Neutralization/water separation tank for esterified product and neutralization/water separation method for esterified product

Patent metadata

Field	Value
Publication number	US-12337262-B2
Application number	US-202017605184-A
Country	US
Kind code	B2
Filing date	Jul 1, 2020
Priority date	Sep 19, 2019
Publication date	Jun 24, 2025
Grant date	Jun 24, 2025

Abstract

A neutralization/water separation tank for an esterified product including: a neutralization part in which a crude product mixture containing alcohol and an ester compound, a neutralizing agent, and water are put to produce a neutralized mixture; a water separation part which divides the neutralized mixture into a floating layer and an aqueous layer; a first partition wall which extends upward from a bottom surface to provide an upper passage and by which the neutralization part and the water separation part are partitioned; and a second partition wall which extends downward from a ceiling to provide a lower passage, wherein the water separation part includes: a first water separation part into which the neutralized mixture is introduced from the neutralization part through the upper passage; and a second water separation part into which the neutralized mixture is introduced from the first water separation part through the lower passage, wherein the first water separation part and the second water separation part are partitioned by the second partition wall.

First claim

The invention claimed is:

1. A neutralization/water separation tank for an esterified product, comprising:
a neutralization part in which a crude product mixture containing alcohol and an ester compound, a neutralizing agent, and water are put to produce a neutralized mixture;
a water separation part which divides the neutralized mixture into a floating layer and an aqueous layer;
a first partition wall which extends upward from a bottom surface of the neutralization/water separation tank to provide an upper passage and by which the neutralization part and the water separation part are partitioned; and
a second partition wall which extends downward from a ceiling of the neutralization/water separation tank to provide a lower passage,
wherein the water separation part comprises:
a first water separation part into which the neutralized mixture is introduced from the neutralization part through the upper passage; and
a second water separation part into which the neutralized mixture is introduced from the first water separation part through the lower passage,

wherein the first water separation part and the second water separation part are partitioned by the second partition wall,
wherein the neutralization/water separation tank for an esterified product further comprises:
a first discharge pump that discharges a resultant product contained in the floating layer from a sidewall of the second water separation part to the outside;
a second discharge pump that discharges a precipitated salt contained in the aqueous layer from a bottom surface of the water separation part to the outside; and
a circulation pump that discharges the neutralized mixture from the neutralization part and put the neutralized mixture again into the neutralization part,

wherein a bottom surface of the water separation part is gradually inclined downward toward a center thereof,
wherein the second discharge pump is connected to the center of the bottom surface of the water separation part, and
wherein the upper passage has a height of 10% to 50% of a height of the first partition wall.

2. The neutralization/water separation tank for an esterified product of claim 1 , further comprising a propeller stirrer installed in the neutralization part to stir the neutralized mixture.

3. The neutralization/water separation tank for an esterified product of claim 1 , wherein the inclination has a range of 5° to 45°.

4. The neutralization/water separation tank for an esterified product of claim 1 , wherein a bottom surface of the neutralization part is gradually inclined downward toward a center thereof.

5. The neutralization/water separation tank for an esterified product of claim 1 , wherein the lower passage has a height of 10% to 50% of a height of the second partition wall.

Assignees

• Lg Chemical Ltd

Inventors

• Choo Yeon Uk
• Lee Sung Kyu
• Kim Hyun Kyu
• Jin Chan Hyu
• Jun Hyoung
• Park Jin Sung

Classifications

• C07B63/00

  Purification; Separation (separation of optically-active compounds C07B57/00); Stabilisation; Use of additives · CPC title

• C02F2301/046

  Recirculation with an external loop · CPC title

• C02F2101/34

  containing oxygen · CPC title

• C02F2001/007

  Processes including a sedimentation step · CPC title

• C02F1/40

  Devices for separating or removing fatty or oily substances or similar floating material (cleaning or keeping clear the surface of open water from oil or like materials E02B15/04; devices in sewers for separating liquid or solid substances from sewage E03F5/14, e.g. for use in drains leading to the sewer E03F5/16) · CPC title