Process for making a glossy finish sandwich composite

Patent metadata

Field	Value
Publication number	US-12397479-B2
Application number	US-201917312780-A
Country	US
Kind code	B2
Filing date	Aug 16, 2019
Priority date	Dec 14, 2018
Publication date	Aug 26, 2025
Grant date	Aug 26, 2025

Abstract

The present invention provides a glossy finish sandwich composite, comprising face sheet as skin element and a core element; wherein, the skin element is a composite selected from the group consisting of inorganic industrial waste particulates reinforced polymeric composite; fibres reinforced polymeric composite; and fibres and particulate reinforced hybrid polymer composite; wherein, the core element is selected from the group consisting of polyurethane foam and wastes reinforced polymeric material. The present invention also provides a novel process for developing glossy finish high performance hybrid sandwich composite(s). Moreover, the sandwich composite(s) of the present invention are unique materials which have versatile applications in wider spectrum of utility in sustainable manner and address issues on waste management, effective utilisation of renewable resources and agro-wastes.

First claim

We claim:

1. A process for making a glossy finish sandwich composite, the process comprising the steps of:
a. dry and wet processing of inorganic industrial waste particulates, wherein the inorganic industrial waste particulates are selected from a group consisting of marble waste, fly ash, lime, gypsum rich wastes mineral, metallurgical, chemical, fertiliser wastes, glass fibre reinforced plastic (GRP) waste and silica fume waste, to obtain processed inorganic industrial waste particulates; dry and wet processing of chopped natural fibres and synthetic fibres, wherein the natural fibres are selected from a group consisting of sisal fibre, jute fibre, banana fibre, flax, cotton, and hemp fibres, followed by hot air curing to obtain the processed natural and synthetic fibres;
b. homogeneous mixing of the processed inorganic industrial waste particulates and the processed natural and synthetic fibres with a polymer selected from a group consisting of epoxy resin, polyester and polyurethane resin, along with a catalyst to prepare a glossy finish reinforced polymeric skin composite material;
C. casting the glossy finish reinforced polymeric skin composite material under compression moulding to form first and second glossy finish reinforced polymeric skin composite sheets;
d. demoulding the first and second glossy finish reinforced polymeric skin composite sheet;
e. curing the first and second glossy finish reinforced polymeric skin composite sheet of step d in a natural or a hot air oven;
f. subjecting polyurethane foam to injection moulding or subjecting agro-wastes reinforced polymeric materials to compressive moulding to form an inner core material between the first and second glossy finish reinforced polymeric skin composite sheets of step e to obtain a glossy finish sandwich composite;
g. casting the glossy finish sandwich composite of step f under compression moulding; and
h. demoulding the glossy finish sandwich composite of step g and curing the glossy finish sandwich composite in a hot air oven.

2. The process as claimed in claim 1 , wherein the inorganic industrial waste particulates are processed using hot water, mechanical grinding and hot air oven curing at 60-80° C. for 2-24 hours; and the processed inorganic industrial waste particulates have a size in a range of 2.0-200 μm, density in a range of 0.85-1.87 g/cc, porosity in a range of 30-68% and water holding capacity in a range of 25 to 110%; and the chopped natural fibres and synthetic fibres are processed using hot water and hot air curing at 60-105° C. for 2-24 hours; and the processed natural and synthetic fibres have a density in a range of 1.25-1.45 g/cc, elongation in a range of 0.3-5.0%, tensile strength in a range of 250-650 MPa and Young's modulus in a range of 5-35 GPa.

3. The process as claimed in claim 1 , wherein 20-80 wt % of the processed inorganic industrial waste particulates and 2-15% processed natural and synthetic fibres are homogeneously mixed with the polymer to prepare the glossy finish reinforced polymeric skin composite material.

4. The process as claimed in claim 1 , wherein the polymer of step b is an epoxy resin or a polyester resin in a volume ratio ranging from 15-35%, and wherein the catalyst is selected from methyl ethyl ketone peroxide (MEKP) and cobalt naphthenate (0.5-5 wt %).

5. The process as claimed in claim 1 , wherein the mixing in step b is performed at a rate of 400-4000 rpm.

6. The process as claimed in claim 1 , wherein the casting is performed at a temperature in a range of 16±2° C. -75±2° C. and a pressure in a range of 2-295 kg/cm 2 ; and the curing in hot air oven is performed at a temperature in a range of 60 -120° C. for 2-24 hours.

7. The process as claimed in claim 1 , wherein the polymer of step b is polyurethane resin in a volume ratio ranging from 20-80 wt %, and wherein the catalyst is poly-isocyanate in a range of 0.5-5 wt %.

Assignees

• Council Scient Ind Res

Inventors

• Pappu Asokan
• GUPTA Manoj Kumar
• Mishra Alka
• Peters Edward
• Kulshreshth Ajay
• Rathore Sanjai Kumar Singh
• Srivastava Avanish Kumar

Classifications

• B29C45/14508

  Joining juxtaposed sheet-like articles, e.g. for making trim panels · CPC title

• B29L2007/002

  Panels; Plates; Sheets · CPC title

• B29K2105/26

  Scrap {or recycled material} · CPC title

• B29K2075/00

  Use of {PU, i.e.} polyureas or polyurethanes {or derivatives thereof}, as moulding material · CPC title

• B29C70/48

  and impregnating the reinforcements in the closed mould, e.g. resin transfer moulding [RTM] {, e.g. by vacuum} · CPC title