Isostatic pressure spark plasma sintering (IP-SPS) net shaping of components using nanostructured materials

Patent metadata

Field	Value
Publication number	US-12358050-B2
Application number	US-202117909301-A
Country	US
Kind code	B2
Filing date	Mar 3, 2021
Priority date	Mar 4, 2020
Publication date	Jul 15, 2025
Grant date	Jul 15, 2025

Abstract

A method of forming a consolidated component having a complex shape includes providing a first component having a first shape similar to the complex shape. The method further includes placing the first component in a chamber and surrounding the first component with a medium. The method further includes applying pressure and at least one of heat or electricity into the chamber to process the first component to form a consolidated component having the complex shape.

First claim

What is claimed is:

1. A method of forming a consolidated component having a complex shape, the method comprising:
providing a first component comprising at least one nanostructured material, wherein the first component has a first shape similar to the complex shape;
placing the first component in a chamber and surrounding the first component with a medium, wherein the medium comprises a fine spherical graphite powder; and
applying pressure and electrical current into the chamber to process the first component to form a consolidated component having the complex shape.

2. The method of claim 1 , wherein applying pressure includes applying pressure uniaxially to the medium, wherein the medium converts the uniaxial pressure into isostatic pressure that is applied to the first component.

3. The method of claim 2 , wherein the isostatic pressure that is applied to the first component provides relatively uniform shrinkage and consolidation of the first component to cause the consolidated component to have the complex shape.

4. The method of claim 1 , wherein providing the first component includes forming the first component using at least one of injection molding, mold powder casting, or net-shape sintering.

5. The method of claim 1 , wherein the medium has a greater compressive strength than the first component.

6. The method of claim 1 , wherein the first component includes a plurality of first components, and applying pressure and electrical current includes applying pressure and electrical current to the chamber while the plurality of first components are in the chamber to form multiple consolidated components, simultaneously.

7. The method of claim 1 , wherein the chamber is a die chamber located inside of a spark plasma sintering (SPS) chamber, and applying pressure and electrical current includes applying uniaxial pressure and high temperature plasma to the die chamber using SPS.

8. The method of claim 7 , wherein placing the first component in the chamber and surrounding the first component with the medium includes placing the first component in the die chamber, surrounding the first component with the medium, and placing the die chamber with the first component and the medium in the SPS chamber.

9. The method of claim 8 , further comprising:
removing an SPS die from the SPS chamber;
removing the medium from the SPS die; and
reusing the medium during a subsequent iteration of the method.

10. A system for forming a consolidated component, the system comprising:
a chamber configured to receive a first component comprising at least one nanostructured material and medium such that the medium surrounds the first component, wherein the medium comprises a fine spherical graphite powder;
a pressure source configured to apply pressure to the chamber; and
an electrical current source configured to apply electrical current to the chamber such that the pressure and the electrical current are applied to the first component via the medium to consolidate the first component.

11. The system of claim 10 , wherein the pressure source is configured to apply the pressure uniaxially to the medium, wherein the medium converts the uniaxial pressure into isostatic pressure that is applied to the first component.

12. The system of claim 10 , wherein the medium has a greater compressive strength than the first component.

13. The method of claim 1 , wherein the at least one nanostructured material comprises nanocrystalline powder with grain sizes below 100 nm.

14. The system of claim 11 , wherein the isostatic pressure that is applied to the first component provides relatively uniform shrinkage and consolidation of the first component to cause the consolidated component to have the complex shape.

15. The system of claim 10 , wherein the first component is formed using at least one of injection molding, mold powder casting, or net-shape sintering.

16. The system of claim 10 , wherein the chamber is configured to receive a plurality of first components, and when the pressure source applies pressure and the electrical current source applies electrical current to the chamber, the plurality of first components in the chamber form multiple consolidated components, simultaneously.

17. The system of claim 10 , wherein the chamber is a die chamber located inside of a spark plasma sintering (SPS) chamber, and wherein applying pressure and electrical current to the chamber includes applying uniaxial pressure and high temperature plasma to the die chamber using SPS.

18. The system of claim 17 , wherein the chamber receives the first component in the chamber by receiving the first component in the die chamber, surrounding the first component with the medium, and placing the die chamber with the first component and the medium in the SPS chamber.

19. The system of claim 18 , wherein the chamber is further configured to:
remove an SPS die from the SPS chamber;
remove the medium from the SPS die; and
reuse the medium during a subsequent iteration of forming a consolidated component.

20. The system of claim 10 , wherein the at least one nanostructured material comprises nanocrystalline powder with grain sizes below 100 nm.

Assignees

• Univ California
• Nat Tech & Eng Solutions Sandia Llc

Inventors

• Lavernia Enrique J
• Zheng Baolong
• Zhou Yizhang
• Monson Todd

Classifications

• B22F3/105 Primary

  by using electric current {other than for infrared radiant energy}, laser radiation or plasma (B22F3/11 takes precedence){; by ultrasonic bonding (B22F3/115 takes precedence)} · CPC title

• B22F1/054

  Nanosized particles · CPC title

• B22F1/065

  Spherical particles · CPC title

• B28B3/025

  Hot pressing, e.g. of ceramic materials · CPC title

• B28B3/086

  The rams working in different directions · CPC title