Process for forming particles

Patent metadata

Field	Value
Publication number	US-12428527-B2
Application number	US-202217831812-A
Country	US
Kind code	B2
Filing date	Jun 3, 2022
Priority date	Jun 3, 2022
Publication date	Sep 30, 2025
Grant date	Sep 30, 2025

Abstract

A process for forming particles. The process includes a step of entraining gas into a precursor material, wherein the gas includes from about 50 vol % to about 100 vol % argon and from about 0 vol % to about 50 vol % other constituents. The precursor material is deposited onto a moving conveyor. The precursor material is cooled to form a plurality of particles.

First claim

What is claimed is:

1. A process for forming particles comprising the steps of:
providing a precursor material ( 20 ) to a feed pipe ( 40 );
entraining gas into said precursor material, wherein said gas comprises from about 50 vol % to about 100 vol % argon and from about 0 vol % to about 50 vol % other constituents;
providing a distributor ( 30 ) comprising a plurality of apertures ( 60 );
transporting said precursor material ( 20 ) from said feed pipe to said distributor;
passing said precursor material through said apertures;
providing a moveable conveyor ( 80 ) beneath said apertures;
depositing said precursor material onto said moveable conveyor; and
cooling said precursor material to form a plurality of particles ( 90 ).

2. The process according to claim 1 , wherein said distributor comprises:
a stator ( 100 ) in fluid communication with said feed pipe;
a cylinder ( 110 ) rotationally mounted about said stator and rotatable about a longitudinal axis (L) of said cylinder, wherein said cylinder has a periphery ( 120 ) and said cylinder comprises said plurality of apertures disposed about said periphery, wherein said apertures are intermittently in fluid communication with said stator as said cylinder rotates about said stator.

3. The process according to claim 2 , further comprising the step of milling said precursor material after the step of entraining gas into said precursor material.

4. The process according to claim 3 , wherein said step of milling said precursor material after the step of entraining gas into said precursor material is performed with an in-line rotor-stator mill.

5. The process according to claim 1 , wherein said gas is entrained as a mixture of gasses.

6. The process according to claim 5 , wherein said mixture of gasses is from a container containing a mixture of said gas.

7. The process according to claim 1 , wherein said argon is provided from a primary container ( 157 a ) and said other constituents of said gas are provided from one or more secondary containers ( 157 b ).

8. The process according to claim 7 , wherein said argon and said other constituents of said gas are combined into a single flow of said gas prior to being entrained into said precursor material.

9. The process according to claim 8 wherein said other constituents of said gas are provided as air from said secondary container.

10. The process according to claim 1 , wherein said argon is entrained at a pressure greater than 2 bars at a minimum flow rate of about 0.5 liters/min.

11. The process according to claim 1 , wherein more than 50 vol % of said other constituents are less soluble in said precursor material than said argon.

12. The process according to claim 1 , wherein said precursor material comprises more than about 20% by weight water soluble polymer.

13. The process according to claim 12 , wherein said water soluble polymer is selected from:
a polyalkylene polymer of formula H—(C 2 H 4 O)—(CH(CH 3 )CH 2 O) y —(C 2 H 4 O) z —OH wherein x is from 50 to 300, y is from 20 to 100, and z is from 10 to 200;
a polyethylene glycol fatty acid ester of formula (C 2 H 4 O) q —C(O)O—(CH 2 ) r —CH 3 wherein q is from 20 to 200 and r is from 10 to 30;
a polyethylene glycol fatty alcohol ether of formula HO—(C 2 H 4 O) s —(CH 2 ) t )—CH 3 wherein s is from 30 to 250 and t is from 10 to 30;
C8-C22 alkyl polyalkoxylate comprising more than 40 alkoxylate units;
polyethylene glycol having a weight average molecular weight from 2000 to 15000;
EO/PO/EO block copolymer;
PO/EO/PO block copolymer;
EO/PO block copolymer;
PO/EO block copolymer;
polypropylene glycol;
ethoxylated nonionic surfactant having a degree of ethoxylation greater than 30;
polyvinyl alcohol;
polyalkylene glycol having a weight average molecular weight from 2000 to 15000; and
mixtures thereof.

14. The process according to claim 1 , wherein said precursor material comprises polyethylene glycol having a weight average molecular weight from about 2000 to about 13000.

15. The process according to claim 1 , wherein said precursor material comprises more than about 40% by weight polyethylene glycol.

16. The process according to claim 1 , wherein said particles have an individual mass between about 0.1 mg to about 2 g.

17. The process according to claim 1 , wherein said precursor material comprises from about 0.1% to about 20% by weight perfume.

18. The process according to claim 1 , wherein the step of cooling said precursor material is conducted by way of ambient cooling.

19. The process according to claim 1 , wherein said precursor material is provided to said feed pipe from a batch mixer ( 10 ).

20. The process according to claim 1 , wherein said other constituents are selected from of oxygen, nitrogen, carbon dioxide, and mixtures thereof.

Assignees

• Procter & Gamble

Inventors

• Huddleston Richard Albert
• Quan Ke Ming

Classifications

• C11D17/06

  Powder; Flakes; Free-flowing mixtures; Sheets · CPC title

• C08J2353/00

  Characterised by the use of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers · CPC title

• C08J2329/04

  Polyvinyl alcohol; Partially hydrolysed homopolymers or copolymers of esters of unsaturated alcohols with saturated carboxylic acids · CPC title

• C08J9/122

  Hydrogen, oxygen, CO2, nitrogen or noble gases · CPC title

• C11D2111/14

  Hard surfaces · CPC title