Treatment method for oily sludge and method for soil remediation

Patent metadata

Field	Value
Publication number	US-12371360-B2
Application number	US-202218041580-A
Country	US
Kind code	B2
Filing date	Oct 17, 2022
Priority date	Apr 8, 2022
Publication date	Jul 29, 2025
Grant date	Jul 29, 2025

Abstract

The present disclosure provides a treatment method for oily sludge and a method for soil remediation. The treatment method for oily sludge includes: mixing the oily sludge with target biochar uniformly according to a first preset mass ratio, and conducting catalytic pyrolysis at a first preset temperature to achieve efficient removal of petroleum hydrocarbons, to obtain a pyrolysis residue used for soil remediation. In the present disclosure, the method realizes resource utilization and harmless utilization of the pyrolysis residue.

First claim

What is claimed is:

1. A treatment method for oily sludge, comprising:
mixing the oily sludge with a target biochar uniformly according to a first preset mass ratio, and conducting catalytic pyrolysis at a first preset temperature to obtain a pyrolysis residue used for soil remediation, wherein
the target biochar has a specific surface area of 14.09 m 2 /g, a pore volume of 0.0359 cm 2 /g, an average pore size of 3.169 nm; and a surface of the target biochar has functional groups;
a preparation method of the target biochar comprises:
subjecting a biomass raw material to anaerobic pyrolysis at a second preset temperature to obtain the target biochar, wherein
the biomass raw material comprises at least one of the following: waste edible fungus residues, distiller's grains, livestock and poultry manure, moldy biomass, fruit shells, straw, wood chips, and bamboo chips.

2. The method according to claim 1 , wherein the second preset temperature comprises 600° C. to 900° C.

3. The method according to claim 2 , wherein the second preset temperature is 600° C., 700° C., 800° C., or 900° C.

4. The method according to claim 1 , wherein the biomass raw material has a particle size of 20 mesh to 40 mesh.

5. The method according to claim 1 , wherein a gas atmosphere of the anaerobic pyrolysis comprises an inert gas atmosphere, and the inert gas comprises at least one or a combination of two or more selected from the group consisting of nitrogen, argon, ammonia, and carbon dioxide.

6. The method according to claim 1 , wherein the first preset temperature ranges from 350° C. to 550° C.

7. The method according to claim 6 , wherein the first preset temperature is 350° C., 400° C., 450° C., or 500° C.

8. The method according to claim 1 , wherein the first preset mass ratio is 8:1 to 1:1.

9. The method according to claim 8 , wherein the first preset mass ratio is 8:1, 7:1, 6:1, 5:1, 4:1, 3:1, 2:1, or 1:1.

10. A pyrolysis residue obtained by the treatment method according to claim 1 .

11. A method for soil remediation using the pyrolysis residue according to claim 10 , comprising:
mixing the pyrolysis residue with polluted soil uniformly according to a second preset mass ratio to remediate the polluted soil.

12. The method according to claim 11 , wherein the second preset mass ratio comprises a dry basis mass ratio, and the dry basis mass ratio is 5:95 to 30:70.

13. The method according to claim 12 , wherein the dry basis mass ratio is 5:95, 10:90, 10:70, or 30:70.

Assignees

• Univ Tianjin
• Univ Tianjin Commerce

Inventors

• Chen Guanyi
• Lin Fawei
• Cheng Zhanjun
• Li Jiantao
• Yan Beibei
• Cui Xiaoqiang
• Li Ning

Classifications

• C10B53/02

  of cellulose-containing material (production of pyroligneous acid C10C5/00) · CPC title

• C02F2103/365

  from petrochemical industry (e.g. refineries) · CPC title

• C02F2101/32

  Hydrocarbons, e.g. oil · CPC title

• B09C1/08 Primary

  chemically · CPC title

• B09C1/06

  thermally · CPC title