Particle size distribution measurement method, particle size distribution measurement device, and calculation device

Patent metadata

Field	Value
Publication number	US-12411068-B2
Application number	US-202117925038-A
Country	US
Kind code	B2
Filing date	Mar 23, 2021
Priority date	May 27, 2020
Publication date	Sep 9, 2025
Grant date	Sep 9, 2025

Abstract

A particle size distribution measurement method includes: an image acquisition step of acquiring a first CT image of a target sample including the granules; a statistical value calculation step of specifying a region of interest by dividing the acquired first CT image into predetermined grids, and calculating a first statistical value including a grid statistical value for each of the grids and an overall statistical value of the entire first CT image regarding a CT value; and a measurement step of measuring a particle size distribution of the granules in the target sample based on the first statistical value and a second statistical value including a grid statistical value and an overall statistical value of a type same as the grid statistical value and the overall statistical value included in the first statistical value in a second CT image of a standard sample including granules having a known particle size.

First claim

The invention claimed is:

1. A particle size distribution measurement method for measuring a particle size distribution of granules having an unknown particle size distribution, the particle size distribution measurement method comprising:
an imaging step of obtaining a first CT image of a target sample including the granules by X-ray CT and a second CT image of a standard sample including granules having a known particle size by X-ray CT;
an image acquisition step of acquiring the first CT image of the target sample including the granules;
a statistical value calculation step of specifying a region of interest by dividing the acquired first CT image into predetermined grids, and calculating a first statistical value including a grid statistical value for each of the grids and an overall statistical value of the entire first CT image regarding a CT value; and
a measurement step including a particle size distribution measurement step of measuring a particle size distribution of the granules in the target sample based on a second statistical value and the first statistical value, the second statistical value including a grid statistical value and an overall statistical value of a type same as the grid statistical value and the overall statistical value included in the first statistical value in the second CT image of a standard sample including granules having the known particle size.

2. The particle size distribution measurement method according to claim 1 , wherein
in the particle size distribution measurement step, the particle size distribution is measured by comparing the first statistical value with a correlation between the second statistical value and a particle size.

3. The particle size distribution measurement method according to claim 2 , wherein
the grid statistical value includes at least one of a maximum value, a minimum value, an average value, and a variance of the CT value,
the overall statistical value includes at least one of a deviation of the variance in the entire first CT image and an average of the variance in the entire first CT image, and
the correlation includes at least one of a first correlation between the average value of the CT value and the particle size, a second correlation between the maximum value of the CT value and the particle size, a third correlation between the deviation of the variance of the CT value and the particle size, and a fourth correlation between the average of the variance and the particle size.

4. The particle size distribution measurement method according to claim 1 , wherein:
the imaging step of obtaining the first CT by X-ray CT is performed using an X-ray having a first energy lower than a second energy of an X-ray in X-ray CT for obtaining the second CT image, wherein
in the particle size distribution measurement step, the particle size distribution is measured based on the first statistical value in the first CT image obtained by the X-ray having the first energy and the second statistical value in the second CT image obtained by the X-ray having the second energy.

5. The particle size distribution measurement method according to claim 4 , wherein
in the particle size distribution measurement step, the particle size distribution is primarily measured based on the first statistical value and a third statistical value in a third CT image obtained by the X-ray having the first energy for the standard sample, and secondary measurement of the particle size distribution is further performed based on the second statistical value in the second CT image for the primarily measured particle size distribution.

6. The particle size distribution measurement method according to claim 1 , wherein
the statistical value calculation step is performed a plurality of times such that the grids have different sizes, and
a removing step of removing an inclusion having a particle size equal to or larger than the size of the grids based on a plurality of the first statistical values acquired based on the grids having different sizes is further included.

7. The particle size distribution measurement method according to claim 1 , wherein
in the statistical value calculation step, the granules in the target sample are specified in the first CT image, and the region of interest in the first CT image is specified by applying a region growth method to a specified portion.

8. The particle size distribution measurement method according to claim 1 , wherein
the granules contain soil.

9. The particle size distribution measurement method according to claim 8 , wherein
the measurement step further includes a moisture content measurement step of measuring a moisture content of the granules.

10. The particle size distribution measurement method according to claim 9 , wherein
in the moisture content measurement step, the moisture content is measured by comparing the first statistical value with a correlation between the second statistical value and the moisture content.

11. The particle size distribution measurement method according to claim 10 , wherein
the grid statistical value includes at least one of a maximum value, a minimum value, an average value, and a variance of the CT value,
the overall statistical value includes at least one of a deviation of the variance in the entire first CT image, and an average of the variance in the entire first CT image, and
the correlation includes at least one of a fifth correlation between the deviation of the variance of the CT value and the moisture content, a sixth correlation between the average value of the CT value and the moisture content, and a seventh correlation between the minimum value of the CT value and the particle size.

12. A particle size distribution measurement device configured to measure a particle size distribution of granules having an unknown particle size distribution, the particle size distribution measurement device comprising:
an X-ray CT device configured to obtain a first CT image of a target sample including the granules by X-ray CT and a second CT image of a standard sample including granules having a known particle size by X-ray CT;
a calculation device including an image acquisition unit configured to acquire the first CT image of the target sample including the granules, a statistical value calculation unit configured to specify a region of interest by dividing the acquired first CT image into predetermined grids and calculate a first statistical value including a grid statistical value for each of the grids and an overall statistical value of the entire first CT image regarding a CT value, and a measurement unit including a particle size distribution measurement unit configured to measure a particle size distribution of the granules in the target sample based on a second statistical value and the first statistical value, the second statistical value including a grid statistical value and an overall statistical value of a type same as the grid statistical value and the overall statistical value included in the first statistical value in the second CT image of a standard sample including granules having the known particle size.

13. A calculation device configured to analyze a particle size distribution of granules having an unknown particle size distribution, the calculation device comprising:
an imaging unit configured to obtain a first CT image of a target sample including the granules by X-ray CT and a second CT image of a standard sample including granules having a known particle size by X-ray CT;
an image acquisition unit configured to acquire the first CT image of the target sample including the granules;
a statistical value calcu

Assignees

• Hitachi High Tech Corp
• Nat Institutes For Cultural Heritage

Inventors

• Takagi Hiroyuki
• Murata Taisuke

Classifications

• G01N2223/419

  computed tomograph · CPC title

• G01N2223/04

  and measuring absorption · CPC title

• G01N23/083

  the radiation being X-rays · CPC title

• G01N23/046 Primary

  using tomography, e.g. computed tomography [CT] · CPC title

• G01N15/1433

  using image recognition · CPC title