composition of step (a) is in the range of 6/1 to 4/1.

11 . The method according to claim 1 , wherein the nutritional powder further comprises dietary fibres which are added during the dry-blending of step (g).

12 . The method according to claim 1 , wherein the amino acids are added to the pre-emulsion or the emulsion prior to step (e) or the amino acids are blended with the base powder in step (g).

13 . A nutritional powder comprising
40-60 wt % of base powder, wherein the base powder comprises fat, digestible carbohydrates and emulsifier, wherein the fat content is at least 32 wt % based on total dry weight of the base powder, the free fat content is less than 3 wt % based on total weight of the fat, and the emulsifier is OSA starch; and one or more ingredients selected from the group consisting of a digestible carbohydrate, a protein, hydrolysed protein, peptide, amino acid, a non-digestible carbohydrate, biotic, vitamin and mineral,
wherein the nutritional powder is an infant formula, follow-on formula or growing-up milk,
wherein the nutritional powder comprises fat, an emulsifier, digestible carbohydrates, and proteinaceous material and contains 95-100 wt. % free amino acids based on total proteinaceous material.

14 . The nutritional powder according to claim 13 , wherein the powder is obtainable by a method for producing a nutritional powder, comprising fat, an emulsifier, digestible carbohydrates, and proteinaceous material, comprising the steps of
a. preparing a liquid containing the digestible carbohydrate and the emulsifier in water by adding the digestible carbohydrate and the emulsifier consecutively or simultaneously to water at a temperature of between 50 and 90 deg C., optionally using a homogenization step; b. providing a fat ingredient containing at least one fat; c. combining the liquid and the fat ingredient to provide a pre-emulsion; d. performing a homogenization step to homogenize the pre-emulsion to form an emulsion, and optionally increasing the dry matter content of the emulsion by a concentration step; e. spray drying the emulsion obtained in step d to provide a base powder; f. optionally further drying the base powder of step e;
wherein the emulsifier is octenylsuccinyl anhydride substituted starch (OSA starch),
wherein the fat content of the base powder is at least 32 wt % on total dry weight of the base powder, wherein the free fat content is less than 3 wt % based on total weight of the fat,
g. adding one or more dry ingredients by dry blending, to obtain the nutritional powder,

wherein the nutritional powder is an infant formula, follow-on formula or growing-up milk,
wherein the nutritional powder comprises 40-60 wt. % of the base powder,
wherein the nutritional powder contains 95-100 wt. % amino acids based on total proteinaceous material.

15 . A method for preventing, reducing and treating allergy or in preventing, reducing and treating metabolic disorders in a subject, comprising administering the composition according to claim 13 to the subject.

Assignees

• Nutricia Nv

Inventors

• Del Rayo Hernandez Sanchez Maria
• Van Der Wel Jordan Nicolaas

Classifications

• A61K47/44

  Oils, fats or waxes according to two or more groups of A61K47/02-A61K47/42; Natural or modified natural oils, fats or waxes, e.g. castor oil, polyethoxylated castor oil, montan wax, lignite, shellac, rosin, beeswax or lanolin (synthetic glycerides, e.g. medium-chain triglycerides, A61K47/14) · CPC title

• A61K47/36

  Polysaccharides; Derivatives thereof, e.g. gums, starch, alginate, dextrin, hyaluronic acid, chitosan, inulin, agar or pectin · CPC title

• A61K31/202

  having three or more double bonds, e.g. linolenic (eicosanoids, e.g. leukotrienes A61K31/557) · CPC title

• A23L33/40

  Complete food formulations for specific consumer groups or specific purposes, e.g. infant formula · CPC title

• A23L29/219

  Chemically modified starch; Reaction or complexation products of starch with other chemicals · CPC title