Method for adjusting an oxygen production unit with different set points for each adsorber

Patent metadata

Field	Value
Publication number	US-12370491-B2
Application number	US-202017613597-A
Country	US
Kind code	B2
Filing date	May 12, 2020
Priority date	May 23, 2019
Publication date	Jul 29, 2025
Grant date	Jul 29, 2025

Abstract

A method for adjusting a gas stream separation unit having N adsorbers, where N≥2, each following a PSA, VSA or VPSA adsorption cycle, with a time lag of a phase time, said adjustment method including continuously measuring a physical parameter associated with the gas stream entering and/or leaving the adsorber; for at least one step of the adsorption cycle, determining at least one characteristic value of the step chosen in step a) which is selected from the values of the physical parameter measured in step a) or a function of those values; comparing this characteristic value with a target value; and modifying the flow of the gas stream in order to obtain the target value, in the event of a variation between the value of this (these) difference(s) and the target values.

First claim

The invention claimed is:

1. A method for adjusting a gas stream separation unit comprising N adsorbers, where N≥2, each following a PSA, VSA or VPSA adsorption cycle, with a time lag of a phase time, said adjustment method comprising the following steps:
continuously measuring a physical parameter associated with the gas a) stream entering and/or leaving the adsorber; for at least one phase of the adsorption cycle, wherein the physical parameter comprises at least one value,
b) determining at least one characteristic value of the physical parameter measured in step a) or a function of the physical parameter;
c) comparing this characteristic value with a target value; thereby determining a value variation, wherein the target value is a pressure or a pressure difference, and
d) modifying the flow of the gas stream whereby the characteristic value is equal the target value,
where steps a) to d) are performed for each adsorber, and
where at least one adsorber has a unique target value that differs from the target value of the other adsorbers,
the target value is in the form: X+delta Xi, where X is a value common to all the adsorbers and delta Xi is a correction to be made to said common value for the adsorber (i),
the target values being pressures or pressure differences, and said target values being the desired values at the adsorption cycle completion.

2. The method according to claim 1 , wherein the target value is determined using adsorption process simulation software, taking into account the specific characteristics of each adsorber.

3. The method according to claim 1 , wherein, before step a), a step of determining the target value for each adsorber is carried out.

4. The method according to claim 1 , wherein the target value is re-assessed periodically.

5. The method according to claim 2 , wherein the target value is determined, by calculation or experimentally, using optimal search software in a multivariable process.

6. A gas stream separation unit comprising at least two adsorbers A and B which follow a PSA, VSA or VPSA pressure cycle and having means for implementing the method of adjusting the unit according to claim 1 .

7. The gas stream separation unit according to claim 6 , wherein the gas stream is chosen from atmospheric air, a gas containing hydrogen, a gas containing CO2 or a gas containing CO, where said unit is designed to produce, respectively, a stream enriched with oxygen, hydrogen or helium, CO2, CO or methane.

Assignees

• Air Liquide
• Air Liquide

Inventors

• Monereau Christian
• Bigot David
• Dehestru Marie

Classifications

• B01D2259/403

  using three beds · CPC title

• B01D2259/40009

  using sensors or gas analysers · CPC title

• B01D2256/12

  Oxygen · CPC title

• B01D53/0446

  Means for feeding or distributing gases · CPC title

• Y02P20/156

  Methane [CH4] · CPC title