Maltodextrin and process of making same

Patent metadata

Field	Value
Publication number	US-12344682-B2
Application number	US-202318299303-A
Country	US
Kind code	B2
Filing date	Apr 12, 2023
Priority date	Aug 15, 2017
Publication date	Jul 1, 2025
Grant date	Jul 1, 2025

Abstract

This specification discloses process for obtaining maltodextrin having DE between 17 and 19.9 and the maltodextrins obtained from the process. The disclosed maltodextrins can be provided as a powder or in shelf stable liquid form. The disclose maltodextrins have a polysaccharide profile similar to those observed for prior art maltodextrins, but make maltodextrin solutions having a high solids content, but reduced viscosity compared to prior art maltodextrins, on equivalent solids-in-solution basis. The process combines adds an alpha-amylase and a pullulanase enzyme to a polysaccharide mixture during a saccharification step. The disclosed maltodextrins make solutions at 50° C. and greater than 65% on a solids dry solids basis having a viscosity between 5,000 and 12,000 cP and having a water activity of less than 0.80.

First claim

The invention claimed is:

1. A process for making maltodextrin from starch, comprising:
applying a liquefaction step comprising adding an acid or an enzyme to an aqueous starch mixture in sufficient amount to hydrolyze the starch to obtain a mixture comprising polysaccharides; and
applying a saccharification step comprising adding an alpha-amylase and a pullulanase to sufficiently hydrolyze the polysaccharides in the mixture to obtain maltodextrin;
wherein the maltodextrin, when in powdered form, has a DE from 17 to 19.9.
wherein the maltodextrin, when in powdered form, has a distribution of polysaccharides comprising less than 5% by weight polysaccharides having DP1, between 4% and 10% by weight polysaccharides having DP2, between 9% and 14% by weight polysaccharides having DP3, and between 75% and 82% by weight polysaccharides having DP4+ of at least 4.

2. The process of claim 1 wherein the liquefaction step comprises adding an acid in sufficient amount such that the pH of the aqueous starch mixture is between 1.8 and 2.2.

3. The process of claim 1 wherein the liquefaction step comprises adding an alpha-amylase in a concentration ranging from 0.05 to 0.80 g of enzyme per kg of starch on a dry basis, and hydrolyzing the starch in the aqueous starch mixture at a temperature between 90°° C. and 110° C. and at a pH ranging from 6.0 to 7.0.

4. The process of claim 1 wherein the liquefaction step runs until the polysaccharide mixture has a DE ranging from 13 to 17.

5. The process of claim 1 further comprising, during the saccharification step, adding to the polysaccharide mixture the alpha-amylase in an amount ranging from 0.01 to 0.05 g per kg of starch on a dry basis and the pullulanase in an amount ranging from 0.30 to 0.60 g per kg of starch on a dry basis, and hydrolyzing the polysaccharides in the mixture at a temperature ranging from 40° C. to 60° C. and at a pH ranging from 4.0 to 7.5, for a time of between 2 and 12 hours.

6. The process of claim 1 comprising, during the saccharification step, adding to the polysaccharide mixture the alpha-amylase in an amount ranging from 0.01 to 0.05 g per kg of starch on a dry basis and the pullulanase in an amount ranging from 0.30 to 0.60 g per kg of starch on a dry basis, and hydrolyzing the polysaccharides in the mixture at a temperature ranging from 40° C. to 60° C. and at a pH ranging from 4.0 to 7.5, for a time of between 2 and 7 hours.

7. The process of claim 1 wherein the liquefaction step is a single dosage liquefaction.

8. The process of claim 1 wherein the liquefaction step is a double dosages liquefaction.

9. The process of claim 1 wherein a maltodextrin solution comprising at least 78% by weight of the maltodextrin on a dry solids basis has a viscosity of between 5,000 and 12,000 cP as measured at 50° C. using a rapid visco analyzer.

10. The process of claim 1 wherein the starch is selected from the group consisting of: corn starch, wheat starch, tapioca starch, potato starch, sweet potato starch, sago starch, barley starch, rice starch, heat/acid treated starch, dextrin, pearl starch, waxy corn starch, sorghum starch, high amylose corn starch and liquid dextrose of high solid content and combinations thereof.

11. The process of claim 1 wherein the starch is a chemically unmodified starch.

Assignees

• Corn Products Dev Inc

Inventors

• Arnoni Laercio
• Bertoli Jose
• Yamamoto Walter

Classifications

• C12P19/22

  produced by the action of a beta-amylase, e.g. maltose · CPC title

• C12P19/16

  produced by the action of an alpha-1, 6-glucosidase, e.g. amylose, debranched amylopectin (non-biological hydrolysis of starch C08B30/00) · CPC title

• C12P19/04

  Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds · CPC title

• C12N9/2457

  Pullulanase (3.2.1.41) · CPC title

• C12N9/2414

  Alpha-amylase (3.2.1.1.) · CPC title